J-KEM Scientific 250 Скачать руководство пользователя страница 21

Section 4:

  

Application Notes

Supplemental application notes on the following topics are available by contacting J-KEM.

Application
Note

Subject

AN1

How to heat oil baths with your controller.  (Included in Appendix)

AN2

Changing the controller’s thermocouple type.

AN3

Changing the heating outlet into a cooling outlet.

AN4

Using the controller for unattended fractional distillations.

AN5

Using the controller with inductive (motors, valves) loads.

4.1

Theory of How the Controller Works – Simply.

For the purpose of explaining how the controller 

works, the example of a solution heated with a heating mantle is used.  The principles are the same for all 
heater types.

Power

ON

J -K EM

  Scie ntific

Instruments for Science

M od el 210

120 Vac, 840 watts

120 vac

Power  to heater

Thermocouple

Heating  mantle

Temperature of process
from the thermocouple

Output

Power  Level

1-10 ml

10-100 ml

50-500 ml

300 ml-2 L

> 2 L

Heat

Off

8 0. 0

o

C

*

Figure 2

The controller, the heating mantle and the thermocouple form a closed loop feedback system.  If 

the process temperature is below the set point, the controller turns the heating mantle on and then 
monitors the temperature rise of the solution.  If a small rise results (indicating a large volume is being 
heated) the controller sets internal parameters appropriate for heating large volumes.  If a large rise in 
temperature results, the controller responds by loading a set of parameters appropriate for heating small 
volumes.    For the controller to work ideally, information needs to travel instantaneously around the 
feedback loop.  That means that any power the controller applies to the heating mantle must reflect itself 
in an instantaneous temperature rise of the solution and the thermocouple.  Unfortunately, this type of 
instantaneous heat transfer from the heating mantle to the solution to the thermocouple just doesn't occur. 
The delay time between when power is applied to the heating mantle and when the solution rises in 
temperature; and also the converse, when power is removed from the heating mantle and the solution 
temperature stops rising is the source of most controller errors.  The reason for this can be seen in a 
simple example.  

Imagine heating a gallon of water to 80

o

 C in a 5 quart pan on an electric range.  Placing the pan 

on the range and turning the heat to ‘high’ you’d observe a delay in heating while the range coil warmed-
up.  This delay might be a little annoying, but it's really no problem.  The real problem comes as the water 
temperature approaches 80

o

 C.  If you turned the range off just as the water reached 80

o

 C the temperature 

21

Содержание 250

Страница 1: ...Temperature Control for Research and Industry Model 250 Temperature Controller User Manual...

Страница 2: ...2...

Страница 3: ...OSE IN NO EVENT SHALL J KEM SCIENTIFIC INC BE LIABLE FOR CONSEQUENTIAL INCIDENTAL OR SPECIAL DAMAGES THE BUYER S SOLE REMEDY FOR ANY BREACH OF THIS AGREEMENT BY J KEM SCIENTIFIC INC OR ANY BREACH OF A...

Страница 4: ...ts When Using Your Controller 16 3 9 Resetting the Controller for Use With Heating Mantles 17 3 10 Changing the Temperature Display Resolution 17 3 11 Changing between PID and ON OFF Operating Modes...

Страница 5: ...e volume of solution being heated not the size of the flask being used The power level switch can be thought of as a solid state variac Volume ranges are printed above this switch as a guide to select...

Страница 6: ...ntrols and data logs up to 16 controllers simultaneously Until KEM Net is available J KEM is offering KEM Log at no charge KEM Log provides remote control and data logging for one J KEM controller KEM...

Страница 7: ...of tuning parameters For the controller to heat with stability it must have programmed with the tuning parameters for the heater currently being used Prior to shipment tuning parameters were programme...

Страница 8: ...ct on the cooling outlet 1 Set the equipment up in the exact configuration it will be used For example to tune to a vacuum oven place the thermocouple in the room temperature oven and plug the oven in...

Страница 9: ...heater has its own thermostat or power controls turn both as high as they ll go With this procedure it s not necessary for the equipment to start at room temperature This procedure can be performed at...

Страница 10: ...ning parameters have been changed or the controller has been autotuned and you want to go back to using heating mantles J KEM recommends that the tuning parameters for heating mantles be loaded manual...

Страница 11: ...e same color plug as the thermocouple input 6 on the front of the controller 7 Controller On Off switch For maximum display accuracy turn on the controller 30 minutes prior to use WARNING Due to the n...

Страница 12: ...feature of J KEM s controllers called Ramp To Setpoint allows you to enter a specific heating rate e g heat to 120o C at a rate of 5o C Hour a second feature called Soak then lets you specify how long...

Страница 13: ...he temperature meter until the word tunE appears in the display then release both keys 2 Press the key 8 times until the word SPrr appears in the display This is were you set the ramp rate in units of...

Страница 14: ...or message inPt FAiL blinks in the temperature meter display and the controller stops heating 3 6 Power Reduction Circuit This circuit 8 is the interface to J KEM s patented power control computer whi...

Страница 15: ...volume isn t included in this power setting it should be used because low temperatures are better regulated with less power Avoid switching between power levels while the controller is heating Specifi...

Страница 16: ...Conditions Set point 70o C 50 ml Toluene 100 ml Round bottomed flask Graph 1 This graph shows typical heating profiles for a laboratory oven and an HPLC column In the example of the oven the heating c...

Страница 17: ...oop should not be broken at any point Don t remove either the thermocouple or heater from the solution without setting the power level to the Heat Off With the thermocouple or heater separated from th...

Страница 18: ...ey press the or key until the value 3 0 appears in the display then let go of all the keys 6 Press the key once and the word CyC t will appear in the display First hold in the key then while holding i...

Страница 19: ...hat the controller must be properly tuned to the heater being used whereas ON OFF mode requires no tuning Since both heating modes have their advantages simplicity vs accuracy instructions to change t...

Страница 20: ...n the display tunE FAiL Autotune routine failed Turn off controller for 10 seconds See Section 2 2 Displayed temperature is incorrect Note Type J The controller has not warmed up The display temperatu...

Страница 21: ...ing a large volume is being heated the controller sets internal parameters appropriate for heating large volumes If a large rise in temperature results the controller responds by loading a set of para...

Страница 22: ...operator control and has a major impact on the amount of overshoot on initial warm up 2 Again referring to the range analogy you d obtain better control when heating small volumes if the range had mor...

Страница 23: ...y after the routine is started and cleared by turning the controller off This procedure must be started every time you want to record temperatures Procedure to Start Temperature Logging 1 Press and ho...

Страница 24: ...he controller may need to be autotuned for the oil bath see User s Manual but this is discouraged unless you ll be using the oil bath frequently 2 If the reason for using an oil bath is that a small v...

Страница 25: ...ed to water since the coefficient of heat for hexane is 0 54 calories g o C and water is0 1 0 calorie gram o C That means that 1000 watt seconds of input power will raise the temperature of 10 g of he...

Страница 26: ...ay Let go of all the keys 10 Press the key once and the word int t will appear in the display Next hold in the key then while holding in the key press the key until the value 10 appears in the display...

Отзывы: