background image

 
 


 

A good indication as to whether the stray light level is within specification may be obtained as 
follows: 
 
1.

 

Set the wavelength to 340 nm. 

2.

 

Set the 

MODE

 button to 

T

3.

 

With the square cuvette adapter in the Sample Compartment without a cuvette close 
the lid and press the 

0A/100%T 

(

) button to set the display to 100.0%. 

4.

 

Remove the cuvette adapter from the Sample Compartment and close the lid.  Make a 
note of the reading that should be at or near 0.00. 

5.

 

Prepare a solution containing 50 mg/L of sodium nitrite (NaNO

2

) in distilled water and 

fill a square cuvette with this solution. 

6. 

Insert the cuvette into the cuvette adapter, place it in the Sample Compartment, and 
close the lid.  The display should read < 0.5%T.  If the reading obtained in 

step

 

4

 is 

greater than 0.00, it should be subtracted from the displayed reading to give the correct 
reading for the stray light value. 

 

Troubleshooting 
PROBLEM 

 

 

Possible Cause 

 

  

       Solution 

Instrument 
Inoperative 
(Power indicator 
has no light) 

Power cord not connected to outlet 

Plug instrument in. 

Dead Power outlet. 
Wrong voltage setting. 

Change to a different outlet. 

Internal fuse blown or defective electronic 
component. 

Call an authorized service 
engineer. 

Instrument can 
not set 100%T 
(0.000A) 

No Cuvette Adapter in the Sample 
Compartment. 
 
 

Cuvette Adapter must be in 
Sample Compartment to 
open sample holder shutter. 

Light beam blocked: 

 

Holder misaligned 

 

Shutter 

Check sample holder. 

Lamp is old or defective. 

Replace lamp/bulb.   

Lamp is off alignment. 

Refer to lamp Replacement 
instructions in this manual. 

Defective electronic component. 

Call an authorized service 
engineer. 

%T can not be set 
to 00.0%T 

Sample holder. 

Remove Cuvette Adapter or 
test tube. 

Sample holder shutter. 

May be stuck open, close 
shutter. 

Defective electronic component. 

Call an authorized service 
engineer. 

Incorrect 

Bubbles or particles in solution. 

Check sample preparation 

Содержание S-1100

Страница 1: ...SPECTROPHOTOMETER MODEL S 1100 Operation Manual United Products Instruments Inc Dayton NJ USA www unicosci com 732 274 1155...

Страница 2: ...trophotometer make sure it is set to the voltage of the local power supply see Installation section The main plug shall be inserted in a socket provided with a protective earth grounded contact The pr...

Страница 3: ...e Monochromator Sample Compartment Detector Digital Display The light from the Halogen Lamp is focused on the entrance slit of the Monochromator where the collimating mirror directs the beam onto the...

Страница 4: ...ion Place the instrument on a dry dust free lab bench top In order to have the best performance from your instrument keep it as far as possible from any strong magnetic or electrical fields or any ele...

Страница 5: ...ept round tube or square cuvets Follow the steps below to change the Cuvette Sample Holder Open the lid of the Sample Holder and locate the Sample Holder Locking Screw Use the Allen Wrench included to...

Страница 6: ...sample cuvette or test tube 4 If you are to test the same sample at other wavelengths repeat step 3 to B 1 4 for each wavelength 5 For each new sample you analyze repeat step 2 to C 4 Output and Data...

Страница 7: ...llowing methods to check wavelength calibration Please note that this test requires the use of a didymium filter or a holmium oxide filter Contact Carolina for availability and pricing of these filter...

Страница 8: ...uld be within 805 809 nm The wavelength accuracy of the unit is 2 nm 9 If a middle wavelength check is desired set the wavelength to 522 nm optional 10 Make sure the cuvette adapter is empty and place...

Страница 9: ...rect reading for the stray light value Troubleshooting PROBLEM Possible Cause Solution Instrument Inoperative Power indicator has no light Power cord not connected to outlet Plug instrument in Dead Po...

Страница 10: ...d properly Check if lamp has been properly installed or has moved during transit Refer to lamp Replacement instructions in this manual Lamp old or defective Replace with a new lamp Sample Holder Misal...

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