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Standard

 

STD 420-0003

  

 

Volvo Group 

 

Version 

Page

 

Note: If the film of fluid contracts, this means that the tensile adhesion with the glass is less than the surface 
tension of the fluid. If it spreads, the tensile adhesion with the glass is greater than the surface tension of the fluid.

 

6.1.2.2 Manual cleaning 

6.1.2.2.1 General 

The seals, metal rings and beakers are washed after each test in accordance with the process described below 
(6.1.2.2.2, 6.1.2.2.3 and 6.1.2.2.4) and kept in a dust-free environment between the tests. 

The glass plates shall be washed before the test (6.1.2.2.5) and stored for 1 h maximum without coming into 
contact with each other, in a dust-free environment. 

Note: Avoid using compressed air to dry the material, as this may be a source of heavy pollution. 

6.1.2.2.2 Cleaning seals 

The seals are washed with the laboratory washing product, rinsed abundantly in water, then in distilled water and 
dried at ambient temperature. Before each test, the seals must be placed for 1 h minimum in an oven set to 120 °C 
to avoid the release problem.  

6.1.2.2.3 Cleaning metal ring 

Metal rings are not to be touched with bare hands. The rings are washed with the laboratory washing product, 
rinsed abundantly in water, then in distilled water and dried using paper. 

6.1.2.2.4 Cleaning of beakers 

The beakers must be touched on the outer surfaces only. 

The beakers are washed with the laboratory washing product and soft paper, rinsed abundantly in water, then in 
distilled water. Allow them to drain for a few moments, then wipe with paper.  

If the beakers have contained greasy products or if the specimens have become damaged during the test leaving a 
deposit on the bottom of the beakers, the beakers shall be washed in acetone before performing the above-
mentioned washing procedure. 

6.1.2.2.5 Cleaning of glass plates 

Wash each plate with a different cotton wad impregnated with acetone so as to remove deposits. 

Wash with the laboratory washing product, paper (4.19) and hot water rinse abundantly in water, then in distilled 
water. 

Dry using paper (4.19), and then place the plates in acetone for 30 minutes minimum. 

The acetone baths shall be changed after every 5 operations. 

When removed, allow the plates to dry in ambient air. If traces due to evaporation of the acetone appear, rinse the 
plate in acetone and dry it with paper (4.19).  

Note: The washing stage is highly important, since the appearance of a deposit is greatly dependent on the surface 
tension of the glass.

 

After the glass plates have been cleaned and dried, check their cleanliness at a point at which no condensation can 
occur during the test by applying a thin film of test fluid (3.4) to the glass surface. The edges of the film shall not 
contract within 2 s. Should the edges contract within this time, repeat the cleaning procedure. Should the edges 
even after repeated cleaning still contract within 2 s, do not use these plates again for measurements. Make a 
visual check that the plates are free of scratches and other defects; if they are not, discard tem.  

Note: If the film of fluid contracts, this means that the tensile adhesion with the glass is less than the surface 
tension of the fluid. If it spreads, the tensile adhesion with the glass is greater than the surface tension of the fluid.

 

Содержание STD 420-0003

Страница 1: ...neral 4 2 Thermostatically controlled bath 4 3 Cooling plates 4 4 Flat bottomed beakers 4 5 Metal rings 4 6 Sealing rings 4 7 Float glass plates 4 8 Filter paper 4 9 Aluminium foil 4 10 Reflector mete...

Страница 2: ...e it is the difference expressed in mg between the masses of the aluminium foil before and after testing 3 Materials 3 1 Thermal transfer fluid for the thermostatically controlled bath The fluid shal...

Страница 3: ...ooling plates designed to be placed on the glass plates to keep them cool The cooling plates shall be hollow and made of corrosion resistant metal with the side facing the glass plate made of aluminiu...

Страница 4: ...uminium foil in order to decrease the risk of their edges being uneven and damaged Great care needs to be excercised so that the aluminium foil does not get contaminated Use lint free cotton gloves or...

Страница 5: ...kaline dishwasher detergents 4 13 Balance with scale divisions of 0 01 mg 4 14 Glass plate rack 4 15 Phosphorpentoxide and silica gel 4 16 Stamping apparatus for circular test pieces 80 1 mm 4 17 Glov...

Страница 6: ...ces containing natural materials 168 h 2 h Coated fabrics 48 h 2 h Other materials 24 h 2 h 6 1 2 Cleaning 6 1 2 1 Cleaning with a dishwasher Wash the sealing rings beakers and metal rings with glass...

Страница 7: ...pe with paper If the beakers have contained greasy products or if the specimens have become damaged during the test leaving a deposit on the bottom of the beakers the beakers shall be washed in aceton...

Страница 8: ...the glass plate is placed on the sealing ring The beakers with test pieces are placed in the bath that has reached the prescribed temperature On top of the glass plate a filter paper is placed follow...

Страница 9: ...culated using the formula 1 4 4 1 2 i j i j F F s where Fi is the fogging value of each point of measuring in 4 is the number of test points on the glass plate This standard deviation indicates the ho...

Страница 10: ...DP Note It is very important not to moisten the walls of the beaker with the DIDP when handling the beaker as this will lead to a larger area with DIDP and a higher test result 6 2 4 Procedure 6 2 4 1...

Страница 11: ...is reported with an accuracy of 0 01 mg 7 Report The report shall contain Reference to this standard Reference to mehod used method F evaluation of fogging using a glossmeter or method G gravimetrica...

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