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SCD and NCD User Manual
7
Performance Verification
Septum purge
15 mL/min
Detector
Base temperature
280°C
Burner temperature
900 °C
Chiller temperature
On
H
2
flow
3 mL/min
Oxidizer flow
8 mL/min, Oxygen
O3 Generator
On
O3 Generator flow
On
Vacuum pump
On
Oven
Initial temp
50 °C
Initial time
3.0 min
Rate 1
25 °C/min
Ramp 1 temp
250 °C
Ramp 1 hold time
2 min
Post run temp
50 °C
ALS settings (if installed)
Sample washes
2
Sample pumps
6
Sample wash volume
8 µL (maximum)
Injection volume
1 µL
Syringe size
10 µL
Solvent A pre washes
0
Solvent A post washes
3
Solvent A wash volume
8 µL (maximum)
Solvent B pre washes
0
Solvent B post washes
3
Solvent B wash volume
8 µL (maximum)
Injection mode (7693A)
Normal
Airgap Volume (7693A)
0
Viscosity delay
0
Table 15
NCD Checkout conditions (continued)