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Instruction Manual: EMP-3

NIC-TD-0000067-01

Nippon Instruments Corporation

6.5.4.4 CALIBRATION PROCEDURE

(1)

Press “MENU” and then “Maintenance”.

(2)

Proceed to the “Calibration/Manufacturer” screen.

(3)

Enter the password.

(4)

The following screen will be displayed. Press “Calibrate”.

(5)

Press the numerical button.

(6)

Enter a standard gas concentration to be used for calibration, and press “Enter”.

Button

Description

Cancel

Cancellation of alteration

Clear

Deletion of all characters

Enter

Determination

Deletion of one character

Summary of Contents for EMP-3

Page 1: ...Portable Mercury Survey Meter EMP 3 INSTRUCTION MANUAL NIC TD 0000067 01 NIPPON INSTRUMENTS CORPORATION...

Page 2: ...FRONT 8 3 INSTALLATION 9 4 MEASUREMENT 10 MEASUREMENT FLOWCHART 10 NECESSITIES FOR MEASUREMENT 11 ARTICLES RECOMMENDED FOR MEASUREMENT 11 PREPARATION FOR MEASUREMENT 12 4 4 1 CHARGING AND CONNECTION O...

Page 3: ...S OF ICONS 33 5 3 2 2 ALTERATIONS OF SCALES CONCENTRATION AND TIME 33 MENU SCREEN 35 5 4 1 CONSTITUTION OF MENU 35 5 4 2 HANDLING OF DATA 36 5 4 2 1 SAVING OF DATA 36 5 4 2 2 CHECK DATA 36 5 4 2 3 EXP...

Page 4: ...FOR PREPARATION OF STANDARD GAS 68 6 5 4 2 CALCULATION PROCEDURE FOR STANDARD GAS CONCENTRATION 69 6 5 4 3 MERCURY QUANTITY IN STANDARD GAS 70 6 5 4 4 CALIBRATION PROCEDURE 71 7 DETAILED SYSTEM SPECIF...

Page 5: ...dust and exposure to rainfall or liquid Observe the installation requirements and installation procedure Otherwise a failure may result Do not install the instrument within a 10 m radius from another...

Page 6: ...used out of the specification range a failure may occur Do not give a shock to the instrument by dropping throwing or the like The limit of fall height is 3cm Do not apply a strong external force to t...

Page 7: ...cibly or use the battery when its lifetime has expired Wipe off dust attached around the power plug and terminals Otherwise a fire may result The battery life decreases because of the self discharge e...

Page 8: ...TD 0000067 01 Nippon Instruments Corporation 4 If the instrument is discarded inadequately environmental pollution or personal damage may result Dispose of it according to the regulations or rules of...

Page 9: ...able Main use is measurement of mercury concentration in working environment and in petroleum gas When option is connected it is also possible to measure liquid samples and high concentration mercury...

Page 10: ...onsists of the cycle of the ZERO check and mercury concentration measurement ZERO Check Sample gas passes through the ZERO filter that adsorbs mercury and gas that does not contain mercury hereinafter...

Page 11: ...nt power 2 LCD Unit With Touch Screen A measurement concentration can be displayed and measuring conditions can be set 3 Inlet Connection for the probe and main unit 4 Probe A filter is connected to t...

Page 12: ...nal contact input output cables 3 USB Memory Connection It is possible to connect a USB memory to export data 4 RS 232C Cable Connection It is possible to connect an RS 232C cable This is used to conn...

Page 13: ...edure Otherwise a failure may result Do not install the instrument within a 10 m radius from another instrument that generates noise such as a high output electric power instrument high frequency inst...

Page 14: ...or carries out Turning On of Power MENU Setting Checking and Alteration of Settings Measurement Mode Gas to Be Measured Temperature Atmospheric Pressure Adjust Initial Adjustment of Instrument Measure...

Page 15: ...n 11 NECESSITIES FOR MEASUREMENT 1 Battery 2 Battery Charger 3 Probe 4 USB Memory ARTICLES RECOMMENDED FOR MEASUREMENT 1 Spare Battery 2 Long Probe 3 Tedlar Bag used to collect sample gas and to prepa...

Page 16: ...wise a fire may result The battery life decreases because of the self discharge even when the battery is not used Check the remaining of battery life before a measurement When the battery has been lef...

Page 17: ...o the dedicated battery charger and charge it Please set the battery charger to 1 0A 2 When the charging is completed the color of the charging lamp of the battery charger changes from red to green 3...

Page 18: ...onnection of the probe is completed Otherwise fine particles will enter the instrument and accurate measurements may become impossible When attaching the probe take care not to damage the probe connec...

Page 19: ...requirements and installation procedure Otherwise a failure may result When carrying the instrument put the belt on the shoulder opposite from the instrument attach the waist belt too Otherwise a fail...

Page 20: ...displayed for 30 seconds or so 3 When the startup is completed characters STANDBY appear and warming up for 10 minutes starts At this point of time check the remaining battery life on the screen If th...

Page 21: ...me conditions settings need not be made again It is also possible to make settings when STANDBY is displayed 4 5 2 1 SETTING OF MEASUREMENT MODE 1 Select MENU 2 Select Setting 3 At Meas Mode select a...

Page 22: ...red from Ambient and NG LPG Ambient Ambient air NG LPG Liquefied natural gas or liquefied petroleum gas In the case of the measurement of gas with small specific gravity select NG LPG The measurement...

Page 23: ...anges the concentration of contained mercury also changes The concentration is converted into a mercury gas concentration in the standard condition generally 0 C and 1 atm so that it is not influenced...

Page 24: ...e has been displayed Default Setting 101 3 kPa 7 Enter an atmospheric pressure in the measurement environment and press Enter for determination From a difference from the set pressure the pressure of...

Page 25: ...ation in an environment with high temperature and humidity or with much dust and exposure to rainfall or liquid Observe the range of the specification If the instrument is used out of the specificatio...

Page 26: ...t an instrument adjustment is carried out for 30 seconds immediately after a measurement start Adjust Instrument Adjustment Flow of Measurement MOBILE Mode STATIC Mode Meas Gas NG LPG ZERO Check Mercu...

Page 27: ...ry concentration 0 g Nm3 is automatically corrected The time required for the ZERO check is automatically determined by the mercury concentration measured in the previous cycle During that time Zero C...

Page 28: ...0000067 01 Nippon Instruments Corporation 24 4 5 3 3 CHECKING OF DATA A measurement result is displayed Check data It is possible to switch the screen to Numeric or Graph Refer to 5 3 MEASUREMENT SCR...

Page 29: ...It is impossible to obtain the correct measurement value unless the influence of interfering components is eliminated If the concentrations of interfering components do not change in the one cycle of...

Page 30: ...rift Press Filter and return to the measurement Other Than 0 g Nm3 There is interference by interfering components The interference of the displayed value has been detected Or there are drift Terminat...

Page 31: ...Corporation 27 4 5 3 5 TERMINATION OF MEASUREMENT When the STOP button is pressed the measurement is terminated 1 Hold down the power button for three seconds or more 2 The following confirmation scr...

Page 32: ...se the instrument in a draft chamber or connect the outlet and draft chamber or exhaust duct using a tube to discharge the gas 1 Install the instrument in a draft chamber or connect the outlet and dra...

Page 33: ...le setup and data Each screen can be started by pressing START or MENU on the main screen Graph Numeric STOP Sample Filter Scale Check Data Export Data Delete Data Data Handling Maintenance Setting Me...

Page 34: ...by long pressing the screen When the screen has been locked all buttons become invalid 4 Remaining Battery Life Icon The remaining battery life is displayed This is not displayed when the AC adapter...

Page 35: ...Level Meter An instantaneous value is visually displayed using a bar It is possible to change the display range using Scale This is displayed in yellow when the value approaches the alarm value and in...

Page 36: ...imum of the scale Press the numerical button of an item to be set 3 Enter a value to be set and press Enter Presettable Range Max 9 9 2100 g Nm3 Min 10 2099 9 g Nm3 The presettable range change accord...

Page 37: ...of the time series graph to arbitrary ranges 1 Press Scale No Name Description 1 Time Series Mercury Concentrations Measurement values are displayed as a time series It is possible to change the disp...

Page 38: ...value to be set and press Enter Presettable Range Max 9 9 2100 g Nm3 Min 10 2099 9 g Nm3 The presettable range change according to the each input value Time duration 1 100 min Time duration must be gr...

Page 39: ...items When any button is pressed the detailed screen appears Button Description Check Data Checking of measurement data Export Data Output of measurement data to a USB memory Delete Data Deletion of...

Page 40: ...to data items to be saved The measurement numbers are the same as those displayed on the measurement screen Data items are saved in the same folder until the instrument is turned off Refer to 5 5 MEAS...

Page 41: ...sible to change the maximum and minimum of the concentration axis and the time duration of the time axis Press the numerical button of an item to be changed 6 Enter a value to be set and press Enter P...

Page 42: ...uments Corporation 38 Button Description Cancel Cancellation of alteration Clear Deletion of all characters Enter Determination BS Deletion of one character 7 Press OK to return to the time series gra...

Page 43: ...pen the cover of the external interface unit and insert the supplied USB memory into the USB port When the USB memory has been recognized correctly the following icon appears in the lower left part of...

Page 44: ...e free space is insufficient delete data 1 Press Delete Data on the menu screen 2 Press a folder name to select a folder to be deleted After the selection the color of the cell changes To select all f...

Page 45: ...and STATIC can be used Select a mode according to application Measurement Mode Usage Resolution Measurement Time MOBILE Portable use 1 g Nm3 Normal 290 sec STATIC Stationary use 0 1 g Nm3 High sensit...

Page 46: ...concentration 1 Press the numerical button 2 Enter a value to be set and press Enter Presettable Range 0 2000 g Nm3 Button Description Cancel Cancellation of alteration Clear Deletion of all characte...

Page 47: ...s In the case of the measurement of hydrocarbon gas select NG LPG The measurement of NG LPG is possible only in the STATIC mode Even if MOBILE has been selected Meas Mode becomes STATIC when NG LPG is...

Page 48: ...he numerical button 2 Enter a reference temperature and press Enter for determination Presettable Temperature Range 10 C to 99 C Button Description Cancel Cancellation of alteration Clear Deletion of...

Page 49: ...rement gas is calculated and a correction is made By setting Ambient Press according to the altitude etc of the measurement environment a more accurate normalization correction can be made Saving Inte...

Page 50: ...ming Default Setting 5 min 1 Press the numerical button 2 Enter a time to be set and press Enter for determination Presettable Range 0 99 min Button Description Cancel Cancellation of alteration Clear...

Page 51: ...ing 75 1 Press the numerical button 2 Slide the slider bar to adjust the brightness Press OK for determination GPS Choose whether GPS data is acquired or not Default Setting Off When ON is set positio...

Page 52: ...n of an item to be set 3 Enter a date or a time and press Enter for determination Presettable Range Year 2000 2037 Hour 0 23 Month 1 12 Minute 0 59 Day 1 31 Second 0 59 Button Description Cancel Cance...

Page 53: ...he replacement of the ZERO filter refer to REPLACEMENT OF ZERO FILTER Be sure to press RESET after the replacement Refer to 6 5 1 REPLACEMENT OF ZERO FILTER When the free space of the micro SD card is...

Page 54: ...3 ADJUSTMENT OF OPTICAL SYSTEM Although the voltages are adjusted properly at the time of a shipment if the inside of the instrument is contaminated because of use during a long period of time or the...

Page 55: ...re version 2 SN Serial number 3 Input 1 Information on Contact Input 1 ON is displayed when the signal is received and OFF is displayed in other cases 4 Input 2 Information on Contact Input 2 ON is di...

Page 56: ...ring initialization Searching Searching for satellites Received Receiving completed Receive Error The receiving error has occurred 2 Latitude Acquired latitude 3 Longitude Acquired longitude 4 Satelli...

Page 57: ...eck 2 Lamp The lamp is turned on and off 3 OUTPUT1 Used to check the signal manually Turning on and off of Contact Output 1 On Signal output Off No signal 4 Buzzer Operation check of the buzzer functi...

Page 58: ...067 01 Nippon Instruments Corporation 54 5 4 4 6 CALIBRATION MANUFACTURER This screen is for simplified calibration and manufacturer setting When doing a simplified calibration consult with our agent...

Page 59: ...e When a measurement is started at 10 30 00 on October 1 2018 the folder name is 20181001_103000 Processing from START to STOP is defined as one measurement and sequential measurement numbers starting...

Page 60: ...he storage capacity shall be sufficient Check it using GLP Refer to 5 4 4 1 GLP Extract data and delete unnecessary data Refer to 5 4 2 3 EXPORT DATA and 5 4 2 4 DELETE DATA Checking at Time of Measur...

Page 61: ...Replacement by our agent or service department is necessary Air Pump 2 years or 2 000 operation hours Replacement by our agent or service department is necessary ZERO Filter 6 months or 80 g of adsor...

Page 62: ...XX XX Displayed for 10 minutes after the instrument is turned on Lamp Life Exceeded Displayed when the lamp lighting up time has exceeded 2000 hours The replacement of the lamp by our agent or service...

Page 63: ...heck the environmental temperature at which the instrument is used It is impossible to use the EMP 3 when the environmental temperature is lower than 0 C Refrain from using the instrument If this erro...

Page 64: ...a warning is issued during a measurement suspend the measurement immediately and replace the filter 1 Open the bottom cover of the EMP 3 2 Remove the ZERO filter Dispose of the removed ZERO filter as...

Page 65: ...Instruction Manual EMP 3 NIC TD 0000067 01 Nippon Instruments Corporation 61 6 Press RESET on GLP Total Hg of the GLP counter is cleared 7 Press Exit to return to the measurement screen...

Page 66: ...The name and criterion of replacement of each component of the probe are as follows No Name Recommended Replacement Period and Criterion 1 Probe Filter 1 month or 500 operation hours 2 Probe Tube 3 m...

Page 67: ...may break If it is difficult to remove them tear the probe tube little by little using a cutter and remove them In that case take care not to get hurt or damage the probe connector 3 Connect a new pr...

Page 68: ...ument 2 Press MENU and then Maintenance 3 Proceed to the Ref Sig Voltage screen 6 5 3 1 AUTOMATIC ADJUSTMENT The voltages are automatically adjusted to 2 5 V Both reference voltage and signal voltage...

Page 69: ...L ADJUST 2 An adjustment screen appears Make an adjustment for SPAN Make an adjustment by changing each voltage gradually by one step at a time using the up and down arrow buttons The adjustment range...

Page 70: ...adjustment to minimize each voltage 5 Press OK The voltages are fixed If Cancel is pressed instead of OK the adjusted voltages will not be set 6 Press Exit to return to the previous screen At the tim...

Page 71: ...he instrument may not be obtained 3 When the signal voltage or reference voltage is 1 0 V or less When only the signal voltage has lowered the inside of the instrument has possibly been contaminated I...

Page 72: ...hat can suck at 1 L min and has a flow control function with precision of 5 or more 1 Adjust the flow rate of the PS 4 or pump to 1 L min beforehand After the flow rate adjustment turn off and on the...

Page 73: ...3 mL of mercury gas has been extracted Gas air has been injected into a Tedlar Bag for three minutes using the PS 4 at a flow rate of 1 L min Since the temperature of the MB 1 is 25 C the concentratio...

Page 74: ...10 693 10 783 10 873 10 964 11 056 18 0 11 148 11 242 11 337 11 433 11 529 11 626 11 724 11 823 11 922 12 022 19 0 12 123 12 225 12 328 12 432 12 536 12 641 12 747 12 854 12 961 13 070 20 0 13 179 13...

Page 75: ...e Calibration Manufacturer screen 3 Enter the password 4 The following screen will be displayed Press Calibrate 5 Press the numerical button 6 Enter a standard gas concentration to be used for calibra...

Page 76: ...ratio F of the measurement value MEASURE to the concentration of the prepared standard gas STD is within the range of 0 67 F 1 5 the calibration is completed and the new F value is recorded When the F...

Page 77: ...m3 STATIC 0 1 g Nm3 Precision RSD 3 2 g Nm3 or more 90 Response Time Within 5sec Measurement Time MOBILE 290 sec About 5min cycle STATIC 50 sec About 1min cycle Measurement Flow Rate Approximately 1 L...

Page 78: ...been no touch operation for a predetermined time the screen brightness is automatically decreased Alarm Function It is possible to set an alarm value 0 to 2000 g Nm3 for the built in buzzer GPS Functi...

Page 79: ...1 Probe Dedicated probe for extracting measurement gas 1 Probe Filter Spare part for replacement of filter housed in probe 1 Probe Connector Spare part for replacement of probe joint 1 Probe Tube Spa...

Page 80: ...n body The above shall not be applied to the MOBILE mode Installation Location Shall be horizontal and have sufficient strength The above shall not be applied to the MOBILE mode MEASURES AGAINST ELECT...

Page 81: ...onal act Consumable that has been consumed or component the life of which has expired 10 CAUTIONS CONCERNING DISPOSAL OF INSTRUMENT If the instrument is discarded inadequately environmental pollution...

Page 82: ...TD 0000067 01 Nippon Instruments Corporation 78 11 CONTACT ADDRESS NIPPON INSTRUMENTS CORPORATION URL https www hg nic com Service Department 14 8 Akaoji cho Takatsuki shi Osaka 569 1146 Japan Phone 0...

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