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D-31   June 2002

 

Emulsion layer(s)—image or image-forming 
layer(s) of photographic films, papers, and plates.

Film base—the plastic support for the emulsion 
and backing layers.

Halation—halo or ghost around the desired 
image on a photographic emulsion. (This is 
caused by the reflection of rays of light from the 
base to the emulsion or by internal scattering of 
light within the film.)

Nitrate film—a photographic film with a base 
consisting of cellulose nitrate. Nitrate-base films 
decompose with age and are not suitable for 
permanent records. The manufacture of nitrate 
film by Eastman Kodak Company in the United 
States of America was discontinued in 1951, but 
older nitrate motion-picture films are often found in 
storage. It is not always possible to determine by 
visual examination if a film has a nitrate base. 
However, neither KODAK nor RECORDAK 
Microfilms in any width were ever made on 
nitrate base.

Non-curl backing layer—a layer, usually made 
of gelatin, applied to the side of the film base 
opposite to that of the emulsion layer, for the 
purpose of preventing curl.

NOTE: It is comparable to the emulsion layer 

in thickness and is not removed in 
processing. (Antihalation or other 
layers removed in processing are 
excluded from this definition.)

Polyester film—a photographic film having a 
polyester base. This type of base manufactured 
by Eastman Kodak Company is called Estar Base. 
It is exceptionally tough and strong and has 
excellent dimensional stability. Microfilm 
emulsions on Estar Base are currently supplied 
for many purposes. Kodak currently manufactures 
only microfilms on Estar Base.

Safety photographic film—photographic film 
which passes the ignition time test and burning 
time test as specified in ANSI and ISO Standards.

Safety poly(ethylene terephthalate) base
a polyester film base for recording materials 
composed mainly of a polymer of ethylene 
glycol and terephthalic acid. All safety films 
(both acetate and polyester) manufactured 
by Eastman Kodak Company meet these 
requirements. This means that they are 
difficult to ignite and are slow burning.

All silver-gelatin Kodak Microfilms on Estar Base, 
when processed as recommended by Kodak, 
meet the current specifications established by the 
American National Standards Institute, Inc., 
(ANSI) for films intended for use as LE 500.

Substratum (subbing or precoat)—the layer 
that bonds the emulsion to the base.

Electronic Imaging

With the coming of electronic digital imaging 
systems, the need for continuing the quality 
concepts already established in the micrographics 
arena has evolved. Following are a few 
key concepts.

Digitization—use of a scanner to convert 
documents (on paper or microforms) to 
digitally coded electronic images suitable 
for electronic storage.

Digital—the use of binary code to record 
information. “Information” can be text in a binary 
code (e.g., ASCII), images in bitmapped form, 
or sound in a sampled digital form or video.

NOTE: Information is recorded digitally for 

accuracy in storage and transmission. 
Some types of data manipulation are 
easier in digital form.

Scanning—1.) In electronic imaging, scanning is 
the operation which precedes digitization, where 
the surface of a document is divided into pixels 
and analog values are collected representing the 
optical density (brightness and possibly color) 
of each pixel.

2.) In electronic imaging, OCR scanning is the 
conversion of marks that represent symbols into 
symbols for use in a data processing system. 
The paper or microfilm with the human-readable 
marks is first scanned as an image, then is 
analyzed to recognize the intended symbol. 
The result is the set of symbolic information, 
in a machine-readable code such as ASCII 
(also known as handprint character recognition, 
intelligent character recognition, and optical 
character recognition).

3.) In micrographics, scanning is the movement of 
an image on a reader screen in a direction 
perpendicular to the direction of roll-film transport. 

4.) Scanning is the systematic examination of 
data (ISO).

Содержание D-31

Страница 1: ...Micrographic Quality D 31 Storage and Preservation of Microfilms ...

Страница 2: ...Low Humidity 5 Molecular Sieves 6 Humidity Control 7 Air Conditioning 7 Moisture Tight Containers 7 Humidification 8 Fungus Growth 8 Microscopic Blemishes 8 Toning 9 Chemical Contamination 9 Composition of Enclosure Materials 10 Paper 10 Plastic 10 Metal 10 Adhesive 10 Printing Inks 10 Theft Protection 10 Processing for Permanence 11 Silver Gelatin Films 11 Fixing Baths 11 Washing 11 Squeegees 12 ...

Страница 3: ...Nuclear Explosions 13 Time Capsule Storage 14 Handling and Filing Film Records 14 Interfiling 14 Inspection 15 Table 1 Applicable Standards for Microfilm 15 Table 2 Storage Life of Microfilms 16 Table 3 Storage Temperature and Relative Humidity 17 Summary of Requirements for Storage and Preservation of Records on Kodak Microfilm 17 Storage Facilities 17 References and Bibliography 18 ...

Страница 4: ...elatin thermally processed silver TPS diazo and vesicular films as they relate to film permanence It also describes the essential requirements of good processing and storage practices NOTE Refer to the latest revision of each ANSI or ISO Standard specified Definitions To help understand storage requirements the composition and structure of microfilm are described and definitions of commonly used t...

Страница 5: ...phthalic acid All safety films both acetate and polyester manufactured by Eastman Kodak Company meet these requirements This means that they are difficult to ignite and are slow burning All silver gelatin Kodak Microfilms on Estar Base when processed as recommended by Kodak meet the current specifications established by the American National Standards Institute Inc ANSI for films intended for use ...

Страница 6: ...e retrieved without significant loss when stored at 21 C and 50 RH For example LE 100 indicates that information can be retrieved for at least 100 years of storage Silver gelatin films have an LE of 500 thermally processed silver TPS have an LE of 100 years Extended term storage conditions storage conditions suitable for the preservation of recorded information on the majority of freshly processed...

Страница 7: ...h pressure to damage or explode the cabinet There is practically no danger of an explosion from the storage of either Estar Base or acetate base safety film under these conditions There are small amounts of organic materials in acetate film base as well as moisture which will expand under heat and under some conditions might generate slight pressure However such intense heat would be required on t...

Страница 8: ...ning in storage the humidity of the work area should not be markedly different from that of the storage area Very large humidity differences may lead to some physical distortion The best relative humidity for storage is the lowest that can be achieved practically and controlled reliably within the limits specified in ANSI PIMA IT9 11 1998 and ISO 189115 or their latest revisions High Humidity Stor...

Страница 9: ...otential film degradation agents such as moisture oxidants solvents and others when kept in close proximity with the films under confined storage 24 Therefore Eastman Kodak Company recommends the use of molecular sieves with triacetate and polyester based films to reduce the physical aging of films and increase the longevity of black and white images under confined storage It also prevents ferroty...

Страница 10: ...ckets is recommended as this is an efficient desiccant Chemically pure silica gel may also be used as a desiccant provided that filtration is used to remove particle layers larger than 0 3 micron See ANSI PIMA IT9 11 1998 and ISO 18911 19985 or their latest revisions Moisture Tight Containers If humidity control of the storage area is not possible the storage of film in moisture tight containers i...

Страница 11: ...ar or thermally processed silver films The Kodak Disaster Recovery Laboratory offers no charge evaluation of suspect microfilm and can be reached at 1 800 EKC TEST 1 800 352 8378 or 1 585 253 3907 Microscopic Blemishes Some processed silver gelatin microfilms in storage for two to twenty years have developed microscopically small colored spots or blemishes The fogged leader at the outside of the r...

Страница 12: ...shes mentioned above Typical contaminants are paint fumes peroxides nitrogen oxides hydrogen sulfide sulfur dioxide and similar gases If an area is to be painted any films stored there should be removed beforehand and should not be returned to the area for three months The removal of contaminating gases from the air requires special consideration 5 14 15 16 17 Contaminants can come from illuminati...

Страница 13: ...hic images can be damaged by adhesives incorporating impurities such as sulfur iron copper or other ingredients that might react with image silver or gelatin Pressure sensitive adhesives and ether linked products should be avoided Rubber based products such as rubber cement should not be used Not only might they contain harmful solvents or plasticizers but they might be compounded with photographi...

Страница 14: ...tion To make sure that there is enough time for the fixing reaction to be completed specific recommendations for each type of film should be followed Undeveloped silver halides are dissolved by the fixer as complex ions of silver and thiosulfate As the silver content of the fixer increases with processing the silver thiosulfate complex becomes increasingly difficult to wash from the film This can ...

Страница 15: ...not recommended for microfilm because some hypo eliminators contain oxidizing agents that can contribute to the formation of emulsion blisters and microscopic blemishes Residual Hypo Test The accepted criterion for adequate washing is the methylene blue method described in ANSI PIMA IT9 17 1998 19 IT9 17 1998 also describes the silver densitometric method which has been suggested by the Associatio...

Страница 16: ...ped methods for safeguarding vital records in the event of a war or a natural catastrophe Many keep their vital records in underground repositories located many miles from large metropolitan areas When microfilm is kept underground in caves mines tunnels subbasements or similar locations special care should be taken to make certain that there is adequate control of the relative humidity Film shoul...

Страница 17: ...n Do not wind different generic film types on the same roll or store them in the same container Diazo and silver gelatin microfilms should be stored separately before and after processing Diazonium salt gases emitted from Diazo microfilm pre and post process can be detrimental to silver gelatin microfilm Continual handling of film even under favorable conditions causes some wear but wear can be ac...

Страница 18: ... is any indication that film records are not keeping properly storage conditions should be improved and other protective treatments given the film Make copies of films that show signs of deterioration because deterioration once initiated is an irreversible process that may be restrained but not terminated by improving storage conditions Therefore extensive and frequent inspections should be made A...

Страница 19: ... per square meter 1 Not above 0 014 grams per square meter 1 No more than perceptible tint by spot stain test All Films Storage Conditions Temperature and Relative Humidity See Table 3 Air Conditioning Not necessary unless film records are subjected to frequent or sustained high humidity 3 Essential including slightly positive air pressure Air Purification Normal Must be free from airborne gases d...

Страница 20: ...considered suitable for black and white silver gelatin thermally processed silver diazo and vesicular Kodak Microfilms Table 3 Storage Temperature and Relative Humidity NOTE If the storage temperature is sufficiently low or if the air where the film is to be handled is quite moist leave the film in its closed container until it warms up to approximate room temperature Otherwise condensation of moi...

Страница 21: ...ment ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1992 17 HVAC Applications ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1991 18 Refrigeration ASHRAE Handbook New York American Society of Heating Refrigerating and Air Conditioning Engineers 1994 19 Recovering Silver from Photographic Materials...

Страница 22: ...ent Imaging Rochester New York 14650 www kodak com go docimaging Kodak Eastman Estar and Prostar are trademarks of Eastman Kodak Company KODAK Publication No D 31 CAT No 811 6386 6 2002 Eastman Kodak Company 2002 Printed in U S A ...

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