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USER MANUAL | ICOS | INSTRUCTIONS | UM/ICOS-EN REV. B.2

Integration of the measured spectra with the measured values of:



Gas temperature



Gas pressure



Path length



Line strength of the probed transition

Enables you to determine the mole fraction directly from the relation:

Use this equation to determine gas concentrations, even in hostile environments without
using calibration gases or reference standards. These values are measured:



Mixtures containing several species



Flows at elevated temperatures and pressures

Summary of Contents for GLA451

Page 1: ... ABB MEASUREMENT ANALYTICS USER MANUAL User Manual ICOS GLA451 Enhanced Performance QC Benchtop Analyzers ...

Page 2: ... 12 1 Analyzer Overview 13 Performance Specifications 13 Ambient Humidity 13 Operating Temperature 13 Maximum Altitude 13 Power Requirements 13 Fuse Ratings 13 Cable Plugs and Voltage for EC Countries 13 External Dimensions 14 Weight 14 Standard Components 15 Optional Components 15 Power Connections 18 Data Interface Connection Ports 19 Plumbing Diagram 20 Standard Plumbing 20 Plumbing Diagram for...

Page 3: ...e Transfer Menu 45 Standard Data File 45 Transfer Data Files 46 Types of directories in the local hard drive 48 Daily Directory 48 Archive Directory 49 File Transfer Error Screen 50 Setup Menu 51 Time Files Tab 52 Calibration Tab 55 Laser Adjust Tab 57 MIU tab 60 Analog Output Tab 61 DCS Tab 62 Service Tab 63 Shutting Down the Analyzer 64 4 Maintenance 65 Daily Operation Checklist 65 Mirror Ring D...

Page 4: ... G Fast Flow Operation 100 Appendix H Batch Mode Operation 105 Appendix I Spectrum Displays 115 GLA451 AAQC Enhanced Performance QC Benchtop Trace Ammonia Analyzer 115 GLA451 N2OI2 Enhanced Performance QC Benchtop Isotopic Nitrous Oxide Analyzer 116 GLA451 N2OI3 Enhanced Performance QC Benchtop Isotopic Nitrous Oxide Analyzer 117 GLA451 OCS Enhanced Performance QC Benchtop Carbonyl Sulfide Analyze...

Page 5: ... corrections Cybersecurity This product is designed to be connected to and to communicate information and data via a network interface It is your sole responsibility to provide and continuously ensure a secure connection between the product and your network or any other network as the case may be You shall establish and maintain any appropriate measures such as but not limited to the installation ...

Page 6: ...fications Symbols Standards Tested and Met 2004 108 EU EMC EN61326 1 Title 21 Code of Federal Regulations chapter 1 sub chapter J WEEE Directive The analyzer is not subject to WEEE Directive 2002 96 EC Waste Electrical and Electronic Equipment or relevant national laws e g ElektroG in Germany The product must be disposed of at a specialized recycling facility Do not use municipal garbage collectio...

Page 7: ...r runs safely without risk to the operator Modifying the analyzer to operate with the case cover open can injure personnel Bypassing the analyzer interlock switch to open the case cover during analyzer operations can cause serious bodily injury Even though the analyzer provides a second layer of protection such as a laser cover to prevent the user from the invisible laser beam or any secondary ref...

Page 8: ...aintenance instructions and maintenance kits Make sure the analyzer is unplugged before working with the internal components Failure to do so may result in damage to the analyzer and electric shock Safety Provisions for a Chemical Spill Follow these precautions when dealing with all chemicals Keep all chemical containers away from heat sparks and open flames Use only on grounded equipment and with...

Page 9: ...t that you type in fields and also button choices that you enter Warning Icons Table 2 shows and describes the warning icons used in this manual Table 2 Warning Icon Descriptions Icon Meaning Emphasizes facts and conditions important to analyzer operation WARNING General Warning Icon gives general safety information that must be followed to avoid hazardous conditions WARNING Electrical Warning Ico...

Page 10: ...f factory service or repair is needed Table 3 lists and describes the safety icons on ABB LGR shipping boxes Follow these instructions when transporting and storing boxed analyzers Table 3 Transportation and Storage Icon Descriptions Icon Meaning Store your analyzer in a sheltered dry area Do not let the box get wet Transport and store the analyzer box with the arrows on the box pointing up The an...

Page 11: ...ng transportation to ABB LGR is at customer s expense 5 No charge repair parts may be sent at ABB LGR s sole discretion to the purchaser for installation by purchaser 6 ABB LGR s liability is limited to repair or replace any part of the analyzer free of charge if ABB LGR s examination discloses the part to be defective The laws of some locations may not allow the exclusion or limitation on implied...

Page 12: ...sued RMA number must be prominently displayed on the return package No returns will be accepted collect or C O D On all warranty returns ABB LGR will pay the shipping charges on the return of the merchandise to the customer Customer Support ABB provides product support services worldwide To receive product support either in or out of warranty contact the ABB office that serves your geographical ar...

Page 13: ...rts per thousand This analyzer is a Class 1 laser product Performance Specifications Ambient Humidity 99 relative humidity non condensing Operating Temperature 0 45o C Maximum Altitude 6 000 Feet Power Requirements 115 230 VAC 50 60 hz 400 Watts steady state Fuse Ratings 250 VAC 10 Amps Cable Plugs and Voltage for EC Countries See page 115 Always use the power supply cord provided by ABB LGR See p...

Page 14: ...USER MANUAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 14 External Dimensions 16 H x 17 W x 45 D Weight 68 kg ...

Page 15: ... modem type Exhaust muffler Applicable for isotopic analyzers Pretreatment box Optional Components Available on select analyzers Multiport Inlet Unit o Multiport Inlet Unit o Power cable o 25 pin control signal cable Batch Injection System o Syringe injection port o 100 mL syringe o Centering needle o Septa box of 50 o Septum puller External pump System o External pump o Pump power cord o Teflon c...

Page 16: ...B 2 16 This analyzer has been CE certified using data cables three meters long or less Connecting the analyzer using longer data cables is not recommended If you have not received all of these components contact ABB LGR at icos support ca abb com ...

Page 17: ...RUCTIONS UM ICOS EN REV B 2 17 Figure 2 shows the front of the analyzer Figure 2 Front Panel Figure 3 shows the back of the analyzer with connections Port locations may vary for different analyzer types Figure 3 Back Panel ...

Page 18: ...ge Selection Toggles the input voltage to the analyzer s power supply between 115 VAC and 230 VAC determined by the country where the analyzer is used Setting an incorrect voltage may damage the analyzer When changing the supply voltage verify that both the Analyzer is powered off or not connected to power AC voltage selection on the analyzer matches the AC voltage being supplied from your power s...

Page 19: ...hm USB ports Used for transferring data to a USB memory device or to connect a USB keyboard and mouse Ethernet port Connects the analyzer to a local area network LAN and allows access to the data directory using an external computer Serial port 9 pin D sub For real time digital measurement output Video port 15 pin D sub Connects an external monitor to the analyzer TO MIU port 25 pin data port For ...

Page 20: ...alyzer type and may not include an external pump For the GLA451 AAQC plumbing diagram refer to Figure 7 For standard operation the pump draws gas through the Sample Inlet port on the back panel of the analyzer The gas is filtered through a filter before entering the pressure controller which determines the analyzer flow rate The gas then travels through the optical cell and is exhausted through th...

Page 21: ...d through a Teflon Membrane filter The gas then travels through the optical cell and is exhausted through the Internal Pump Exhaust port 1 4 Swagelok Figure 7 shows the plumbing diagram for the GLA431 AAQC Figure 7 Plumbing diagram for the GLA431 AAQC Optional Fast Flow Mode Analyzers with fast flow capabilities external pump on internal pump off measure data at a higher flow rate Cap the Internal...

Page 22: ...s the compatible pump options Flow through times of the available external pumps ACC DP3H pump provides flow through 1 e time 1 2 seconds ACC DP4H pump provides flow through 1 e time 0 7 seconds Dry Scroll pump provides flow through 1 e time 0 1 seconds Table 5 describes the compatible pump options Table 5 Pump Options Modes of Operation Internal N920 N940 XDS 35 Remarks Standard Mode X X Fast Flo...

Page 23: ...TERNAL PUMP port must remain capped with the provided cap Exhaust ports for internal pumps The Internal Pump Exhaust port is located on the back panel of the analyzer It can either be connected to the provided muffler Figure 9 to expel exhaust into the room air or the exhaust can be routed to the facility ventilation system using tubing Figure 9 Exhaust Muffler External pump exhaust ports For opti...

Page 24: ...es a description of the warning labels Figure 11 shows the location of the labels on the analyzer Table 6 Warning Labels and Descriptions Label Description The laser is rated Class 3 invisible laser radiation when the housing is open Only trained maintenance personnel may open the analyzer housing General laser warning label Figure 11 Warning Label Locations ...

Page 25: ...ower cord If mounting the analyzer in an equipment rack no side clearance is required The analyzer is equipped with a three prong power plug The third prong of the facility electrical outlets must be grounded Failure to ground the third prong may result in electrical damage to the analyzer and electrical shock to the operator Emergency Shutdown Procedure If the analyzer malfunctions and requires e...

Page 26: ...nections 1 For the GLA451 N2OI2 GLA451 OCS GLA451 N2OI3 and GLA451 AAQC connect the provided exhaust muffler with Swagelok adaptor to the INTERNAL PUMP EXHAUST port to exhaust into the room air or route to your facility ventilation system using tubing Figure 12 Figure 12 Exhaust Muffler 2 If applicable connect a sample tube not provided from the INLET port on the back panel of the analyzer to your...

Page 27: ...ons to between 1 4 and 1 2 turn past finger tight Leave a gap of at least 3 5 mm as shown in Figure 13 2 Table 7 lists the Swagelok fitting sizes and recommended wrench sizes Figure 13 Swagelok Connection Gap Table 7 Recommended Wrench Sizes for Swagelok Fittings Swagelok Fitting Size Recommended Wrench Size 1 4 9 16 3 8 11 16 ...

Page 28: ...bbreviated name of the gas analyzer For example the GLA451 OCS button displays OCS Figure 16 b If you don t make a selection within 120 seconds the analyzer automatically defaults to the Main Panel Numeric display Figure 20 3 Click on the maintenance SERVICE button Figure 16 if you need more time or need to choose a maintenance setting Figure 17 Once a month the analyzer automatically performs a t...

Page 29: ...e the integrity check runs The integrity check runs for one to two minutes before launching the analyzer s control software Do not turn off the computer while the integrity check is running Figure 15 File System Integrity Check Screen Thermal Stabilization Run the analyzer for four hours before collecting data This allows the internal temperature to stabilize The exact final cell temperature will ...

Page 30: ...launch countdown to manually start recording measurements by clicking the launch button o The launch button is the abbreviated name of the gas analyzer For example the GLA451 OCS launch button displays OCS as shown in Figure 16 Open the auto launch window by clicking Service Turn off the analyzer by clicking Shutdown Figure 16 shows the Launch Service screen Figure 16 Launch Service Screen ...

Page 31: ...he Service button on the Launch Service screen From this interface you can Change the auto launch delay timing Transfer files from the internal hard drive to an external storage device connected via USB by clicking Files Restore the analyzer s factory settings by clicking Restore Figure 17 shows the Auto Launch Screen Figure 17 Auto Launch Screen ...

Page 32: ...n on the User Interface Control Bar Figure 18 Figure 18 Control Bar Security Button 2 For initial login use the default Linux credentials for the username and password Figure 19 as follows User lgr Password 3456789 If you change and forget this password you will not be able to recover it without a factory restore There is only one Linux account Figure 19 Login Dialog Box 3 Click Login ...

Page 33: ...lyzer is displayed at the bottom of the main panel Green The analyzer is functioning properly Yellow The data may not be reliable or maintenance is required soon Red The analyzer requires maintenance to correct an identified fault Refer to the Alarm Status Display section on pages 37 39 for detailed Temperature Status and Analyzer Status descriptions This panel contains the User Interface Control ...

Page 34: ...USER MANUAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 34 User Interface Control Bar Use the control bar to operate the analyzer Figure 21 User Interface Control Bar ...

Page 35: ...ts the rate at which data is written to the log file Figure 27 Parameter Window Displays the Time Current time Data File Current filename to log data Gas Temperature Temperature in Cell Celsius C Gas Pressure Pressure in Cell Torr Laser A τ Laser A ring down time micro seconds µs Laser B τ Laser B ring down time micro seconds µs o Only applicable for two laser systems MIU Multiport Inlet Unit Rate...

Page 36: ...eric Display The four displays within the display function are Numeric Alarm Spectrum Time Chart This section describes the displays Numeric Display The Numeric Display is the default display It appears when the analyzer is first turned on or re initialized Figure 22 shows an example of the Numeric Display screen It displays the numeric readout of the last measurements of gas at a specific concent...

Page 37: ...l status of the analyzer The Alarm Status is color coded Green The analyzer is functioning properly Yellow The data may not reliable or maintenance is required soon Red The analyzer requires maintenance to correct an identified fault Figure 23 shows the Alarm Status Display with all parameters functioning properly Figure 23 Alarm Status ...

Page 38: ...he operating temperature range 11 CROSS OVER 14 Analyzer Temp Temperature High Low Warning The temperature is the high warning set point The temperature is the low warning set point 17 Fault NaN reading Occurs when there is a false or undefined value NaN not a number 19 Dead Band 20 Acceptable Range No warning alarm No warning alarm If the Alarm Status is Yellow or Red please refer to the Maintena...

Page 39: ...d Occurs when laser signal power has degraded by 20 of the factory value 10 Maintenance Maintenance needed now Occurs when the analyzer requires maintenance every 381 days 11 CROSS OVER 12 Data Health A B Fit is not optimal The laser fitting condition is not optimal Occurs when residuals of fit go above normal operational values 13 Pressure Noisy Occurs when the specified operational pressure is n...

Page 40: ...lack circles and the peak fit resulting from signal analysis as a blue line For an analyzer that is a dual laser system there is a drop down selector in the lower right portion of the Spectrum Display that lets you toggle between the two lasers Laser 1 also referred to as laser A Laser 2 also referred to as laser B The measured concentrations are shown in parts per million ppm parts per billion pp...

Page 41: ... 25 shows a Spectrum Displays in dry air Figure 25 Spectrum Display Dry Air Table 10 Spectrum Displays for different analyzer types Analyzer Type Figure for Reference GLA451 AAQC Figure 115 GLA451 N2OI2 Figure 116 GLA451 N2OI3 Figure 117 GLA451 OCS Figure 118 ...

Page 42: ...tration vs time Figure 26 shows the Time Chart with a continuous flow of gas A 10 point running average in black is shown going through the raw data shown in blue Click on the drop down box in the lower right corner of either window to toggle between available gases and to adjust the number of significant figures The data is saved to the file indicated in the left corner of the parameter window Fi...

Page 43: ...ntrol adjustments to the operating mode and plot frequency Selections in this window will vary depending on analyzer type Figure 27 Rate Control Screen GLA451 N2OI3 The Operating Mode radio buttons allow you to change the rate at which data is written to the log file To adjust the rate 1 Click the Rate button clock icon on the User Interface Control Bar The Data Rate Control Adjustment panel appea...

Page 44: ...frequency 1 Click the Rate button clock icon on the User Interface Control Bar Figure 21 a The Data Rate Control Adjustment panel appears Figure 27 2 Click the Plot on Demand radio button to manually plot the data a When selected the Refresh Plot button appears on the Main Panel display When Refresh Plot button is selected current data is added to the Main Panel display 3 Click the Plot every Nth ...

Page 45: ...tten in text ASCII format and contain labeled columns displaying The time stamp of each recorded measurement Gas concentration Delta values if applicable Cell pressure Torr Cell temperature Celsius Ambient Temperature Celsius The format can be changed in the Time Files menu of the Setup panel Figure 35 Figure 28 shows a typical data file example Figure 28 The Beginning of a Typical Data File For e...

Page 46: ... Figure 29 Figure 29 File Transfer Menu Local Hard Drive left pane and USB Flash Drive right pane 4 Transfer data files from the analyzer hard drive to a USB storage device by dragging and dropping the files from the hard drive pane to the USB device pane Use the left mouse button to highlight one or multiple files in the window The directory windows default to the local hard drive on the left scr...

Page 47: ...ring files 5 Click the Unmount USB button Wait for the Safe to Remove USB Memory Device message before removing the USB memory device 6 Click Close to exit the File Transfer Menu Removing the USB memory device before seeing the Safe to Remove pop up message may result in loss of data ...

Page 48: ...ure 29 creates a daily folder containing new data files for each day that the analyzer operates To access the data files for a specific date double click the folder Each file from that day is displayed in chronological order Figure 30 Each file is a single zipped txt file using the following convention Example XXX_YYYY MM DD_f0000 txt zip Examples of files in the daily directory are shown in Figur...

Page 49: ...rganized by date Figure 31 To access the archived files double click the Archive folder Figure 29 Each file is a single zipped txt file using the following convention YYYY MM DD zip Each zipped file contains the data files for the day that the analyzer operated Examples of files in the archive directory are shown in Figure 31 Figure 31 Archive Directory ...

Page 50: ...EV B 2 50 File Transfer Error Screen The File Transfer Error screen Figure 32 displays when The USB Key does not have enough storage space The device is not recognized Try again with a correctly inserted USB device Figure 32 File Transfer Error ...

Page 51: ...ervices Selections in this menu will vary depending on analyzer type To enter Setup mode 1 Click the Setup button on the User Interface Control Bar Figure 33 Figure 33 Setup Button on the User Interface Control Bar 2 The default Time Files screen is displayed Figure 34 Figure 34 Setup Menu Tabs with Time Files Screen Selected ...

Page 52: ...ial Output Calibrate the analyzer to a local gas standard Enable the laser offset adjustment Configure the optional Multi Port Inlet Unit MIU Configure the optional External Dynamic Dilution System EDDS Service screen for technicians to check on the status of the analyzer Use these function tabs to make adjustments to the analyzer and its operation Time Files Tab The Time Files menu allows you to ...

Page 53: ... data files The available timestamp formats are shown in Table 11 New file creation intervals when running continuously can be set by adjusting the value in the Output Interval minutes spinner control box Table 11 Available Time Stamp Formats Time Stamp Name Format Absolute Local American mm dd yyyy hh mm ss sss Absolute Local European dd mm yyyy hh mm ss sss Absolute GMT American mm dd yyyy hh mm...

Page 54: ...arity Stop Bits The actual rate of the serial output is equal to the Logged File Rate i e 1 Hz divided by the Rate specified in the Time Files menu Use a null modem serial cable to connect the analyzer serial port to an external computer About The About section displays analyzer specific information such as the Build Date of the current software Version of the code IP Address Serial Number of the ...

Page 55: ... Interface Control Bar Figure 33 2 Select the Calibration tab at the top of the screen to enter the Calibration menu Figure 36 Figure 36 shows a example of the Calibration screen Figure 36 Calibration Setup Screen 3 On the top right panel of the screen under Reference Gas Settings select the checkbox next to the gas you want to calibrate For the GLA451 N2OI2 and GLA451 N2OI3 the N2O isotopes must ...

Page 56: ...right panel of the calibration screen as the analyzer performs the calibration Figure 37 shows the calibration process as a flow chart Figure 37 Calibration Flow 9 When the Calibration Complete message is displayed click the CLOSE button 10 Enter TimeChart by selecting the Display button on the User Interface Control Bar and verify that the displayed concentration correctly corresponds to your loc...

Page 57: ...t may be needed for the following reasons The laser s wavelength has drifted beyond the target range of the analyzer The analyzer is operated outside the recommended temperature range Figure 38 shows a example of the offset between absorption peaks and target lines For a 2 laser system both lasers are adjusted separately Figure 38 Absorption peaks off of target lines Laser voltage adjustment neede...

Page 58: ...ng the arrow buttons to shift the peaks until they are centered on their respective target lines a Up Arrow Peaks adjust to the right b Down Arrow Peaks adjust to the left 5 Deselect the Disable Laser Frequency Lock check box The software resumes automatic tracking and control of the laser wavelength 6 Click Close to exit the menu and return to the Main Panel Figure 39 and Figure 40 shows the lase...

Page 59: ...USER MANUAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 59 Figure 40 Absorption Peaks Centered Correctly on Target Lines Ambient Air ...

Page 60: ...d configuration These ports are directed to the inlet port of the analyzer for sampling unknown gases and reference gases The MIU menu can be configured to control which gases are introduced to the analyzer and for how long Figure 41 See Appendix E Multi Port Inlet Unit on page 90 for detailed instructions on configuring and controlling the MIU Figure 41 Control Menu for the Optional Multi Port In...

Page 61: ...mple Set 5 Volts 10 ppm on the expectation that the gases measured will be in the range near 2 ppm with occasional bursts up to almost 10 ppm Set 5 Volts 5 ppm to get exactly two times greater sensitivity on the analog output with the expectation that the concentration will not go above 5 ppm If the measured concentration goes above the maximum expected value for the Analog Output the on screen di...

Page 62: ... It extends the upper range up to 100x through automated dilution and maintains the target concentration at that level The EDDS can be enabled disabled using the radio buttons and the dilution factor can be set using the drop down selection box on the DCS screen Figure 43 See Appendix F External Dynamic Dilution System Optional on page 95 for detailed instructions on setting up and operating the E...

Page 63: ...ndent and are set based upon the last fixed setting Figure 44 Service Screen The Service tab contains 3 Service buttons Reset Tau Power button resets the mirror ringdown time and laser power to current settings This is typically done after mirrors have been cleaned Reset Counter button resets the of days that maintenance is required This is typically done after yearly maintenance Launch TeamViewer...

Page 64: ...ion Figure 46 Figure 45 User Interface Control Bar Exit button 3 Click the OK button to halt data acquisition close the current data file and display the shutdown screen Figure 46 Figure 46 Analyzer Shutdown Prompt 4 When the You may turn off the instrument message displays Figure 47 you can safely shut off power to the analyzer by pushing the OFF switch on the front of the analyzer Figure 2 Figur...

Page 65: ...t if necessary Figure 38 Mirror Ring Down Time and Maintenance Measurement cell mirrors are protected from contamination by an internal inlet filter With continued use the mirrors may gradually decline in reflectivity For the GLA451 OCS if a significant change occurs in the mirror ring down time for example greater than 20 reduction the precision of the measurements may be reduced For the GLA451 A...

Page 66: ... a flathead screwdriver to remove the fuse a Insert the head of the screwdriver into the slot below the fuse Figure 49 Figure 49 Remove the Fuse b Push down on the screwdriver handle to remove the fuse holder from the power inlet c Remove the fuse from the fuse holder Figure 50 Figure 50 Remove the Fuse from the Fuse Holder 4 Insert a new fuse into the fuse holder 5 Re insert the holder into the p...

Page 67: ...ere Iv is the transmitted intensity through the sample at frequency Io is the reference laser intensity prior to entering the cell S is the absorption line strength of the probed transition L is the optical path length of the laser beam through the sample 𝛘 is the mole fraction P is the gas pressure Φv is the line shape function of the transition at frequency 𝞾 In this case If the laser line width...

Page 68: ...ngth Line strength of the probed transition Enables you to determine the mole fraction directly from the relation Use this equation to determine gas concentrations even in hostile environments without using calibration gases or reference standards These values are measured Mixtures containing several species Flows at elevated temperatures and pressures ...

Page 69: ...ctive optical path length is 2500 meters Figure 52 Schematic Diagram of an Off Axis ICOS Analyzer Because the path length depends only on optical losses in the cavity and not on a unique beam trajectory like conventional multi pass cells or cavity ring down systems the optical alignment is very robust allowing for reliable operation in the field The effective optical path length is determined rout...

Page 70: ...Protocol request when the analyzer is initialized If the analyzer does not receive a reply the analyzer Disables the Ethernet port Does not attempt another DHCP request until the analyzer is restarted When both conditions are met the data directory can be accessed using a Windows computer on the same LAN To access the data directory 1 Click Start Run and enter the IP address of the analyzer Exampl...

Page 71: ...cal Area Network LAN is not available plug the analyzer into a standalone broadband router example Netgear Model RP614 to enable the analyzer to obtain a Dynamic Host Configuration Protocol DHCP address from the router when the analyzer is started Then plug any Windows computer into the same broadband router to access the data directory A crossover Ethernet cable will NOT allow an external compute...

Page 72: ...www tp link com support and enter the TP Link model number TL WR802N You must restart the analyzer whenever you change router modes for the mode change to take effect Local Connection You can also bypass the wireless router if you want to connect the analyzer to a local network Refer to the Connect Analyzer to Local Network section on page 76 for instructions on this configuration Wireless Control...

Page 73: ...ptop connect to the router using the SSID and password on the router Figure 53 Figure 53 Router SSID and Password Location 2 On the same device launch a Web browser then type http tplinkwifi net in the address bar Figure 54 Figure 54 Logging In 3 Enter admin in lowercase for both the username and password 4 Click Login ...

Page 74: ...Point button Figure 55 8 Click Next 9 In the Wireless Setting screen do one of the following Figure 56 a To keep the default Wireless Network Name and or AP Wireless Password click Next b To change the default Wireless Network Name and or AP Wireless Password change the names in the Wireless Network Name and or AP Wireless Password fields then click Next Figure 56 Wireless Setting Screen ...

Page 75: ...USER MANUAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 75 10 In the Network Setting screen click Next Figure 57 Figure 57 Network Setting Screen 11 Click Finish 12 Restart the analyzer ...

Page 76: ...ernet Union 2 Remove the Ethernet union next to the router Figure 58 3 Plug the black cable into either port of the Ethernet union Figure 59 Figure 59 Plug Cables into Ethernet Union 4 Plug the blue cable into the other port of the Ethernet union Figure 59 5 Connect a local area network LAN cable from an external computer to the analyzer Ethernet port located on the external side panel ...

Page 77: ...oftware on the device you are connecting to the analyzer Set up VNC Software on Android Devices 1 On the Android device go to Settings WiFi Connect to Wireless Network 2 Connect to the wireless SSID network listed on the router sticker Enter the TP Link wireless router example TP LINK 775C as shown in Figure 53 a For ultraportable analyzers the TP Link wireless router is installed inside the analy...

Page 78: ... compete for dynamic addresses If the 192 168 100 100 address does not connect then use 192 168 100 101 8 Record the IP address of the Android device because it will be necessary to refer to it in Step 12 9 Install the VNC software by searching and installing from the Google Play store Search for Android vnc viewer and install the application by tapping on the Install button Figure 62 An Internet ...

Page 79: ... Application Installation Setup Screen 12 In the Address field enter the address of the analyzer 192 168 100 100 or 192 168 100 101 that you recorded in Step 8 The IP address of the analyzer will be whichever address the Android device is not For example if the IP address of the Android device that was displayed in Step 8 is 192 168 100 101 then the IP address of the analyzer will be 192 168 100 1...

Page 80: ...button to connect the Android device to the analyzer The analyzer software interface screen displays on the device The screen size is adjustable to fit the screen of the device Figure 65 Figure 65 Analyzer Software Interface Display with Size Adjustment for Android Devices ...

Page 81: ...r ultraportable analyzers the TP Link wireless router is installed inside the analyzer and may be accessed by opening the case For all other analyzers the optional TP Link wireless router is attached to the outside of the case 3 Select your SSID network For example TP LINK D036 Figure 66 Figure 66 Network Connections Screen 4 The Enter Password screen appears Figure 67 In the Password field enter ...

Page 82: ... addresses If the 192 168 100 100 address does not connect then use 192 168 100 101 8 Record the IP address of the iOS device because it will be necessary to refer to it in Step 12 Figure 69 Device IP Address Confirmation Screen 9 Install the VNC software by searching and installing it from the App store a Mocha VNC Lite for iOS is the software used in this example Figure 70 b An Internet connecti...

Page 83: ...d password Figure 72 Figure 72 Mocha VNC Lite Configure Screen 12 Enter the analyzer s address in the VNC server address field 192 168 100 100 or 192 168 100 101 from Step 8 The IP address of the analyzer will be whichever address the iOS device is not For example if the IP address of the iOS device that was displayed in Step 8 is 192 168 100 101 then the IP address of the analyzer will be 192 168...

Page 84: ...ess Figure 73 Figure 73 Setup Configurations Screen 15 To connect the iOS device to the analyzer tap the IP Config you set up The analyzer software will display on the device Figure 74 The screen size is adjustable to fit the screen of the device Figure 74 Analyzer Software Interface Screen Size Adjustment for iOS Devices ...

Page 85: ...onnections icon in the bottom left of the screen Figure 75 to open the Windows Wireless Networks dialog box Figure 76 Figure 75 Wireless Connections Icon Figure 76 Windows Wireless Networks 4 Select the SSID network name listed on the router sticker Example TP LINK 775C to display the Connect to a Network dialog box Figure 77 5 In the Security key field enter the wireless password located on the r...

Page 86: ...USER MANUAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 86 6 Click OK Figure 77 Network Connections Security Screen 7 The Connection Status dialog box displays Figure 78 Figure 78 Current Connectivity Screen ...

Page 87: ...he device is connected through the wireless router by selecting the router Figure 79 Figure 79 Wireless Network Connection Screen 9 Verify the IP address of the Windows device a Right click on the TP LINK 775C network connection b Click Status Figure 80 Figure 80 Current Connectivity Screen ...

Page 88: ...10 The Wireless Network Connection Status dialog box displays Figure 81 Figure 81 Wireless Network Connection Status Window 11 Click the Details button to display the Network Connection Details window Figure 82 Figure 82 Network Connection Details Window ...

Page 89: ... www realvnc com products vnc documentation 5 0 guides user Chapter1 html 14 Open the program by clicking the Connect button Figure 83 Figure 83 Real VNC Viewer Installation Screen 15 Enter the analyzer s address in the VNC server address field 192 168 100 100 or 192 168 100 101 from Figure 82 The IP address of the analyzer will be whichever address the Windows device is not For example if the IP ...

Page 90: ... order and for how long By sampling references periodically during an ongoing data run you can post correct the data for long term drift when active calibration cannot be done ABB LGR offers two versions of the MIU 8 port 16 port Figure 84 shows the front panel of a 16 port MIU Figure 84 16 Port MIU Front Panel Control of the MIU is unidirectional The analyzer does not receive feedback on the MIU ...

Page 91: ... Components 1 Connect the provided power cable into the fused power entry module on the back panel 2 Connect the 25 pin control cable from the MIU to the TO MIU port on the back panel of the analyzer 3 Connect a 1 4 Teflon tube from your gas source into one of the numbered inlet ports Repeat for multiple gases 4 When connecting the tubing push the tube into the port until you feel a click in order...

Page 92: ...ontrol Bar Figure 88 2 Click on the MIU tab at the top of the Setup menu selection bar Figure 86 a The MIU setup menu becomes active Use the menu to specify what ports are sampled and for how long Figure 86 shows the Gas Manifold Control Screen for the MIU not yet enabled Figure 86 Gas Manifold Control Screen for the MIU not yet enabled ...

Page 93: ...Screen for the MIU Enabled If a valve is set to 0 the entry is ignored Each defined gas is sampled sequentially in its respective group unknown or reference 4 Populate the reference gas valve sequence a Valve The current valve being referenced Corresponds to the port number on the MIU b Seconds How long the analyzer should reference the gas in seconds c Description Input a short text description a...

Page 94: ...oses as specified on the MIU tab when the analyzer software has properly initialized While the MIU is operating the current valve being sampled referenced and its text description is shown in the parameter window of the User Interface Control Bar Figure 88 The description is Displayed on the parameter window of the User Interface Control Bar during analysis Figure 88 Saved to a data file Figure 88...

Page 95: ...e in concentration will cause the concentration to over range for up to 2 minutes while the DCS adjusts the concentration to target The sample and the zero air flow in through the gas inlets and are mixed in the EDDS Both the sample and the zero air must Be pressurized to between 15 and 50 PSIG Have a sample gas flow capability of 200 SCCM Have a zero air flow capability of 2 2 SLPM When transitio...

Page 96: ... a The OUTPUT TO ANALYZER INLET port on the EDDS b The SAMPLE INLET port on the analyzer 3 Zero air line Use a 9 16 wrench to connect the 6 x 1 4 Teflon tubing between a The ZERO AIR 15 50 psig port on the EDDS b Your house air supply 4 Line to sample supply Use a 9 16 wrench to connect the 6 x 1 4 Teflon tubing between a The SAMPLE 15 50 psig port on the EDDS b Your sample supply 5 Power cord Con...

Page 97: ...Figure 91 Inlet T Configuration for the EDDS If you do not use the inlet tee and connect the gases directly to the analyzer the mass flow controllers will not maintain proper dilution Depending on the sample concentration the mass flow controllers adjust the amount of dilution Sample flow can vary from 0 to 200 SCCM Zero air flow can vary from 0 to 2 2 SLPM Flow through the measurement cell should...

Page 98: ...tle valve Figure 92 lets you adjust the gas flow to the analyzer Use the throttle valve to restrict the Total flow into the analyzer to less than 200 SCCM Source gas to less than 180 SCCM for proper dynamic dilution control The flow rate can be measured at the inlet if necessary Figure 92 External Throttle Valve ...

Page 99: ...n on the User Interface Control Bar 2 Click on the DCS tab at the top of the Setup menu selection bar Figure 94 3 Use the radio buttons to Enable or Disable the EDDS 4 Use the drop down selection box to set the dilution factor 5 Click Save 6 Click Close to begin the dilution Figure 94 shows the DCS Screen for the EDDS enabled Figure 94 Enable EDDS ...

Page 100: ... analyzer Use an external pump to increase the flow rate of gas during measurement Use a throttle valve to adjust the pressure inside the analyzer Figure 95 shows a plumbing diagram of an analyzer with the Fast Flow option Figure 95 Plumbing Diagram for Fast Flow Mode The AAQC and OCS analyzers do not include a throttle valve since they are back side pressure controlled ...

Page 101: ... used in conjunction with the electronic pressure controller to adjust the flow through the analyzer The throttle valve reduces the pressure of the gas to the pressure controller while the pressure controller regulates the fine adjustments to maintain cell pressure The high flow throttle valve Provides coarse manual control of the flow to compensate for various external inlet configurations Optimi...

Page 102: ... POWER port on the back panel of the analyzer b Connect the provided 6 x 3 8 Teflon tubing with Swagelok fittings from the external pump to the TO EXT PUMP port on the back panel of the analyzer c Press the Power switch on the front of the pump 2 With the Internal pump running in standard mode make note of the Gas Pressure reading within the Parameter Window of the User Interface Control Bar Figur...

Page 103: ... a The gas flow will be routed through the electronic pressure controller b The pressure controller is fully open but not able to pass sufficient flow to the cell at its target pressure 7 Turn the throttle valve counter clockwise to open while watching the Gas Pressure reading in the Parameter Window of the User Interface Control Bar Figure 98 a Find the midpoint control range by slowly opening an...

Page 104: ...ange with the set point at 140 Torr Figure 100 Control Range Diagram 8 Verify that the cell pressure is the same in both flow modes with external pump and internal pump The maximum range and reading display of the pressure transducer is approximately 155 Torr any time the cell pressure is above 155 Torr the display will remain locked at 155 Torr To determine if your analyzer is capable of fast flo...

Page 105: ...figuration for the optional batch mode Figure 101 Batch Injection Plumbing Diagram Accessories Required for Batch Injection The necessary hardware and supplies for batch mode operation include An external pump KNF 920 o Pump slave power cord o Pump connection kit Additional ports on the front and back panels of the analyzer Figure 102 o Syringe injection port front panel o Zero air inlet 1 4 Swage...

Page 106: ...g with Swagelok fittings from the external pump to the TO EXT PUMP port on the back panel of the analyzer c Connect the provided exhaust muffler to the exhaust port of the pump to exhaust into the room air or route to your facility ventilation system 2 Connect your Zero Air source to the Swagelok Zero Air Inlet port on the back panel of the analyzer Figure 102 a Zero Air flow should be set between...

Page 107: ...r is configured with this optional accessory To disable the MIU i Click Setup on the User Interface Control Bar Figure 103 Figure 103 Setup Button on the User Interface Control Bar ii Click on the MIU tab at the top of the Setup screen Figure 104 iii Uncheck the checkbox at the bottom of the screen to disable the MIU Figure 104 iv Click Save Changes Figure 104 v Click Close to exit the Setup menu ...

Page 108: ...etup on the User Interface Control Bar Figure 105 Figure 105 Setup button on the User Interface Control Bar ii Click on the WVISS tab at the top of the Setup screen Figure 106 iii Select Single Stage WVISS Disabled in the drop down menu in the WVISS mode section Figure 106 iv Click Save Changes Figure 106 v Click Close to exit the Setup menu Figure 106 Figure 106 Control Menu for the Optional WVIS...

Page 109: ...n in the User Interface Control Bar Figure 107 Figure 107 Click the Rate Button 3 The Operating Mode pop up menu displays Figure 108 a Select either Syringe Injection Syringe Injection Dilution x10 if applicable o The sample will be diluted x10 by filling the cavity with zero air before measurement 4 Click Save Figure 108 Rate Selection Menu ...

Page 110: ...lays Figure 109 a This screen combines the three Main Panel display modes on one screen Numeric Display Spectrum Display TimeChart Display b The Batch Mode Status display box in the lower right screen shows the status of the current injection Figure 109 Figure 109 Batch Injection Measurement Screen ...

Page 111: ...sting the sample 4 Prompts you to inject sample of 60 ml gas into the syringe port a You have 120 seconds to inject the sample If you take longer than 120 seconds to complete the injection the Failed Injection message displays and instructs you to restart the injection process Figure 110 shows the Batch Injection Measurement screen displayed as a flow diagram to show the batch measurement procedur...

Page 112: ... analyzer Prompts you to inject 140mL of Sample Gas into the syringe port on the front panel of the analyzer e Fill the 140mL syringe with your sample and insert the needle into the syringe port on the front of the analyzer ii The suction from the cavity should automatically draw your sample into the cavity Light pressure on the syringe will help to introduce the sample iii You have 120 seconds to...

Page 113: ...107 2 The Operating Mode pop up menu displays Figure 111 3 Set the analyzer to Slow Continuous Flow mode by selecting one of the radio buttons under the Slow option Figure 111 Figure 111 Rate Control Screen set to Slow Flow Mode 4 Unscrew the septum nut from the injection port as shown in Figure 112 Figure 112 Septum Nut with used septum 5 Remove the red septum with white Teflon coating from the i...

Page 114: ...eptum inserted on needle with Teflon coating facing away from the septum nut 8 Slide the needle with septum assembly onto the injection port on the front panel of the analyzer Figure 114 Figure 114 Needle and Septum assembly attached to the injection port 9 Hand tighten the septum nut firmly 10 Manually actuate the needle five times to confirm that the septum is adequately pre drilled 11 Remove th...

Page 115: ...zer Type Figure for Reference GLA451 AAQC Figure 115 GLA451 N2OI2 Figure 116 GLA451 N2OI3 Figure 117 GLA451 OCS Figure 118 GLA451 AAQC Enhanced Performance QC Benchtop Trace Ammonia Analyzer Figure 115 shows the Spectrum Display for the GLA451 AAQC Figure 115 Spectrum Display GLA451 AAQC ...

Page 116: ...OS INSTRUCTIONS UM ICOS EN REV B 2 116 GLA451 N2OI2 Enhanced Performance QC Benchtop Isotopic Nitrous Oxide Analyzer Figure 116 shows the Spectrum Display for the GLA451 N2OI2 Figure 116 Spectrum Display GLA451 N2OI2 ...

Page 117: ...OS INSTRUCTIONS UM ICOS EN REV B 2 117 GLA451 N2OI3 Enhanced Performance QC Benchtop Isotopic Nitrous Oxide Analyzer Figure 117 shows the Spectrum Display for the GLA451 N2OI3 Figure 117 Spectrum Display GLA451 N2OI3 ...

Page 118: ...UAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 118 GLA451 OCS Enhanced Performance QC Benchtop Carbonyl Sulfide Analyzer Figure 118 shows the Spectrum Display for the GLA451 OCS Figure 118 Spectrum Display GLA451 OCS ...

Page 119: ... ICOS INSTRUCTIONS UM ICOS EN REV B 2 119 Appendix J Cables Table 13 describes the power cables shipped with your analyzer Table 13 Power Cables Region Cable Specifications Australia and New Zealand United Kingdom ...

Page 120: ...USER MANUAL ICOS INSTRUCTIONS UM ICOS EN REV B 2 120 Europe United States ...

Page 121: ...egard to purchase orders the agreed particulars shall prevail ABB does not accept any responsibility whatsoever for potential errors or possible lack of information in this document We reserve all rights in this document and in the subject matter and illustrations contained therein Any reproduction disclosure to third parties or utilization of its contents in whole or in parts is forbidden without...

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