14
Calculations (for the nominal volume)
Mean value
̅
∑
,
x
i
= results of weightings
n = number of weightings
Mean volume
̅ ̅
,
Z = correction factor
(e. g. 1.0029 μl/mg at 20 °C, 1013 hPa)
Accuracy
Standard deviation
̅
V
0
= nominal volume
√
∑
̅
Coefficient of variation
̅
11.
Trouble Shooting
Problem
Possible cause
Corrective action
Piston difficult to
move
-
Formation of
crystals, dirty
-
Stop dispensing immediately. Loose
piston by circular motion, but do not
disassemble. Follow all cleaning
instructions.
Filling not
possible
-
Volume adjusted to
minimum setting
-
Sticking filling valve
-
Set to required volume.
-
Clean the filling valve. If necessary
replace the valve with sealing washer.
Instrument does
not dispense
liquid
-
Discharge tube
closure cap pushed
on
-
Discharge tube not
firmly connected or
damaged
-
Remove closure cap.
-
Push on the closure cap. Hold the
piston in place, and push the original
manufacturer‘s discharge tube on
firmly. Replace a deformed or damaged
discharge tube.
Air bubbles in the
instrument
-
Reagent with high
vapor pressure has
been drawn in too
quickly
-
Slowly draw in reagent.
Содержание 550.001.305
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