background image

After the controller is reprogrammed, place a fine gage wire thermocouple 
(  1/3 the size of kite string; available from J-KEM) in the bottom third of

 

the heating mantle and fit the flask snugly on top so that the thermocouple 
is in intimate contact with the heating mantle.  Set the power reduction 
circuit to the power level shown in the table at the right.  Turn the 
controller on and enter the set point.

Heating

Power

Mantle Size

Level

5 & 10 ml

1-10 ml

25 ml

10-100 ml

50 ml - 22 L

50 - 500 ml

For temperatures over ≈ 120 oC, 
the next higher power level may 
be necessary

Procedure to Load Tuning Parameters for External Thermocouples.

1.

Press and hold in both the 

 and 

 keys on the front of the temperature meter until the word “

tunE

” appears in the display, then release 

both keys.

2.

Press the 

 key once and the word “

bAnd

” will appear in the display.  While holding in the ‘*’ key press the 

 or 

 key until the value

 

5

” appears in the display, then release all keys.

3.

Press the 

 key once and the word “

int.t

” will appear in the display.  While holding in the ‘*’ key press the 

 or 

 key until the value

 

2

” appears in the display, then release all keys.

4.

Press the 

 key once and the word “

dEr.t

” will appear in the display.  While holding in the ‘*’ key press the 

 or 

 key until the value

 

5

” appears in the display, then release all keys.

5.

Press the 

 key once and the word “

dAC

” will appear in the display.  While holding in the ‘*’ key press the 

 or 

 key until the value

 

5.0

” appears in the display, then release all keys.

6.

Press the 

 key once and the word “

CyC.t

” will appear in the display.  While holding in the ‘*’ key press the 

 or 

 key until the value

 

5.0

” appears in the display, then release all keys.

7.

Press and hold in both the 

 and 

 keys until the temperature appears in the display, then release both keys.

To return to using thermocouples in solution, perform Procedure 1 in Section 3.9.

4.3

Automatic Storage of Min/Max Temperatures

The controller will automatically record the 

minimum and maximum temperatures of a process by following the procedure below.  These temperatures 
are updated continuously after the routine is started and cleared by turning the controller off.  This 
procedure must be started every time you want to record temperatures.

Procedure to Start Temperature Logging

1.

Press and hold in both the 

 and 

 keys on the front of the temperature meter until the word “

tunE

” appears in the display, then release 

both keys.

2.

Press the 

 key once and the word “

LEUL

” appears in the display.  While holding in the ‘*’ key press the 

 key until the value “

3

” 

appears in the display, then release all keys.

3.

Press the 

 key until the word “

ChEy

” appears in the display.  While holding in the ‘*’ key press the 

 key until “

on

” appears in the 

display, then release all keys.

4.

Hold in both the 

 and 

 keys until the temperature appears in the display then release both keys.  Automatic temperature logging is

 

now on and will remain on until the controller is turned off or logging is turned off manually by repeating this procedure except in Step 3 
pressing the 

 key until the word “

off

” appears.

Procedure to Read Minimum and Maximum Temperatures

1.

Press and hold in both the 

 and 

 keys on the front of the temperature meter until the word “

tunE

” appears in the display, then release 

both keys.

2.

Press the 

 key once and the word “

LEUL

” appears in the display.  While holding in the ‘*’ key press the 

 key until the value “

3

” 

appears in the display, then release all keys.

3.

Press the 

 key until the word “

rEAd

” appears in the display.  The “

rEAd

” screen displays 3 parameters.

1.

Variance (the difference between the highest and lowest logged temperatures) Hold in the ‘*’ key and the display will alternate 
between “

UAr

o

” and number of degrees of variance.

2.

High Temperature (the highest temperature since the logging option was turned on).  While holding in the ‘*’ key press the 

 key

 

once and the display will alternate between “

hi o

” and the highest recorded temperature.

3.

Low Temperature.   While holding in the ‘*’ key press the 

 key once and the display will alternate between “

Lo o

” and the 

lowest recorded temperature.

The High and Lo temperatures can be examined as often as you like since updating and monitoring continues until the monitor is stopped 
by turning the controller to the off position.

4.

Press and hold in both the 

 and 

 keys until the temperature appears in the display, then release both keys.

23

Содержание 250

Страница 1: ...Temperature Control for Research and Industry Model 250 Temperature Controller User Manual...

Страница 2: ...2...

Страница 3: ...OSE IN NO EVENT SHALL J KEM SCIENTIFIC INC BE LIABLE FOR CONSEQUENTIAL INCIDENTAL OR SPECIAL DAMAGES THE BUYER S SOLE REMEDY FOR ANY BREACH OF THIS AGREEMENT BY J KEM SCIENTIFIC INC OR ANY BREACH OF A...

Страница 4: ...ts When Using Your Controller 16 3 9 Resetting the Controller for Use With Heating Mantles 17 3 10 Changing the Temperature Display Resolution 17 3 11 Changing between PID and ON OFF Operating Modes...

Страница 5: ...e volume of solution being heated not the size of the flask being used The power level switch can be thought of as a solid state variac Volume ranges are printed above this switch as a guide to select...

Страница 6: ...ntrols and data logs up to 16 controllers simultaneously Until KEM Net is available J KEM is offering KEM Log at no charge KEM Log provides remote control and data logging for one J KEM controller KEM...

Страница 7: ...of tuning parameters For the controller to heat with stability it must have programmed with the tuning parameters for the heater currently being used Prior to shipment tuning parameters were programme...

Страница 8: ...ct on the cooling outlet 1 Set the equipment up in the exact configuration it will be used For example to tune to a vacuum oven place the thermocouple in the room temperature oven and plug the oven in...

Страница 9: ...heater has its own thermostat or power controls turn both as high as they ll go With this procedure it s not necessary for the equipment to start at room temperature This procedure can be performed at...

Страница 10: ...ning parameters have been changed or the controller has been autotuned and you want to go back to using heating mantles J KEM recommends that the tuning parameters for heating mantles be loaded manual...

Страница 11: ...e same color plug as the thermocouple input 6 on the front of the controller 7 Controller On Off switch For maximum display accuracy turn on the controller 30 minutes prior to use WARNING Due to the n...

Страница 12: ...feature of J KEM s controllers called Ramp To Setpoint allows you to enter a specific heating rate e g heat to 120o C at a rate of 5o C Hour a second feature called Soak then lets you specify how long...

Страница 13: ...he temperature meter until the word tunE appears in the display then release both keys 2 Press the key 8 times until the word SPrr appears in the display This is were you set the ramp rate in units of...

Страница 14: ...or message inPt FAiL blinks in the temperature meter display and the controller stops heating 3 6 Power Reduction Circuit This circuit 8 is the interface to J KEM s patented power control computer whi...

Страница 15: ...volume isn t included in this power setting it should be used because low temperatures are better regulated with less power Avoid switching between power levels while the controller is heating Specifi...

Страница 16: ...Conditions Set point 70o C 50 ml Toluene 100 ml Round bottomed flask Graph 1 This graph shows typical heating profiles for a laboratory oven and an HPLC column In the example of the oven the heating c...

Страница 17: ...oop should not be broken at any point Don t remove either the thermocouple or heater from the solution without setting the power level to the Heat Off With the thermocouple or heater separated from th...

Страница 18: ...ey press the or key until the value 3 0 appears in the display then let go of all the keys 6 Press the key once and the word CyC t will appear in the display First hold in the key then while holding i...

Страница 19: ...hat the controller must be properly tuned to the heater being used whereas ON OFF mode requires no tuning Since both heating modes have their advantages simplicity vs accuracy instructions to change t...

Страница 20: ...n the display tunE FAiL Autotune routine failed Turn off controller for 10 seconds See Section 2 2 Displayed temperature is incorrect Note Type J The controller has not warmed up The display temperatu...

Страница 21: ...ing a large volume is being heated the controller sets internal parameters appropriate for heating large volumes If a large rise in temperature results the controller responds by loading a set of para...

Страница 22: ...operator control and has a major impact on the amount of overshoot on initial warm up 2 Again referring to the range analogy you d obtain better control when heating small volumes if the range had mor...

Страница 23: ...y after the routine is started and cleared by turning the controller off This procedure must be started every time you want to record temperatures Procedure to Start Temperature Logging 1 Press and ho...

Страница 24: ...he controller may need to be autotuned for the oil bath see User s Manual but this is discouraged unless you ll be using the oil bath frequently 2 If the reason for using an oil bath is that a small v...

Страница 25: ...ed to water since the coefficient of heat for hexane is 0 54 calories g o C and water is0 1 0 calorie gram o C That means that 1000 watt seconds of input power will raise the temperature of 10 g of he...

Страница 26: ...ay Let go of all the keys 10 Press the key once and the word int t will appear in the display Next hold in the key then while holding in the key press the key until the value 10 appears in the display...

Отзывы: