Performance Verification
7
SCD and NCD User Manual
111
Burner temperature
800 °C
Upper H
2
flow
38 mL/min
Lower H
2
flow
8 mL/min
Oxidizer flow
50 mL/min, Air
O3 Generator
On
O3 Generator flow
On
Vacuum pump
On
FID-SCD Tandem settings
FID temp
350 °C
FID hydrogen flow
35 mL/min
FID air flow
500 mL/min
FID N
2
makeup flow
20 mL/min
SCD oxidizer flow
0
SCD upper H
2
flow
40 mL/min
Lower H
2
flow
Not applicable for FID-SCD
Oven
Initial temp
50 °C
Initial time
3.0 min
Rate 1
25 °C/min
Ramp 1 temp
160 °C
Ramp 1 hold time
2 min
Post run temp
50 °C
ALS settings (if installed)
Sample washes
2
Sample pumps
6
Sample wash volume
8 µL (maximum)
Injection volume
1 µL
Syringe size
10 µL
Solvent A pre washes
0
Solvent A post washes
3
Solvent A wash volume
8 µL (maximum)
Solvent B pre washes
0
Table 14
SCD Checkout conditions (continued)