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14

D-31   June 2002

 

Time-Capsule Storage

Only silver-gelatin films conforming to ANSI/PIMA 
IT9.1-1998

2

 or ISO 18901-1999 should be used 

for time capsules or sealed in cornerstones of 
buildings. Film intended for this kind of storage 
should be conditioned to a low relative humidity 
(20-30% is recommended for acetate-base films) 
in a conditioning room or chamber. During 
conditioning, air should be circulated against 
both roll surfaces. Conditioning times should be at 
least two weeks for 16 mm film and four weeks for 
35 mm film. This conforms to ANSI/PIMA IT9.11-
1998 and ISO 18911-1999.

5

During conditioning, the film should be in the form 
intended for final storage (wound on itself or a 
glass rod, not on a conventional core or reel) 
because the possibility of rapid moisture change 
makes it inadvisable to rewind the film after 
conditioning. The capsule should be loaded in the 
conditioning chamber, if possible; if not, the film 
should be transferred immediately to the capsule 
and sealed tightly.

The capsule should be a stainless steel cylinder 
gasketed cover. When there is more than one roll 
of film, it is a good idea to separate rolls with 
stainless steel disks of the same inside diameter 
as that of the capsule. Cores, reels, or wrapping of 
any kind should not be included; only the film itself 
should be put into the capsule.

Handling and Filing 
Film Records

Well-planned filing systems and proper handling 
of film records are important in the storage of 
records. The custodian should set up safeguards 
against loss or misplacement of valuable records 
and also make sure that the methods of filing and 
handling do not add unnecessary wear to the 
records. When films must be used, duplicates 
should be made and originals retained in storage.

Interfiling

Microfilm may be subject to interactions when 
stored with films of different generic types 
(e.g., diazo and silver-gelatin). Do not wind 
different generic film types on the same roll or 
store them in the same container. Diazo and 
silver-gelatin microfilms should be stored 
separately before and after processing. 
Diazonium salt gases emitted from Diazo 
microfilm (pre- and post-process) can be 
detrimental to silver-gelatin microfilm.

Continual handling of film, even under favorable 
conditions, causes some wear, but wear can be 
accelerated greatly by certain factors which can 
be controlled. Scratching occurs when film is dirty 
or equipment is poorly maintained or wrongly 
used. “Cinching” causes scratches and occurs 
when film is made to slide layer on layer 
(e.g., when the end of a loose roll of film is pulled). 
Tearing and fingerprinting occur when equipment 
and handling methods are not suitable.

Remove dirt from film by wiping with a lintless 
fabric pad moistened with film cleaner or its 
equivalent. Carry out cleaning operations in an 
atmosphere of about 50% relative humidity to 
minimize the possibility that the film will become 
electrostatically charged and attract dust particles.

Another proven method for removing foreign 
matter from film is the use of Particle Transfer 
Roller (PTR) technology. These rollers are a 
polyurethane material whose tackiness and 
cushiness pick up dust, hair, and other unwanted 
material from a continuous moving film surface. 
These rollers can be mounted in-line with most 
film operations. They can be cleaned easily with 
warm water and mild soap. For more information 
about Particle Transfer Roller technology call 
FPC, Inc., (an Eastman Kodak Company) 
at 1-323-468-5774 or contact your local 
Kodak Representative.

Cleanliness of the work space is essential to 
success in these operations. Static discharge 
devices are available for use when handling film 
which has been in dry storage. Alternatively, film 
can be conditioned to a higher relative humidity 
before cleaning and then reconditioned to the 
original low relative humidity. Other suggestions 
for improving handling operations can be found in 
Eastman Professional Motion Picture Films

20

 and 

The Book of Film Care.

22

Содержание D-31

Страница 1: ...Micrographic Quality D 31 Storage and Preservation of Microfilms ...

Страница 2: ...Low Humidity 5 Molecular Sieves 6 Humidity Control 7 Air Conditioning 7 Moisture Tight Containers 7 Humidification 8 Fungus Growth 8 Microscopic Blemishes 8 Toning 9 Chemical Contamination 9 Composition of Enclosure Materials 10 Paper 10 Plastic 10 Metal 10 Adhesive 10 Printing Inks 10 Theft Protection 10 Processing for Permanence 11 Silver Gelatin Films 11 Fixing Baths 11 Washing 11 Squeegees 12 ...

Страница 3: ...Nuclear Explosions 13 Time Capsule Storage 14 Handling and Filing Film Records 14 Interfiling 14 Inspection 15 Table 1 Applicable Standards for Microfilm 15 Table 2 Storage Life of Microfilms 16 Table 3 Storage Temperature and Relative Humidity 17 Summary of Requirements for Storage and Preservation of Records on Kodak Microfilm 17 Storage Facilities 17 References and Bibliography 18 ...

Страница 4: ...elatin thermally processed silver TPS diazo and vesicular films as they relate to film permanence It also describes the essential requirements of good processing and storage practices NOTE Refer to the latest revision of each ANSI or ISO Standard specified Definitions To help understand storage requirements the composition and structure of microfilm are described and definitions of commonly used t...

Страница 5: ...phthalic acid All safety films both acetate and polyester manufactured by Eastman Kodak Company meet these requirements This means that they are difficult to ignite and are slow burning All silver gelatin Kodak Microfilms on Estar Base when processed as recommended by Kodak meet the current specifications established by the American National Standards Institute Inc ANSI for films intended for use ...

Страница 6: ...e retrieved without significant loss when stored at 21 C and 50 RH For example LE 100 indicates that information can be retrieved for at least 100 years of storage Silver gelatin films have an LE of 500 thermally processed silver TPS have an LE of 100 years Extended term storage conditions storage conditions suitable for the preservation of recorded information on the majority of freshly processed...

Страница 7: ...h pressure to damage or explode the cabinet There is practically no danger of an explosion from the storage of either Estar Base or acetate base safety film under these conditions There are small amounts of organic materials in acetate film base as well as moisture which will expand under heat and under some conditions might generate slight pressure However such intense heat would be required on t...

Страница 8: ...ning in storage the humidity of the work area should not be markedly different from that of the storage area Very large humidity differences may lead to some physical distortion The best relative humidity for storage is the lowest that can be achieved practically and controlled reliably within the limits specified in ANSI PIMA IT9 11 1998 and ISO 189115 or their latest revisions High Humidity Stor...

Страница 9: ...otential film degradation agents such as moisture oxidants solvents and others when kept in close proximity with the films under confined storage 24 Therefore Eastman Kodak Company recommends the use of molecular sieves with triacetate and polyester based films to reduce the physical aging of films and increase the longevity of black and white images under confined storage It also prevents ferroty...

Страница 10: ...ckets is recommended as this is an efficient desiccant Chemically pure silica gel may also be used as a desiccant provided that filtration is used to remove particle layers larger than 0 3 micron See ANSI PIMA IT9 11 1998 and ISO 18911 19985 or their latest revisions Moisture Tight Containers If humidity control of the storage area is not possible the storage of film in moisture tight containers i...

Страница 11: ...ar or thermally processed silver films The Kodak Disaster Recovery Laboratory offers no charge evaluation of suspect microfilm and can be reached at 1 800 EKC TEST 1 800 352 8378 or 1 585 253 3907 Microscopic Blemishes Some processed silver gelatin microfilms in storage for two to twenty years have developed microscopically small colored spots or blemishes The fogged leader at the outside of the r...

Страница 12: ...shes mentioned above Typical contaminants are paint fumes peroxides nitrogen oxides hydrogen sulfide sulfur dioxide and similar gases If an area is to be painted any films stored there should be removed beforehand and should not be returned to the area for three months The removal of contaminating gases from the air requires special consideration 5 14 15 16 17 Contaminants can come from illuminati...

Страница 13: ...hic images can be damaged by adhesives incorporating impurities such as sulfur iron copper or other ingredients that might react with image silver or gelatin Pressure sensitive adhesives and ether linked products should be avoided Rubber based products such as rubber cement should not be used Not only might they contain harmful solvents or plasticizers but they might be compounded with photographi...

Страница 14: ...tion To make sure that there is enough time for the fixing reaction to be completed specific recommendations for each type of film should be followed Undeveloped silver halides are dissolved by the fixer as complex ions of silver and thiosulfate As the silver content of the fixer increases with processing the silver thiosulfate complex becomes increasingly difficult to wash from the film This can ...

Страница 15: ...not recommended for microfilm because some hypo eliminators contain oxidizing agents that can contribute to the formation of emulsion blisters and microscopic blemishes Residual Hypo Test The accepted criterion for adequate washing is the methylene blue method described in ANSI PIMA IT9 17 1998 19 IT9 17 1998 also describes the silver densitometric method which has been suggested by the Associatio...

Страница 16: ...ped methods for safeguarding vital records in the event of a war or a natural catastrophe Many keep their vital records in underground repositories located many miles from large metropolitan areas When microfilm is kept underground in caves mines tunnels subbasements or similar locations special care should be taken to make certain that there is adequate control of the relative humidity Film shoul...

Страница 17: ...n Do not wind different generic film types on the same roll or store them in the same container Diazo and silver gelatin microfilms should be stored separately before and after processing Diazonium salt gases emitted from Diazo microfilm pre and post process can be detrimental to silver gelatin microfilm Continual handling of film even under favorable conditions causes some wear but wear can be ac...

Страница 18: ... is any indication that film records are not keeping properly storage conditions should be improved and other protective treatments given the film Make copies of films that show signs of deterioration because deterioration once initiated is an irreversible process that may be restrained but not terminated by improving storage conditions Therefore extensive and frequent inspections should be made A...

Страница 19: ... per square meter 1 Not above 0 014 grams per square meter 1 No more than perceptible tint by spot stain test All Films Storage Conditions Temperature and Relative Humidity See Table 3 Air Conditioning Not necessary unless film records are subjected to frequent or sustained high humidity 3 Essential including slightly positive air pressure Air Purification Normal Must be free from airborne gases d...

Страница 20: ...considered suitable for black and white silver gelatin thermally processed silver diazo and vesicular Kodak Microfilms Table 3 Storage Temperature and Relative Humidity NOTE If the storage temperature is sufficiently low or if the air where the film is to be handled is quite moist leave the film in its closed container until it warms up to approximate room temperature Otherwise condensation of moi...

Страница 21: ...ment ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1992 17 HVAC Applications ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1991 18 Refrigeration ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1994 19 Recovering Silver from Photographic Materials...

Страница 22: ...ent Imaging Rochester New York 14650 www kodak com go docimaging Kodak Eastman Estar and Prostar are trademarks of Eastman Kodak Company KODAK Publication No D 31 CAT No 811 6386 6 2002 Eastman Kodak Company 2002 Printed in U S A ...

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