Operation
Agilent Sample Introduction Pump System SIPS 10/20 User’s Guide
45
b
You can choose to use
Auto set standards
,
Manually entered
standards
or
User premixed standards
as the calibration
mode.
4
On the
Measurement
page, enter a value for the
Read Delay
.
This represents the time required to pump solutions introduced
with SIPS through the pump tubing to the T-piece.
5
On the
Standards
page (if you are using Auto set standards):
a
Enter the concentration of the standard to be used for the
calibration in the
Bulk standard concentration
field.
b
Enter the number of standards to be used for the calibration
in the
Standard count
field.
6
Fill in the remaining pages as required and click
OK
.
7
Switch to the
Analysis
window.
8
Ensure the diluent tubing is connected to the Mariotte vessel
then select
Calibration
from the
Instrument
menu. Select the
method you want to calibrate and click
OK
. The blank is
measured automatically.
9
At the prompt for the standard (if the
Sampling Mode
selected
for the method is manual), place the pump tubing in the bulk
standard and press
Read
. SIPS will prepare the number of
standards specified in the method.
SIPS 20
To calibrate a method using SIPS 20:
1
Develop or modify a method as described previously for SIPS 10
with the following exceptions:
a
On the
SIPS
page, select
Bulk Standard
in the
Right Pump
group.
b
Place the tubing from the right pump in the bulk standard.
(The left pump will only be used for samples.)
2
Proceed with the Autocalibration from Step 8 of the SIPS 10
procedure, above.
