－
5
－
ME12973A
(16)Mount the cryogenic gas suction on to the goniometer cover. Then, connect the cable to the
goniometer cover for the cryogenic gas suction. (Fig.10) Fix the cryogenic gas suction to the
goniometer cover without any screws as the stand of the suction is magnetic and securely
attaches to the metal cover.
(17)Turn on the switch of the main body of cryogenic gas suction and make sure that the fan is
running inside the main body and makes a little noise.
(18)Mount the X-ray enclosure of the
XtaLAB mini
.
(19)Mount the nozzle of Low-Temperature Gas Cooler to the
XtaLAB mini
main body.
(20)Remove the protective cover on the detector. Mount the collimator and beam stop.
2.2 Fine alignment of the cryogenic gas suction pipe
(1) Turn on the switch on the main body of cryogenic gas suction.
(2) Turn on the power of
XtaLAB mini
and the water chiller system.
(3) Launch
CrystalClea
r and log into it. After login in the system, the dialog window
Open
sample
will be displayed. Click the
Cancel
button.
(4) Click on the
Manual Instrument Control
under the menu bar item
Instrument
.
(5) Click the
Initialize
button in the
Manual Instrument Control
dialog window to get
synchronization between goniometer and software.
(6) Move the Omega axis to -70 degrees.
(7) Mount the goniometer head, which holds the sample, to the goniometer.
(8) Launch
RAXVIDEO
and center the sample.
(9) Move the Omega axis to 90 degrees.
Fig.10 Installation of the main body of cryogenic gas suction
Cable to the goniometer cover
Goniometer cover
for cryogenic gas
suction
