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TOC EVOLUTION: 

USER &  

MAINTENANCE MANUAL 

Page: 

4/74

 

Instructions No.: 10844        

 

 

This document is the property of SERES and cannot be reproduced without authorization

 

8.2.3

 

The multi-channel block (multi-channel configuration) ____________________________________________________ 24

 

8.2.4

 

The multi-function reactor (oxidation) _________________________________________________________________ 25

 

8.2.5

 

The Condenser  ____________________________________________________________________________________ 25

 

8.2.6

 

The measuring cell (NDIR)  __________________________________________________________________________ 25

 

8.2.7

 

The Liquid Seal (Sample Overflow and Pressure Drop Security) ____________________________________________ 26

 

8.2.8

 

The pumps ________________________________________________________________________________________ 26

 

8.2.9

 

Air flow rate control ________________________________________________________________________________ 26

 

8.2.10

 

Carbon treatment cartridge __________________________________________________________________________ 27

 

8.2.11

 

Chlorine treatment cartridge (depend upon application)  __________________________________________________ 27

 

8.2.12

 

The compressor ____________________________________________________________________________________ 28

 

8.2.13

 

The power supply __________________________________________________________________________________ 28

 

8.2.14

 

The touch screen (PLC board or MMI)  ________________________________________________________________ 28

 

8.2.15

 

The Measuring Board _______________________________________________________________________________ 29

 

8.2.16

 

The Input/Output Board  ____________________________________________________________________________ 30

 

8.3

 

D

ESCRIPTION OF THE SCREEN MENUS

  ____________________________________________________________ 34

 

8.3.1

 

Description of the Main screen  _______________________________________________________________________ 34

 

8.3.2

 

Measurement Menu (Measurement data, thresholds, coefficient, etc.)________________________________________ 36

 

8.3.3

 

Tools menu  _______________________________________________________________________________________ 36

 

9

 

INSTALLATION MANUAL _____________________________________________________________________ 42

 

9.1

 

L

OCATION

 _________________________________________________________________________________ 42

 

9.2

 

M

OUNTING CONDITIONS

  ______________________________________________________________________ 42

 

9.3

 

E

LECTRICAL CONNECTIONS

 ____________________________________________________________________ 42

 

9.3.1

 

Power supply ______________________________________________________________________________________ 42

 

9.3.2

 

Communication ____________________________________________________________________________________ 44

 

9.3.3

 

JBUS connection (RS485)  ___________________________________________________________________________ 46

 

9.4

 

H

YDRAULIC CONNECTIONS

  ____________________________________________________________________ 48

 

9.4.1

 

Sample to be analysed _______________________________________________________________________________ 48

 

9.4.2

 

Standard for calibrating the analyser __________________________________________________________________ 48

 

9.4.3

 

Compressed air ____________________________________________________________________________________ 48

 

10

 

USER MANUAL _______________________________________________________________________________ 50

 

10.1

 

P

RELIMINARY START

-

UP

  ______________________________________________________________________ 50

 

10.2

 

S

ETTING UP THE REAGENTS

 ____________________________________________________________________ 50

 

10.3

 

L

AUNCHING OF THE ANALYSER

 _________________________________________________________________ 50

 

10.4

 

P

UMP PRIMING

 ______________________________________________________________________________ 51

 

10.5

 

S

ETTING THE MEASUREMENT THRESHOLD PARAMETERS

 ______________________________________________ 51

 

10.6

 

S

ETTING THE PARAMETERS OF THE 

4-20 

M

A

 RANGE

 _________________________________________________ 52

 

10.7

 

T

IMING OF SAMPLE PURGING LINE 

(O

PTION ON SPECIFIC CUSTOMER REQUEST

) _____________________________ 53

 

10.8

 

L

AUNCH OF THE CONTINUOUS CYCLES

____________________________________________________________ 53

 

10.9

 

V

ISUALISATION AND RECOVERY OF THE DATA

 ______________________________________________________ 53

 

10.10

 

S

TOPPING THE ANALYSER

  ___________________________________________________________________ 54

 

11

 

MAINTENANCE MANUAL _____________________________________________________________________ 56

 

11.1

 

P

REVENTIVE MAINTENANCE

  ___________________________________________________________________ 56

 

11.2

 

R

EGULAR MAINTENANCE

 ______________________________________________________________________ 56

 

11.2.1

 

TOC calibration  ___________________________________________________________________________________ 56

 

11.2.2

 

Manual measure TOC  ______________________________________________________________________________ 58

 

11.2.3

 

Zero calibration TOC (only if activated by SERES) ______________________________________________________ 59

 

11.2.4

 

Maintenance cycle – Periodic trigger (option) ___________________________________________________________ 59

 

11.2.5

 

Reagent change ____________________________________________________________________________________ 60

 

11.2.6

 

Replacing the pump pipes  ___________________________________________________________________________ 60

 

11.2.7

 

Soda lime and activated carbon cartridges ______________________________________________________________ 63

 

11.2.8

 

Copper cartridge (depend upon application) ____________________________________________________________ 64

 

11.2.9

 

Solenoid valves (Air and Water)  ______________________________________________________________________ 65

 

11.2.10

 

Compressor and Desiccant cartridge ___________________________________________________________________ 65

 

11.2.11

 

Capillary columns __________________________________________________________________________________ 65

 

11.3

 

SPECIFIC

 

MAINTENANCE __________________________________________________________________ 65

 

11.3.1

 

Replacing the touch screen ___________________________________________________________________________ 65

 

11.3.2

 

Replacing the measuring board _______________________________________________________________________ 66

 

11.3.3

 

Replacing the input/output board _____________________________________________________________________ 66

 

11.3.4

 

Replacing a pump __________________________________________________________________________________ 66

 

11.3.5

 

The reactor  _______________________________________________________________________________________ 67

 

11.3.6

 

The NDIR  ________________________________________________________________________________________ 67

 

Содержание TOC

Страница 1: ...This document is the property of SERES and cannot be reproduced without authorization User and Maintenance Manual TOC Online analyzer for TOC monitoring in water N 10844_revS...

Страница 2: ...lime and activated carbon cartridges removal procedure part 11 2 10 BOUTRELLE Julien GOZZI Marc 08 2017 I Without Persulfate deleted DALIA Nicolas GOZZI Marc 09 2017 J UPDATE Drawing DALIA Nicolas GOZ...

Страница 3: ...13 6 4 APPLICATION _______________________________________________________________________________ 13 6 5 REAGENTS _________________________________________________________________________________ 13...

Страница 4: ...________________________________________48 10 USER MANUAL _______________________________________________________________________________ 50 10 1 PRELIMINARY START UP _________________________________...

Страница 5: ...________________________69 11 3 9 Replacing the mass controller ________________________________________________________________________70 11 3 10 Replacing the Air filter_____________________________...

Страница 6: ...ed with the equipment can be affected Any spare part has to be replaced exclusively by a qualified person using only the parts specified by the manufacturer It is always recommended that all power sup...

Страница 7: ...lectrical hazard IEC 60417 No 6040 Ultraviolet radiation instructional safeguard 3 4 After Sale Service Contact After Sale Service Lagreze Johnny Tel 04 42 97 37 91 psav seres ol com Spare parts Sauri...

Страница 8: ...ion access or User W Possible Actions Consulting the measure in process Stop of the measure in process access to the settings menu Thresholds Setting 4 20mA outputs Once the access code is entered if...

Страница 9: ...nnot be reproduced without authorization 4 Unpacking book 4 1 Precaution Position the box corectly Up Down Unpack carefully the analyser Check the analyzer for damage o If the device seems to be damag...

Страница 10: ...Page 10 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 1 EQUIPMENT FILE 5 INTRODUCTION 6 MEASURING PRINCIPLE 7 TECHNICAL SPECIFI...

Страница 11: ...nored and the TOC analysis often requires determining each of these forms TOC The TOC EVOLUTION analyser from SERES is designed for determining these different carbonated compounds Non Purgeable Organ...

Страница 12: ...essary The sample and filter line is cleaned either by using the Black Cleaning technique counter current cleaning or with compressed air on a case by case basis 6 1 2 Removal of mineral carbon The sa...

Страница 13: ...ndustrial sites 0 1 to 5 10 mg l Production of demineralised water for general and chemical uses Condensate waters from vapour production systems Medium Pressure or Very High Pressure systems in therm...

Страница 14: ...e characteristic values of the method are expressed as a percentage on Full scale Measuring system NDIR Measuring range Low range configuration 0 2 ppm Limit of Detection 0 01 ppm Repeatability 2 FS A...

Страница 15: ...ibration on TOC Phtalate Calibration on TOC End Step 2 may not be implemented in the device depending on the configuration Only for ranges 20ppm The Manual measure on TIC and Zero measure may not be p...

Страница 16: ...ing cycle The measuring cycle is included in a 5 to 10 min interval but it also depends on the type of sample used program derivative function and on the parameters being measured Name Reference Valid...

Страница 17: ...UTION USER MAINTENANCE MANUAL Page 17 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization 6 9 Hydraulic diagrams Figure 1 Hydraulic diagram 1...

Страница 18: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 18 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 2 Multi Channel Hydraulic diagram...

Страница 19: ...according to the range but it also depends on the nature of the sample and on the type of measurement The spacing between the measurements can be adjusted 7 2 3 Standard dimensions Casing l x h x d 9...

Страница 20: ...acuation The gas shall be evacuated into free outside air For Cleaning the Sample Collecting Treatment System Pressure 7 bar maximum Adjustment at 2 5 bar pressure reducer 7 2 8 Electrical connections...

Страница 21: ...the top part accommodates the electronic system external communication display and the bottom part the hydraulic system The useful information is displayed via a touch screen located at the front whos...

Страница 22: ...C EVOLUTION USER MAINTENANCE MANUAL Page 22 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 3 General dimensional drawing 1 channe...

Страница 23: ...ON USER MAINTENANCE MANUAL Page 23 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 4 General dimensional drawing Multi channel con...

Страница 24: ...is a sampling system when the sample inlet is pressurised The client connects the sample inlet this sample circulates inside the loop and flows in free air via a pan The sample is collected in the dir...

Страница 25: ...ried out on the entire system which is protected by the protective cover on which are stuck the safety labels UV and Temperature 8 2 5 The Condenser This system is used to recover the condensation dro...

Страница 26: ...pression of a pipe with a medium flowrate enabling the collection of the sample Metering peristaltic pumps SERES low flowrate for the injection of reagents They are volumetric pumps 8 2 9 Air flow rat...

Страница 27: ...parts One contains activated carbon and the other soda lime This allows the elimination of CO2 and to have a high quality air carrier A desiccant cartridge is placed upstream of this cartridge Humidi...

Страница 28: ...e power supply The entire system is supplied with a switching mode power supply with the following characteristics Input voltage range 100V 230V AC Frequency 50 60hz Output voltage 24 V 13A 300W Prote...

Страница 29: ...n This board is directly connected to the power supply observed previously It communicates with the PLC board through an Ethernet connection via an Ethernet Switch 8 2 15 2 The functionalities Figure...

Страница 30: ...d by the term 4 20mA 6 digital outputs identified by the terms RELAYS and OUTPUTS VOLTAGE and distributed as follows o 4 Output Relays 24V Dry Contacts at 1A max for information on the status of the m...

Страница 31: ...ame Function Analogue Outp ut 2 4 20mA 1 4 20mA Digital 4 20mA 1 4 20mA Digital Channel 2 Measurement 0 24V 1 RELAY 1 2 D C Reserved Threshold 1 RELAY 1 2 D C Reserved Threshold 1 Channel 2 1 RELAY 2...

Страница 32: ...exceeding the threshold Multi channel configuration The corresponding threshold 1 overrun channel 2 output is accessible on pins 1 2 3 of connector X3 of board W1128007 as a dry contact relay output...

Страница 33: ...channel 2 information is accessible on pins 10 11 12 of connector X3 of board W1128007 as a dry contact 8 2 16 3 6 Wiring of the end of cycle shutdown channel input option INPUT 2 This input is used...

Страница 34: ...nel data Calculated data and measurement parameters such as the thresholds and range 8 Measured concentrations Concentration measured per channel 9 Channel in progress Number of the channel in progres...

Страница 35: ...Log file copy To load the Log files onto a USB key in order to read the data recorded by the analyser Electrical tests Access to the pumps actuator as EV lamp heating relay 4 20 mA parameter History...

Страница 36: ...hannel x tab where we find The command activating or not the channel A light indicating whether the cycle is running A warning light relating to the water fault in channel x Two indicator lights relat...

Страница 37: ...ble it In order to enable the Sample peristaltic pump o Press ON to enable the pump or OFF to disable it Sample pump command 8 3 3 1 2 Relay tab In order to test a relay o Press the Relay tab o Press...

Страница 38: ...ab o Press ON to enable or OFF to disable 8 3 3 1 4 Actuator tab In order to control the UV lamp heating compressor o Press the Actuator tab o Press ON to enable or OFF to disable 8 3 3 1 5 4 20mA out...

Страница 39: ...his window allows you to visualise the state of the inputs This window is empty if no input has been requested by the customer 8 3 3 2 Options Setpoints date time etc It is possible to modify the setp...

Страница 40: ...ture setpoint C is the control temperature of the condenser The water default setpoint V below this voltage the water defect alarm is generated This menu can also contain according to the requested op...

Страница 41: ...NUAL Page 41 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 2 INSTALLATION MANUAL 9 1 LOCATION 9 2 FASTENING 9 3 ELECTRICAL CONN...

Страница 42: ...he device tank sewer etc on the left A power supply of 110V or 230V 50 60Hz An inlet for the sample to be analysed at a max pressure of 3 bar minimum 0 5bar 50 l h 100 to 500l h if a sampling treatmen...

Страница 43: ...e reproduced without authorization The power supply to the analyzer must be connected downstream of a secured electrical installation in accordance with local standards For a 110V supply a special set...

Страница 44: ...ructions No 10844 This document is the property of SERES and cannot be reproduced without authorization 9 3 2 Communication Figure 9 Input output board terminal drawing 1 channel For more information...

Страница 45: ...UTION USER MAINTENANCE MANUAL Page 45 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization Figure 10 Input output board terminal drawing Multi...

Страница 46: ...y the device and can be retrieved at any time this table is therefore specific to the configuration of the analyzer Go to the Tools tab Copy log files menu For the two different communication modes RS...

Страница 47: ...he device The connection is made via the Ethernet connector available on the right side of the analyzer on the outside Simply mount the Ethernet cable in the connector and plug the connector For this...

Страница 48: ...atmosphere on the left side of the analyser at 3 points 9 4 2 Standard for calibrating the analyser The standard inlet required for calibrating the device will be implemented via the other channel of...

Страница 49: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 49 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 3 USER MANUAL...

Страница 50: ...and at the height of the device at room temperature A tray can be provided optional for setting them down To implement the reagent containers wear appropriate protection gloves goggles and protective...

Страница 51: ...s the Electrical test menu Access the Solenoid Valve SV tab o Enable the draining solenoid valve Access the Pumps tab o Press ON to enable each reagent pump Check that the reagents are injected correc...

Страница 52: ...hout authorization The Measurement window appears Press on the value of the threshold to modify them 10 6 Setting the parameters of the 4 20 mA range From the main screen Press of the relevant channel...

Страница 53: ...and measuring This time is called in the Option menu Timing of sample purging line 10 8 Launch of the continuous cycles In order to start the continuous analysis press button in the main window 10 9...

Страница 54: ...o do so Launch 1 measuring cycle with demineralised water instead of the sample Press button when the reactor is filled Enable the draining solenoid valve Purge the reagent pumps with demineralised wa...

Страница 55: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 55 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization SECTION 4 MAINTENANCE MANUAL...

Страница 56: ...his occasion we will check the cleanliness of the reactor Replacing the pipes of the peristaltic pumps every 3 months Complete disassembly of all sub assemblies on a yearly basis in order to clean and...

Страница 57: ...ients The maximum deviation between the calculated coefficient and the current coefficient is of 50 of the current coefficient For example if the current coefficient is equal to 1 the calculated ratio...

Страница 58: ...re the chemical method requires some measurements before giving a significant result One or several manual steps are then carried out before a calibration to obtain a correct calibration coefficient F...

Страница 59: ...ogress from the main screen press Enter the authorised user code Access the Tools tab Push on Maintenance Start the ZERO measure by pressing At the end of the cycle a window displays the zero mass and...

Страница 60: ...ctor during the reagent priming phase Stop the cycle in progress by pressing Stop Access the Tools tab Enter the authorised user code Access the Electrical test menu Press ON to run the pumps and OFF...

Страница 61: ...SERES and cannot be reproduced without authorization o Switch off the analyser Unscrew the three screws on the front panel Remove the front panel of the pump body Remove the pipe from its compartment...

Страница 62: ...pipes Perform a new calibration Replacing a pipe of the supply pump for the sample and water The pump pipes are to be changed every three months Important before replacing the pump pipes o Before chan...

Страница 63: ...sure gauge MAN014 indicates less than 0 2 bars There is no air flow into the solenoid valve In such a case remove and clean up the device The soda lime granules have a fully violet coloring CO2 satura...

Страница 64: ...occurs a second cartridge can be installed to upsized the TOC Once the reloading is done it is mandatory to fix the air circuit pressure to 3 bars 11 2 8 Copper cartridge depend upon application Copp...

Страница 65: ...of the air and water network solenoid valves every 3 months replace the membrane if necessary 11 2 10 Compressor and Desiccant cartridge The compressor does not require any specific maintenance The re...

Страница 66: ...crew this board replace and reconnect the cables 11 3 4 Replacing a pump Tooling Open ended wrenches Flathead screwdriver Hex wrench Before changing a pump it is recommended to empty it and or rinse i...

Страница 67: ...ged systematically and provided with the new lamp WARNING Use anti UV protective glasses if an operation must be carried out on the entire system which is protected by the protective cover on which ar...

Страница 68: ...easuring cell this action is quite simple Repeat the operations of section 11 3 6 1 to remove the cover Unscrew the two screws of the black part that supports the receiver Replace with the new receive...

Страница 69: ...against the radiator and place the condenser system on top After adjusting the position screw the 4 fastening screws of the part The Peltier is maintained Insert the cables through the hole on the cas...

Страница 70: ...leeves Replace with the new heating unit Connect the 2 sleeves Reconnect the 2 electrical components 11 3 9 Replacing the mass controller Switch the analyser OFF before performing the maintenance oper...

Страница 71: ...side of the controller Unscrew the Earth braid The controller is removed To reassemble proceed by going back through the steps 11 3 10 Replacing the Air filter Switch the analyser OFF before performi...

Страница 72: ...nd pressure at the sampling point The filling solenoid valve does not operate correctly Check that the filling solenoid valve is connected properly and that the LED lights up One or more hydraulic pip...

Страница 73: ...if there is one operates correctly otherwise it may be necessary to install one The sewer system is blocked Check the condition of the pipes The zero of the device is calibrated incorrectly Check the...

Страница 74: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 74 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization 13 Annexs NF EN ISO 9001 2015...

Страница 75: ...TOC EVOLUTION USER MAINTENANCE MANUAL Page 75 74 Instructions No 10844 This document is the property of SERES and cannot be reproduced without authorization DECLARATION CE UKCA OF CONFORMITY...

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