－
2
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ME12973A
2. Cryogenic gas suction attachment - installation and adjustment
2.1 Wiring the electric power supply cable
(1) Turn on the power of the
XtaLAB mini
and water chiller system.
(2) Launch
CrystalClear
and login. After logging in the dialog window
Open sample
will be
displayed. Click the
Cancel
button.
(3) Click the
Manual Instrument Control
under the menu bar item
Instrument
.
(4) Click the
Initialize
button in the
Manual Instrument Control
dialog window to get
synchronization between goniometer and software.
(5) Move the Omega axis to 90 degrees.
(6) Close the
CrystalClear
software and turn off power to the
XtaLAB mini
and the water chiller
systems.
(7) Remove the collimator and beam stop from the
XtaLAB mini
and mount the protective cover
on to the face of the detector (Fig.2).
(8) Remove the nozzle of Low-Temperature Gas Cooler from the
XtaLAB mini
.
(9) Remove the X-ray enclosure of the
XtaLAB mini
.
(10) Remove the three screws on the goniometer cover (Fig.3) and remove the goniometer cover.
Fig.3 Screws on goniometer cover
Fig.2 Detector face cover
Detector face cover
(
XtaLAB mini
accessory)
