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D-31   June 2002

7

Humidity Control

Control of relative humidity is required for 
preservation of permanent records.

Air Conditioning

Properly controlled air conditioning of the storage 
area is definitely recommended for the optimum 
long-term preservation of permanent records. 
The air should be filtered to remove dust, 
cleansed of gaseous contaminants, if present, 
and controlled to the desired relative humidity and 
temperature. Slightly positive air pressure should 
be maintained within the storage room or vault. 
Film should be conditioned to this environment 
and then placed in containers.

Where air conditioning is not available and high 
humidities are likely to be present, the humidity 
of the storage area can be lowered by electrical 
refrigeration-type dehumidifiers. These are readily 
available and inexpensive. The storage space 
should first be vapor-sealed by covering the walls 
with asphalt or aluminum paint or, better yet, 
paper-laminated aluminum foil or other water-
vapor barriers. Painting the storage area is 
suggested, but follow the painting precautions. 
A humidistat set at the desired level of humidity 
should be used to control the dehumidifier. The 
humidity level should be checked frequently with a 
reliable hygrometer, such as a sling psychrometer. 
For added protection against short-term moisture 
effects, such as dehumidifier failure, tape the 
containers as described in the following section, 
“Moisture-Tight Containers.”

Dehumidifiers using desiccants should be used 
with caution. They may create a danger of fine 
dust particles getting on the film and causing 
abrasion when the film is used. Also, when some 
chemical-desiccant particles are trapped in rolls 
of microfilm, they may form bleached spots. 
Therefore, inert desiccates should be used, and 
it is essential that the system be designed so 
that particulate material cannot enter the storage 
area. The use of molecular sieve packets is 
recommended, as this is an efficient desiccant. 
Chemically pure silica gel may also be used as 
a desiccant, provided that filtration is used to 
remove particle layers larger than 0.3 micron. 
See ANSI/PIMA IT9.11-1998 and ISO 18911-
1998

5

 or their latest revisions.

Moisture-Tight Containers

If humidity control of the storage area is not 
possible, the storage of film in moisture-tight 
containers is required to maintain the film’s 
humidity limits. The film must be conditioned to 
the required humidity before being sealed in the 
container. This requires the temporary use of an 
air-conditioned cabinet or room, or an electrical 
dehumidifier. Smaller quantities of film can be 
conditioned for two or three weeks in a desiccator 
containing activated silica gel, and then removed 
and quickly sealed.

Only properly sealed metal or glass containers 
are considered moisture- and gas-proof. They 
are preferred when long-term air conditioning is 
not practical, when gaseous impurities may 
regularly be present, or when low-temperature 
storage is used.

Plastic boxes, such as Kodak Microfilm Plastic 
Storage Cartons (CAT No. 108-6867—16 mm; 
CAT No. 841-8741—35 mm), can be used as 
protective containers in controlled areas. They 
provide satisfactory protection against short-term 
problems of moisture or gaseous impurities, 
such as might occur with floods, dehumidifier 
failures, smoke from a fire, or moisture released 
by insulation (upon exposure to heat) in certain 
fire-resistant safes and cabinets.

With both metal and plastic containers, all 
materials (including any gaskets and protective 
paints or lacquers) must be non-corroding and 
free of peroxides, reactive fumes, and exudations 
during storage. Closed containers with friction-
type or threaded twist-on lids may require no other 
seal, but should be tested for imperviousness.

If the container is in an area having the prescribed 
humidity and known to be free of harmful gases, 
taping is not required. If these conditions are not 
met, taping will provide satisfactory protection.

Plastic boxes or cans are preferable, as they 
provide more insulation in case of fire.

Содержание D-31

Страница 1: ...Micrographic Quality D 31 Storage and Preservation of Microfilms ...

Страница 2: ...Low Humidity 5 Molecular Sieves 6 Humidity Control 7 Air Conditioning 7 Moisture Tight Containers 7 Humidification 8 Fungus Growth 8 Microscopic Blemishes 8 Toning 9 Chemical Contamination 9 Composition of Enclosure Materials 10 Paper 10 Plastic 10 Metal 10 Adhesive 10 Printing Inks 10 Theft Protection 10 Processing for Permanence 11 Silver Gelatin Films 11 Fixing Baths 11 Washing 11 Squeegees 12 ...

Страница 3: ...Nuclear Explosions 13 Time Capsule Storage 14 Handling and Filing Film Records 14 Interfiling 14 Inspection 15 Table 1 Applicable Standards for Microfilm 15 Table 2 Storage Life of Microfilms 16 Table 3 Storage Temperature and Relative Humidity 17 Summary of Requirements for Storage and Preservation of Records on Kodak Microfilm 17 Storage Facilities 17 References and Bibliography 18 ...

Страница 4: ...elatin thermally processed silver TPS diazo and vesicular films as they relate to film permanence It also describes the essential requirements of good processing and storage practices NOTE Refer to the latest revision of each ANSI or ISO Standard specified Definitions To help understand storage requirements the composition and structure of microfilm are described and definitions of commonly used t...

Страница 5: ...phthalic acid All safety films both acetate and polyester manufactured by Eastman Kodak Company meet these requirements This means that they are difficult to ignite and are slow burning All silver gelatin Kodak Microfilms on Estar Base when processed as recommended by Kodak meet the current specifications established by the American National Standards Institute Inc ANSI for films intended for use ...

Страница 6: ...e retrieved without significant loss when stored at 21 C and 50 RH For example LE 100 indicates that information can be retrieved for at least 100 years of storage Silver gelatin films have an LE of 500 thermally processed silver TPS have an LE of 100 years Extended term storage conditions storage conditions suitable for the preservation of recorded information on the majority of freshly processed...

Страница 7: ...h pressure to damage or explode the cabinet There is practically no danger of an explosion from the storage of either Estar Base or acetate base safety film under these conditions There are small amounts of organic materials in acetate film base as well as moisture which will expand under heat and under some conditions might generate slight pressure However such intense heat would be required on t...

Страница 8: ...ning in storage the humidity of the work area should not be markedly different from that of the storage area Very large humidity differences may lead to some physical distortion The best relative humidity for storage is the lowest that can be achieved practically and controlled reliably within the limits specified in ANSI PIMA IT9 11 1998 and ISO 189115 or their latest revisions High Humidity Stor...

Страница 9: ...otential film degradation agents such as moisture oxidants solvents and others when kept in close proximity with the films under confined storage 24 Therefore Eastman Kodak Company recommends the use of molecular sieves with triacetate and polyester based films to reduce the physical aging of films and increase the longevity of black and white images under confined storage It also prevents ferroty...

Страница 10: ...ckets is recommended as this is an efficient desiccant Chemically pure silica gel may also be used as a desiccant provided that filtration is used to remove particle layers larger than 0 3 micron See ANSI PIMA IT9 11 1998 and ISO 18911 19985 or their latest revisions Moisture Tight Containers If humidity control of the storage area is not possible the storage of film in moisture tight containers i...

Страница 11: ...ar or thermally processed silver films The Kodak Disaster Recovery Laboratory offers no charge evaluation of suspect microfilm and can be reached at 1 800 EKC TEST 1 800 352 8378 or 1 585 253 3907 Microscopic Blemishes Some processed silver gelatin microfilms in storage for two to twenty years have developed microscopically small colored spots or blemishes The fogged leader at the outside of the r...

Страница 12: ...shes mentioned above Typical contaminants are paint fumes peroxides nitrogen oxides hydrogen sulfide sulfur dioxide and similar gases If an area is to be painted any films stored there should be removed beforehand and should not be returned to the area for three months The removal of contaminating gases from the air requires special consideration 5 14 15 16 17 Contaminants can come from illuminati...

Страница 13: ...hic images can be damaged by adhesives incorporating impurities such as sulfur iron copper or other ingredients that might react with image silver or gelatin Pressure sensitive adhesives and ether linked products should be avoided Rubber based products such as rubber cement should not be used Not only might they contain harmful solvents or plasticizers but they might be compounded with photographi...

Страница 14: ...tion To make sure that there is enough time for the fixing reaction to be completed specific recommendations for each type of film should be followed Undeveloped silver halides are dissolved by the fixer as complex ions of silver and thiosulfate As the silver content of the fixer increases with processing the silver thiosulfate complex becomes increasingly difficult to wash from the film This can ...

Страница 15: ...not recommended for microfilm because some hypo eliminators contain oxidizing agents that can contribute to the formation of emulsion blisters and microscopic blemishes Residual Hypo Test The accepted criterion for adequate washing is the methylene blue method described in ANSI PIMA IT9 17 1998 19 IT9 17 1998 also describes the silver densitometric method which has been suggested by the Associatio...

Страница 16: ...ped methods for safeguarding vital records in the event of a war or a natural catastrophe Many keep their vital records in underground repositories located many miles from large metropolitan areas When microfilm is kept underground in caves mines tunnels subbasements or similar locations special care should be taken to make certain that there is adequate control of the relative humidity Film shoul...

Страница 17: ...n Do not wind different generic film types on the same roll or store them in the same container Diazo and silver gelatin microfilms should be stored separately before and after processing Diazonium salt gases emitted from Diazo microfilm pre and post process can be detrimental to silver gelatin microfilm Continual handling of film even under favorable conditions causes some wear but wear can be ac...

Страница 18: ... is any indication that film records are not keeping properly storage conditions should be improved and other protective treatments given the film Make copies of films that show signs of deterioration because deterioration once initiated is an irreversible process that may be restrained but not terminated by improving storage conditions Therefore extensive and frequent inspections should be made A...

Страница 19: ... per square meter 1 Not above 0 014 grams per square meter 1 No more than perceptible tint by spot stain test All Films Storage Conditions Temperature and Relative Humidity See Table 3 Air Conditioning Not necessary unless film records are subjected to frequent or sustained high humidity 3 Essential including slightly positive air pressure Air Purification Normal Must be free from airborne gases d...

Страница 20: ...considered suitable for black and white silver gelatin thermally processed silver diazo and vesicular Kodak Microfilms Table 3 Storage Temperature and Relative Humidity NOTE If the storage temperature is sufficiently low or if the air where the film is to be handled is quite moist leave the film in its closed container until it warms up to approximate room temperature Otherwise condensation of moi...

Страница 21: ...ment ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1992 17 HVAC Applications ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1991 18 Refrigeration ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1994 19 Recovering Silver from Photographic Materials...

Страница 22: ...ent Imaging Rochester New York 14650 www kodak com go docimaging Kodak Eastman Estar and Prostar are trademarks of Eastman Kodak Company KODAK Publication No D 31 CAT No 811 6386 6 2002 Eastman Kodak Company 2002 Printed in U S A ...

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