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PS-3220

 Assembling the Titration Setup (See figure on next page)

13

013-16026A

Other Titrations

Titrations with different solutions can be performed using the same equipment and procedure. Other probes (such 

as conductivity or ORP) can be used in place of the pH probe.

Theory of Operation

The Wireless Drop Counter uses an infrared light source and a photodetec

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tor. Lenses spread the light into a “sheet” and refocus it onto the photode

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tector. When a drop of fluid passes through the Wireless Drop Counter, it 

partially blocks this sheet of light, and the photodetector registers a 

momentary decrease in light intensity.
The Wireless Drop Counter uses infrared light and ignores visible light. On 

power up, it automatically adjusts the light level for the best sensitivity. Use 

the Wireless Drop Counter away from direct sunlight or other sources of 

infrared that may interfere with it.

Troubleshooting the Sensor 

If the sensor loses Bluetooth connection and will not reconnect, try cycling the ON button. Press and briefly 

hold

 the button until the status LEDs blink in sequence, and then release the button. Start the sensor in the 

usual way.

If the sensor stops communicating with the computer software or tablet application, try restarting the software 
or application. If the problem remains, press and 

hold

 the ON button on the sensor for 10 seconds and then 

release. Start the sensor in the usual way.

On the computing device, turn Bluetooth off and then back on. Retry.

If the Wireless Drop Counter will not turn on, use the micro USB cable to connect it to a USB port or charger.

See the PASCO web site at www.pasco.com for more information.

Probe Care and Maintenance

The Wireless Drop Counter Sensor is splash resistant but not waterproof. Do not immerse the sensor in liquid. If 
the inside surfaces of the rectangular drop window need to be cleaned, Use a piece of lens paper or a lint free cloth 
and water or a glass cleaner. 

Tips

Except for opening and closing the stopcocks, do not touch the syringe of the Drop Dispenser during the 
titration; otherwise, the drop size may change significantly.

The drop rate must remain approximately constant (for example, about 2 drops per second) in order for the 
drop size to remain constant.

Drop size depends on the exact position of the stopcock valves. Therefore, the average drop size will be 
different for every titration. For each different titration, re-calibrate the sensor because the new titrant may have 
different sized drops if it has a different density.

Problem

Cause

Solution

Indicator light flashes twice for a single 
drop. Wireless Drop Counter registers 
more drops than actually dispensed.

Fluid is splashing back into the drop 
window.

Adjust the position of the beaker, 
Wireless Drop Counter, or Drop 
Dispenser to eliminate splash back

Indicator LED remains on constantly. 
Wireless Drop Counter does not register 
drops.

Lenses in drop window are dirty or 
wet.

Clean lenses in the drop window with 
water or a glass cleaner and dry with a 
cotton swab or tissue.

detector

collimating

lens

focusing 
lens

sheet of light

drop

infrared light 

source

Summary of Contents for PS-3214

Page 1: ...Reference Guide 013 16026A Wireless Drop Counter PS 3214 a b d c e f Power Rechargeable Battery or USB Cable Connection...

Page 2: ...t or smart phone when the sensor is connected PASCO Capstone will work on a PC or Mac The Wireless Drop Counter can be mounted on a support rod The counter is equipped with two integrated probe holder...

Page 3: ...blocking the drop window To turn the sensor on press and hold the ON button When the battery status LED shines red for a moment release the ON button Then the Bluetooth status LED will blink This ind...

Page 4: ...elp from the Help menu or press F1 LED Information The drop LED operates as follows The drop LED blinks when a drop is detected passing through the drop window If the lens in the drop window becomes o...

Page 5: ...in the liquid in the beaker Assemble the Drop Dispenser 1 Remove the plunger from the syringe Remove the protective white plastic caps from the stopcock valves 2 Connect the two stopcocks together Con...

Page 6: ...e figure on next 6 013 16026A Syringe with 50 mL of 0 1 M NaOH Wireless pH Sensor Direct Connect pH Probe Wireless Drop Counter Drop Tip Stopcock Stopcock Syringe Holder Support Rod Micro Stir Bar Mag...

Page 7: ...drops from the drop tip and give you a measure of the volume 5 Start Capstone Pair the Wireless Drop Counter wirelessly to the computing device e g computer In Capstone open the Hardware Setup window...

Page 8: ...om stopcock so that the drops fall at a rate of about 1 drop per second Close the top valve after the rate is achieved Discard the titrant as directed by your instructor 4 Align the drop tip with the...

Page 9: ...me is the measurement selected as default The Templates window also opens with Graph Table and Graph and Digits as the choices 8 In the Templates window touch or click the Graph template to open a Gra...

Page 10: ...e that the Fluid Volume measurement also has a Calibrate measurement icon 10 Click or touch the Calibrate measurement icon to open the Calibrate Sensor Select Measurement window 11 In the Calibrate Se...

Page 11: ...the number of drops as they are counted 13 After about 5 mL of titrant has collected in the graduated cylinder close the bottom stopcock Carefully measure the exact volume of titrant in the graduated...

Page 12: ...ibrate Acid Base Titration Calibration Method 1 Setup the equipment and consumables as shown 2 Start the data acquisition software 3 In the software pair connect the Wireless Drop Counter and a Wirele...

Page 13: ...d then back on Retry If the Wireless Drop Counter will not turn on use the micro USB cable to connect it to a USB port or charger See the PASCO web site at www pasco com for more information Probe Car...

Page 14: ...e that it will be recycled in a manner that protects human health and the environment To find out where you can drop off your waste equipment for recycling please contact your local waste recycle disp...

Page 15: ...he System Report button Select Bluetooth from the sidebar on the left underneath Hardware Scan down the list of information until you find LMP Version If your Mac is equipped with Bluetooth SMART the...

Page 16: ...Wireless Drop Counter Appendix A Bluetooth Compatibility 16 013 16026A...

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