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IKA RV 10 auto, Руководство по эксплуатации

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实用信息

本仪器配置了蒸发瓶安全操作装置。若发生电源中断，玻璃组

件内部会产生真空，再次通电前请通风系统。电源中断时，内

置气弹簧将蒸发瓶自动提升至加热锅以上位置。

每次使用前必须进行日常检查升降

系统的安全性，详见章节“安全说明”

中的“升降系统”部分。

除提供手动和半自动操作模式外，该旋转蒸发仪还可以实现

全自动蒸馏和定量蒸馏过程。全自动操作的标准配置包括双

位真空控制器、冷却水的温度差测量传感器以及冷却水的流

速计。通过内置真空控制器，实现了对真空进行双位控制和速

度控制。该仪器为操作冷却水供给系统（如实验室恒温器）而

设计，但也可在连接供水管时使用。请参考

”

技术参数

“

有关冷

却水压、温度恒定性、流速和周边环境要求的信息。

连接水管操作时推荐使用

 RV 10.5001 

阻流阀。

该阀可调节水流，且在完成蒸馏过程时可自动切断冷却水供

应。

RV 10.5002 

过滤器可防止污物颗粒流过水管进入阀系统。

若需减压，我们推荐使用 

RV 10.5003 

压力调节阀调节冷却水

压。

蒸馏是利用物质的特性、气压与沸点关系进行蒸馏，然后冷凝

从而达到分离液体组分的热力学过程。

沸点温度随外部气压的降低而降低，这意味着很多工作通常

都可以在减压后进行。在此过程中，加热锅保持在一个稳定的

温度

 (

如：

60 °C)

；使用真空控制器，沸点和蒸汽温度约为

40 °C

，

冷凝器冷却水温度不高于

 20 °C (60-40-20 

原则

)

。

带真空控制器的化学隔膜泵可用于真空控制，真空缓冲回流

瓶可有效防止残留溶剂流入真空泵。使用喷射泵控制真空度

时，溶剂会对环境造成污染。

转速、温度、蒸发瓶大小以及系统压力均影响蒸发仪排气量。

冷凝管最佳蒸汽量为

 60%

，该数值相当于冷却旋管冷却量的

2/3

，更大的蒸汽量有可能导致未冷却的溶剂溢出。

为防止上述情况发生，可启用冷凝管负载安全监控系统。启用

安全监控前，需进行多次蒸馏，通过菜单

“EVAPORATOR 

 Ad-

vanced 

 Max power of cooler(

最大冷凝率

)”

，按以下公式计算

冷凝率：

冷凝率阈值

 = 

最大冷凝率

 * 1.3

将结果输入

“EVAPORATOR 

 Advanced 

 Cooler power limit(

冷凝率阈值

)”

中。若该值大于冷凝管的阈值，仪器此时会停止

测量并发出错误信号。若修改冷凝管的设置或其蒸馏过程，则

可能需要重新评估冷凝管的最大负载。

 小心

• 

开箱检查

- 

请小心拆除包装并检查仪器，

- 

如果发现任何损坏，请填写损坏报告并立即通知货运公司。

• 

交货清单

开箱

RV 10 auto 

主机

HB digital 

加热锅

竖直玻璃组件

 RV 10.1

竖直玻璃组件

 RV 10.10 

镀防爆膜

真空缓冲回流瓶

 

真空缓冲回流瓶支架

 

冷凝管锁定装置

 

真空软管

 (2 x 0.55 m) 

排水管

 (1 x 1 m) 

蒸汽管

 

梅花扳手

 

防护手柄

 

RV 10.4002 

实验室真空系统电磁阀

 

IKA

 V

acstar digital 

真空泵

 

使用说明

RV 10 control V

x x x

x x x x x x x x x

x

RV 10 control V-C

x x

x x x x x x x x x x

x

RV 10 control FLEX

x x

x x x x x x x x x

x

RV 10 auto V  

x x x

x x x x x x x x

x

RV 10 auto V-C

x x

x x x x x x x x x

x

RV 10 auto FLEX

x x

x x x x x x x x

x

RV 10 auto pro V  

x x x

x x x x x x x x

x x

RV 10 auto pro V-C

x x

x x x x x x x x x

x x

RV 10 auto pro FLEX

x x

x x x x x x x x

x x

Содержание RV 10 auto

Страница 1: ...IKA RV 10 control IKA RV 10 auto Operating instructions EN 4 ZH 29 KO 54 JA 79 TH 104 Petunjuk pengoperasian ID 129...

Страница 2: ...EN A RV 10 auto drive B Heating bath C Bracket D Woulff bottle E Glassware JA A RV 10 auto B C D E TH A RV 10 auto B C D E KO A RV 10 auto B C D E ID A Drive RV 10 auto B Bak pemanas C Bracket D Beja...

Страница 3: ...J Back key K Start Stop knob E H J F K G D C B A ZH A B C D E F G H J K KO A B C D E F G H J K JA A B C D E F G H J K TH A B C D E F G H J K ID A Sakelar Daya B Tombol Daya C Tombol posisi lift D Tom...

Страница 4: ...100 A copy of the complete EU Declaration of Conformity can be requested at sales ika com Interfaces and outputs 24 Maintenance and cleaning 25 Accessories 25 Error messages 26 Warranty 27 Technical d...

Страница 5: ...pt lift movement Safe operation is only guaranteed with the accessories described in the Accessories chapter Refer to the operating instructions for the accessories e g vacuum pump heating bath Positi...

Страница 6: ...lifted out of the heating bath When using for the first time or after a long period of inactivity proceed as follows use the motor to move the lift several times to the top and bottom positions by pre...

Страница 7: ...60 C Using the vacuum the boi ling point is set with a steam temperature of approx 40 C The cooling water for the condensation cooler should not be warmer than 20 C 60 40 20 rule A chemical resistant...

Страница 8: ...ot be adjusted Once the target value is reached the suction line is interrupted The device will fall slightly short of the target value setting due to the minimum time difference from detection of the...

Страница 9: ...d the lift with your hand on the height position and remove the thumb screw 1 by turning counterclockwise on the back of the appliance Once the transportation lock has been removed the lift moves slow...

Страница 10: ...kwise Then you can see a red mark Feed the vapour tube in until it stops Then lock the locking device by turning it clockwise by 60 Pushing the lock knob to the end position the red mark should be cov...

Страница 11: ...rectly the strong forces at the Velcro strap can cause stresses within the glass which in turn can cause damage to the glass condenser After the condenser has been fitted the stand is attached to the...

Страница 12: ...10 1 1 1 1 1 1 12 Screw joint cap 4 4 4 2 4 4 13 Hose connection 4 4 4 2 4 4 14 Manifold 1 1 1 15 Cover cap 1 16 Cartridge 1 17 Ring slotted 1 18 Washer 1 1 1 1 1 19 O ring 1 20 Plug high vacuum 1 1 N...

Страница 13: ...he vacuum hose to the valve Connect RV 10 4002 RV 10 auto operation No additional valve is required for vacuum normal operation with a speed vacuum control pump Connect the pump s vacu um inlet direct...

Страница 14: ...ted correctly Automatic distillation cannot be carried out if the water inlet and outlet hoses are not fitted according to the instructions and illus trations since this would cause the temperature re...

Страница 15: ...bol means that device is connected to a computer and that it is being controlled by the computer Program controlled This symbol means that device is being controlled by a program Rotation This symbol...

Страница 16: ...e Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point Name Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Densi...

Страница 17: ...e Delete Edit Edit Insert Insert Rotation Speed Rotation Speed Delete Delete hh mm ss hh mm ss Rotation Speed limit Interval mode Minimum 5 rpm Ccw Interval Maximum 300 rpm Cw Activate Value 00 10 Val...

Страница 18: ...te info Pump max 100 Rot speed min 5 rpm Operating hours 0 hours hPa g White Torr Logic version Display version Pressure max 1100 mbar Pressure min 1 mbar Pump min 0 Rot speed max 300 rpm Pressure Bac...

Страница 19: ...entry is a link to the Programs menu 100 Solvent The distillation process is stopped when the measured cooling water temperature difference falls below a threshold va lue i e as soon as a solvent has...

Страница 20: ...shows that the option is activated Display In the Timer menu the user can specify that the timer is dis played on the display working screen A tick shows that the opti on is activated Calculator It h...

Страница 21: ...asurement Save as Save the distillation sequence as a program Edit Edit the selected program parameters Start to edit the selected program parameters by pressing on menu option Edit with start stop kn...

Страница 22: ...mp manually without actual distilling Temperature adjustment User can set the different temperature to zero when there is no vapor liquefaction The correct temperature adjustment helps the auto distil...

Страница 23: ...ld not be filled more than half its volume Automatic filling Prior to filling the evaporation flask a vacuum controller is used to regulate the glass apparatus to the target pressure Now fill the evap...

Страница 24: ...enerally sent from the computer Master to the device Slave The lab device sends only at the computer s request Even fault indications cannot be sent spontaneously from the machine to the computer auto...

Страница 25: ...must ascertain with IKA that this method does not destroy the device Spare parts order When ordering spare parts please give device type serial number see type plate position number and description o...

Страница 26: ...tion error Vacuum calibration value is out of range Input wrong vacuum actual va lue when doing calibration Set wrong vacuum calibration value Sensor is broken Check and calibration again Check the se...

Страница 27: ...t Contact service department Internal communica tion error Internal Communication Error Internal communication error Switch device on off Contact service de partment PC communication error Error comma...

Страница 28: ...a constant temperature Adjustment accuracy vacuum mbar adjustable hysteresis Two position vacuum control mbar 1 Speed vacuum control set value 100 mbar 1 Speed vacuum control set value 100 mbar Measu...

Страница 29: ...29 ZH Device setup 2 29 30 31 32 32 33 34 40 49 50 50 51 52 53 154 156 Solvent table excerpt 159...

Страница 30: ...30 25 C EN 61010 2 010 1 mbar 3 1 kg 1 1200 gr 400 gr 280 gr 100 gr 1980 gr 3100 gr 1980 gr 1120 gr 3 1 kg IKA 3 0 kg...

Страница 31: ...31 IKA 100...

Страница 32: ...m RV 10 4002 IKA Vacstar digital RV 10 control V x x x x x x x x x x x x x RV 10 control V C x x x x x x x x x x x x x RV 10 control FLEX x x x x x x x x x x x x RV 10 auto V x x x x x x x x x x x x R...

Страница 33: ...33 RV 10 auto RV 10 control RV 10 4002 RV 10 control VC 2 4 RV 10 auto RV 10 4002 IKA Vacstar digital RV 10...

Страница 34: ...34 30 1 30 RV 10 auto 1 140 mm 2 1 2 1...

Страница 35: ...35 1 60 60 CLICK 1...

Страница 36: ...36 2 1 3 4 1 5 6 4 6 1 2 5 6 4 3 1 2 3b 3a 3c 3a 3a 2 3b 120 rpm 20 3b 1 2 3a 3b 3c...

Страница 37: ...5 RV 10 50 RV 10 6 RV 10 60 1 1 1 1 1 1 1 2 1 1 1 1 1 1 4 1 1 1 1 1 1 5 1 1 1 1 1 6 1 1 1 1 1 1 7 1 1 1 1 1 8 1 1 1 1 1 10 1000 ml 1 1 1 1 1 1 11 RV 05 10 1 1 1 1 1 1 12 4 4 4 2 4 4 13 4 4 4 2 4 4 14...

Страница 38: ...RV 10 control RV 10 4002 RV 10 4002 RV 10 auto RV 10 dT dT RV 10 3_30 RV 10 2_20 RV 10 1_10 RV 10 4_40 RV 10 5_50 RV 10 6_60 5 6 7 8 RV 10 5001 RV 10 4002 6 mm 7 mm 1 10 10 10 10 10 10 6 7 8 9 2 3 4...

Страница 39: ...39 RV 10 5001 RV 10 5001 1 2 1 2 RV 10 5001 RV 10 4002 RV 10 control...

Страница 40: ...40 IKA USB USB USB PC 100 RV 10 auto...

Страница 41: ...re Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point Name Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point...

Страница 42: ...re Delete Delete Edit Edit Insert Insert Rotation Speed Rotation Speed Delete Delete hh mm ss hh mm ss Rotation Speed limit Interval mode Minimum 5 rpm Ccw Interval Maximum 300 rpm Cw Activate Value 0...

Страница 43: ...ion mbar mL Black Value 100 Value 100 mmHg Firmware update info Pump max 100 Rot speed min 5 rpm Operating hours 0 hours hPa g White Torr Logic version Display version Pressure max 1100 mbar Pressure...

Страница 44: ...gram Programs 100 Solvent Drying Cleaning Start after Duration Pump speed Clean now Limits Manual Pump Hysteresis Automatic 10 Manual Solvent Library Name Formula Bath temperature Rotation speed Boili...

Страница 45: ...Interval Activate Speed limit Beep after timeout 00 00 00 Activate Display Timer Calculator Actions after distillation Advanced Flow control Bath medium 20 C 90 C 20 C 180 C Cooler power limit Max pow...

Страница 46: ...46 5 Program Program 1 10 1 10 10 Interval Ccw cw Interval Mode Ccw cw Rotation Select Edit Edit Delete Save as Edit Edit Delete 10 Edit Insert Delete...

Страница 47: ...ture adjustment Continue after power failure 100 Activate Time 8 Settings Languages Units Display Firmware Update Info Sound Factory Settings Communication Device name Bluetooth Labworldsoft 5 protoco...

Страница 48: ...48 2 3 1 2 1 0 6 cm 3 kg IKA HB 2 3 50 mm 2 3 IKA 50 mm 3 IKA RV 10 3000 150 mm 1 2...

Страница 49: ...AMUR NAMUR rev 1 1 NAMUR IKA IKA Windows IKA NAMUR m X 2 X 3 X 4 X 60 1 5999 1 m 5999 X 61 1 1440 1 m 1440 X 62 OUT_SP_62 1 X 63 OUT_SP_62 1 X 66 X 70 X 74 OUT_SP_74 0 OUT_SP_74 1 NAMUR IN_NAME IN_PV_...

Страница 50: ...50 IKA IKA IKA IKA www ika com IKA www ika com 4 IKA www ika com...

Страница 51: ...51 RV 10 4002 RV 10 4002 IN OUT VENT IN OUT VENT PCB PCB 40 C PCB...

Страница 52: ...52 PCB PC RS 232 USB LWS LWS PCB EEPROM EEPROM EEPROM IKA IKA IKA 2...

Страница 53: ...0 45 hh mm ss 00 00 00 99 59 59 mm ss 00 00 60 00 mbar hPa 1 1050 mbar hPa 2 1014 mbar 2 1 mbar mbar 1 100 mbar 1 100 mbar K 7 K 0 5 USB RS 232 labworldsoft RV 10 1 10 10 10 2 10 20 cm2 1500 l h 30 l...

Страница 54: ...54 KO Device setup 2 54 55 56 57 57 58 59 65 74 75 75 75 77 78 154 156 Solvent table excerpt 159...

Страница 55: ...55 25 EN 61010 2 010 1 mbar UV...

Страница 56: ...56 IKA 3 1 kg 1 1200 gr 400 gr 280 gr 100 gr 1980 gr 3100 gr 1980 gr 1120 gr Power 3 1kg IKA 3 0 kg 100...

Страница 57: ...x x x x x x x x x RV 10 control V C x x x x x x x x x x x x x RV 10 control FLEX x x x x x x x x x x x x RV 10 auto V x x x x x x x x x x x x RV 10 auto V C x x x x x x x x x x x x RV 10 auto FLEX x x...

Страница 58: ...58 RV 10 control 2 RV 10 5001 RV 10 5002 RV 10 5003 RV 10 auto RV 10 control 2 RV 10 4002 RV 10 control VC 2 4 2 2 RV 10 auto 2 RV 10 4002 IKA Vacstar digital RV 10...

Страница 59: ...59 30 1 30 RV 10 auto 1 140 mm 2 1 2 1...

Страница 60: ...60 1 60 60 CLICK 1...

Страница 61: ...61 2 1 4 1 3 5 Velcro 6 4 Velcro 6 1 2 5 6 4 3 Vapor tube 1 2 3a 3b 3c 3a 3a 2 3b 120 rpm 20 3b 1 2 3a 3b 3c...

Страница 62: ...5 RV 10 50 RV 10 6 RV 10 60 1 1 1 1 1 1 1 2 1 1 1 1 1 1 4 1 1 1 1 1 1 5 1 1 1 1 1 6 1 1 1 1 1 1 1 7 1 1 1 1 1 8 1 1 1 1 1 10 1000 ml 1 1 1 1 1 1 11 RV 05 10 1 1 1 1 1 1 12 4 4 4 2 4 4 13 4 4 4 2 4 4...

Страница 63: ...trol RV 10 4002 RV 10 4002 RV 10 auto RV 10 RV 10 control RV 10 dT dT RV 10 3_30 RV 10 2_20 RV 10 1_10 RV 10 4_40 RV 10 5_50 RV 10 6_60 5 6 7 8 RV 10 5001 RV 10 4002 6 mm 7 mm 1 10 10 10 10 10 10 6 7...

Страница 64: ...64 RV 10 5001 RV 10 5001 1 2 1 2 RV 10 5001 RV 10 4002 RV 10 control LOAD...

Страница 65: ...65 IKA Bluetooth RV 10 Bluetooth PC Blu etooth USB USB RV 10 USB PC 100 RV 10 RV 10 auto...

Страница 66: ...re Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point Name Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point...

Страница 67: ...re Delete Delete Edit Edit Insert Insert Rotation Speed Rotation Speed Delete Delete hh mm ss hh mm ss Rotation Speed limit Interval mode Minimum 5 rpm Ccw Interval Maximum 300 rpm Cw Activate Value 0...

Страница 68: ...ion mbar mL Black Value 100 Value 100 mmHg Firmware update info Pump max 100 Rot speed min 5 rpm Operating hours 0 hours hPa g White Torr Logic version Display version Pressure max 1100 mbar Pressure...

Страница 69: ...Pump 100 1 Volume Solvent Target Efficiency Adjustment Program 100 Solvent Drying Cleaning Start after Duration Pump speed Clean now Limits Manual Pump Hysteresis Automatic 10 Manual Solvent Library...

Страница 70: ...me Interval mode Interval Activate Speed limit Beep after timeout 00 00 00 Activate Display Calculator 3 2 Actions after distillation Advanced Flow control Bath medium 20 C 90 C 20 C 180 C Cooler powe...

Страница 71: ...71 5 Program Program 1 10 1 10 10 rpm Ccw cw Ccw cw Select Edit Delete Last measurement Save as Edit Delete 10 Edit Insert Delete...

Страница 72: ...Languages Units Display Sound Valves Pump Temperature adjustment Factory Settings Communication Device name Bluetooth Bluetooth Bluetooth Labworldsoft 5 protocol Labworldsoft 5 RV 10 auto Information...

Страница 73: ...73 2 3 1 2 1 0 6 cm 3 kg IKA HB 2 3 50 mm 2 3 on off IKA 50 mm 3 L IKA RV 10 3000 150 mm 1 2...

Страница 74: ...r zip USB IKA USB IKA PC COM COM RS 232 hex 0x20 CR LF hex 0x0d hex 0x0A 128 hex 0x2E NAMUR NAMUR rev 1 1 NAMUR IKA PC IKA labworldsoft MS Windows IKA NAMUR m X 2 X 3 X 4 X 60 1 5999 1 m 5999 X 61 1 1...

Страница 75: ...B 2 0 USB PC 1 2 RxD 3TxD 4 5 GND 6 7 RTS 8 CTS 9 1 RxD 2 TxD 3 4 GND 5 6 RTS 7 CTS 8 9 PC 1 2 3 4 5 6 7 8 9 9 8 7 6 5 4 3 2 1 1 2 3 4 5 USB USB 1 2 3 4 IKA IKA IKA www ika com IKA IKA www ika com 4 I...

Страница 76: ...76 RV 10 4002 RV 10 4002 PCB...

Страница 77: ...77 PCB 21 C 30 C PCB PCB PC RS 232 USB PC LWS RV 10 control RV 10 control LWS PC PCB EEPROM EEPROM EEPROM IKA 24...

Страница 78: ...0 45 hh mm ss 00 00 00 99 59 59 mm ss 00 00 60 00 mbar hPa 1 1050 mbar hPa 2 1014 mbar 2 1 mbar 2 mbar 1 100 mbar 1 100 mbar K 7 K 0 5 USB RS 232 labworldsoft RV 10 1 10 10 10 2 10 20 cm2 1500 l h 30...

Страница 79: ...79 JA Device setup 2 79 80 81 82 82 83 84 90 99 100 100 100 102 103 154 156 Solvent table excerpt 159...

Страница 80: ...80 25 EN 61010 2 010 1 3 1 1200 gr 400 gr 280 gr 100 gr 1980 gr 3100 gr 1980 gr 1120 gr...

Страница 81: ...81 IKA 3 1 kg IKA 3 0 kg 100...

Страница 82: ...x x x x x x x x RV 10 control V C x x x x x x x x x x x x x RV 10 control FLEX x x x x x x x x x x x x RV 10 auto V x x x x x x x x x x x x RV 10 auto V C x x x x x x x x x x x x RV 10 auto FLEX x x...

Страница 83: ...83 RV 10 control 2 RV 10 5001 RV 10 5002 RV 10 5003 RV 10 auto RV 10 control RV 10 control 2 RV 10 4002 RV 10 control VC 2 4 2 2 RV 10 auto 2 RV 10 4002 IKA Vacstar digital RV 10 2...

Страница 84: ...84 30 1 30 RV 10 auto 1 140 mm 2 1 1 2 1...

Страница 85: ...85 1 60 60 CLICK 1...

Страница 86: ...86 1 2 4 1 3 5 Velcro 6 4 Velcro 6 1 2 5 6 4 3 I 1 2 3b 3a 3c 3a 3a 2 3b 120 rpm 20 3b 1 2 3a 3b 3c...

Страница 87: ...5 RV 10 50 RV 10 6 RV 10 60 1 1 1 1 1 1 1 2 1 1 1 1 1 1 4 1 1 1 1 1 1 5 1 1 1 1 1 6 1 1 1 1 1 1 7 1 1 1 1 1 8 1 1 1 1 1 10 1000 ml 1 1 1 1 1 1 11 RV 05 10 1 1 1 1 1 1 12 4 4 4 2 4 4 13 4 4 4 2 4 4 14...

Страница 88: ...V 10 control RV 10 4002 RV 10 4002 RV 10 auto RV 10 RV 10 RV 10 dT dT RV 10 3_30 RV 10 2_20 RV 10 1_10 RV 10 4_40 RV 10 5_50 RV 10 6_60 5 6 7 8 RV 10 5001 RV 10 4002 6 7 1 10 10 10 10 10 10 6 7 8 9 2...

Страница 89: ...89 RV 10 5001 RV 10 5001 1 2 1 2 RV 10 5001 RV 10 4002 RV 10 control LOAD...

Страница 90: ...90 IKA Bluetooth RV 10 Bluetooth PC Bluetooth USB RV 10 USB USB PC 100 RV 10 RV 10 auto...

Страница 91: ...re Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point Name Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point...

Страница 92: ...re Delete Delete Edit Edit Insert Insert Rotation Speed Rotation Speed Delete Delete hh mm ss hh mm ss Rotation Speed limit Interval mode Minimum 5 rpm Ccw Interval Maximum 300 rpm Cw Activate Value 0...

Страница 93: ...ion mbar mL Black Value 100 Value 100 mmHg Firmware update info Pump max 100 Rot speed min 5 rpm Operating hours 0 hours hPa g White Torr Logic version Display version Pressure max 1100 mbar Pressure...

Страница 94: ...100 1 Volume Solvent Efficiency Adjustment Program 100 Solvent Drying Cleaning Start after Duration Pump speed Clean now Limits Manual Pump Hysteresis Automatic 10 Manual Solvent Library i 5 Name and...

Страница 95: ...tion Time Interval mode Interval Activate Speed limit Beep after timeout 00 00 00 Activated Display Actions after distillation Advanced Flow control Bath medium 20 C 90 C 20 C 180 C Cooler power limit...

Страница 96: ...96 5 Program 1 10 10 rpm Note Ccw cw Ccw cw Select Edit Delete Save as Edit Delete 5 Edit Insert Delete...

Страница 97: ...alves 8 Settings Languages Units Display Pump Temperature adjustment Sounds Factory Settings Communication Device name Bluetooth Bluetooth Blue tooth Labworldsoft 5 Protocol Labworldsoft 5 RV 10 contr...

Страница 98: ...98 2 3 1 2 1 0 6 cm 3 kg IKA HB 50 mm 2 3 IKA 50 3 IKA RV 10 3000 150 mm 1 2...

Страница 99: ...x 0x0A 128 Code hex 0x2E NAMUR NAMUR recommendations for the design of electrical plug connections for analogue and digital sig nal transmission on individual items of laboratory control equipment rev...

Страница 100: ...B 2 0 USB 1 2 RxD 3TxD 4 5 GND 6 7 RTS 8 CTS 9 1 RxD 2 TxD 3 4 GND 5 6 RTS 7 CTS 8 9 PC 1 2 3 4 5 6 7 8 9 9 8 7 6 5 4 3 2 1 1 2 3 4 5 USB USB 1 2 3 4 IKA IKA IKA www ika com IKA IKA www ika com IKA 4...

Страница 101: ...101 RV 10 4002 RV 10 4002 IN OUT VENT I IN OUT VENT PCB...

Страница 102: ...102 PCB 40 C PCB PCB PC RS 232 USB PC LWS RV 10 RV 10 LWS PC PCB EEPROM EEPROM EEPROM IKA 24 IKA...

Страница 103: ...0 0 45 hh mm ss 00 00 00 99 59 59 mm ss 00 00 60 00 mbar hPa 1 1050 mbar hPa 2 1014 mbar 2 1 mbar 2 mbar 1 100 mbar 1 100 mbar K 7 K 0 5 USB RS 232 labworldsoft RV 10 1 10 10 10 2 10 20 cm2 1500 l h 3...

Страница 104: ...104 TH Device setup 2 104 105 106 107 107 108 109 115 124 125 125 126 127 128 154 156 Solvent table excerpt 159...

Страница 105: ...105 flash point 25 fire point EN 61010 2 010 fume hood gas wash bottle 1 stress tempering medium...

Страница 106: ...106 IKA fine chemicals 3 1 1 1200 400 280 100 1980 3100 1980 1120 return distillation distributor slip on condenser 3 1 T IKA 3 0 resonance behavior 100...

Страница 107: ...ol V x x x x x x x x x x x x x RV 10 control V C x x x x x x x x x x x x x RV 10 control FLEX x x x x x x x x x x x x RV 10 auto V x x x x x x x x x x x x RV 10 auto V C x x x x x x x x x x x x RV 10...

Страница 108: ...108 RV 10 control RV 10 5001 RV 10 5002 RV 10 5003 RV 10 auto RV 10 control RV 10 4002 RV 10 control Hysteresis VC 2 4 Hysteresis RV 10 auto RV 10 4002 Vacstar IKA RV 10...

Страница 109: ...109 30 1 30 Drive RV 10 auto thumb screw 1 140 2 1 2 1...

Страница 110: ...110 1 60 60 CLICK 1...

Страница 111: ...111 1 thumb screw 2 4 1 3 5 Velcro 6 4 Velcro 6 Velcro 1 2 5 6 4 3 1 2 union nut 3b 3a 3c 3a 3a 2 3b 20 120 3b 1 2 3a 3b 3c...

Страница 112: ...2 1 1 1 1 1 1 4 1 1 1 1 1 1 5 1 1 1 1 1 6 1 1 1 1 1 1 7 1 1 Introduction sleeve 1 1 1 8 1 1 1 1 1 10 1 000 1 1 1 1 1 1 11 Ball joint clamp RV 05 10 1 1 1 1 1 1 12 Screw joint cap 4 4 4 2 4 4 13 4 4 4...

Страница 113: ...0 control RV 10 4002 RV 10 4002 RV 10 auto RV 10 RV 10 control RV 10 dT dT RV 10 3_30 RV 10 2_20 RV 10 1_10 RV 10 4_40 RV 10 5_50 RV 10 6_60 5 6 7 8 RV 10 5001 RV 10 4002 6 7 1 10 10 10 10 10 10 6 7 8...

Страница 114: ...114 RV 10 5001 RV 10 5001 1 2 1 2 RV 10 5001 RV 10 4002 RV 10 con trol...

Страница 115: ...115 IKA Bluetooth RV 10 Blue tooth Bluetooth USB RV 10 USB USB 100 RV 10 RV10 auto...

Страница 116: ...ure Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point Name Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling poin...

Страница 117: ...ure Delete Delete Edit Edit Insert Insert Rotation Speed Rotation Speed Delete Delete hh mm ss hh mm ss Rotation Speed limit Interval mode Minimum 5 rpm Ccw Interval Maximum 300 rpm Cw Activate Value...

Страница 118: ...ion mbar mL Black Value 100 Value 100 mmHg Firmware update info Pump max 100 Rot speed min 5 rpm Operating hours 0 hours hPa g White Torr Logic version Display version Pressure max 1100 mbar Pressure...

Страница 119: ...Pump 100 1 Volume Solvent Target Efficiency Adjustment Program 100 Solvent Drying Cleaning Start after Duration Pump speed Clean now Limits Manual Pump Hysteresis Automatic 10 Manual Solvent Library N...

Страница 120: ...n Time Interval mode Interval Activate Speed limit Beep after timeout 00 00 00 Activate Display Calculator 3 2 Actions after distillation Advanced Flow control Bath medium 20 90 20 180 Cooler power li...

Страница 121: ...121 5 Program Program 1 10 1 10 10 Ccw cw Ccw cw I Select Edit Delete Save as Edit Delete 10 Back Edit Insert Delete...

Страница 122: ...Display Firmware Update Info Sound Sound Valves Pump Temperature adjustment Factory Settings Communication Device name Bluetooth Bluetooth Bluetooth Labworldsoft 5 protocol Labworldsoft 5 RV 10 auto L...

Страница 123: ...123 2 3 1 2 1 0 6 1 2 3 IKA HB 2 3 50 2 3 IKA 50 3 extension plate RV 10 3000 IKA 150...

Страница 124: ...a lws download usb driver zip IKA USB COM COM RS 232 hex 0x20 CR LF hex 0x0d hex 0x0A 128 hex 0x2E NAMUR NAMUR 1 1 NAMUR IKA s for communication between the IKA labworld soft MS Windows NAMUR IKA m X...

Страница 125: ...USB 2 0 USB 1 2 RxD 3TxD 4 5 GND 6 7 RTS 8 CTS 9 1 RxD 2 TxD 3 4 GND 5 6 RTS 7 CTS 8 9 PC 1 2 3 4 5 6 7 8 9 9 8 7 6 5 4 3 2 1 1 2 3 4 5 USB USB 1 2 3 4 IKA IKA IKA www ika com IKA IKA www ika com IKA...

Страница 126: ...126 RV 10 4002 RV 10 4002 IN OUT VENT Venting IN OUT VENT Analog pump PCB...

Страница 127: ...127 PCB 40 PCB i PCB i RS 232 USB LWS RV 10 control RV 10 control LWS PCB EEPROM EEPROM EEPROM IKA IKA 24...

Страница 128: ...m 60 0 45 hh mm ss 00 00 00 99 59 59 mm ss 00 00 60 00 mbar hPa 1 1050 mbar hPa 2 1014 mbar 2 1 mbar Hysteresis l mbar 1 100 1 100 K 7 K 0 5 USB RS 232 Ramp programming labworldsoft RV 10 1 10 10 10 2...

Страница 129: ...gan perkakas dari kaca 154 Gambar penyambungan sistem selang 156 Solvent table excerpt 159 BAHAYA BAHAYA KEHATI HATIAN PERINGATAN PEMBERITAHUAN Menunjukkan adanya situasi berbahaya yang sebentar seben...

Страница 130: ...cocok untuk operasi manual kecuali gerakan angkat Operasi aman hanya dijamin dengan aksesori yang diuraikan dalam bab Aksesori Rujuklah petunjuk pengoperasian untuk akseseori mis pompa vacuum bak pema...

Страница 131: ...rtama kali atau setelah tidak aktif dalam jangka waktu yang lama lanjutkan sebagai berikut gunakan motor untuk menggerakkan lift beberapa kali ke posisi atas dan bawah dengan menekan tombol fungsi lif...

Страница 132: ...s 60 C Dengan menggunakan vacuum titik didih diatur dengan suhu uap kurang lebih 40 C Air pendinginan untuk pendingin kondensasi tidak boleh lebih hangat dari 20 C kaidah 60 40 20 Pompa selaput tahan...

Страница 133: ...ah nilai sasaran tercapai saluran penyedot dihentikan Per angkat akan sedikit di bawah pengaturan nilai sasaran dikarena kan selisih waktu minimal dari deteksi nilai tekanan perbandin gan nilai sasara...

Страница 134: ...g lift dengan tangan Anda pada posisi tinggi dan melepas sekrup 1 dengan memutar berlawanan dengan arah jarum jam pada bagian belakang peralatan Setelah kunci pengangkutan dilepas lift bergerak perlah...

Страница 135: ...kas dari kaca untuk penanganan secara aman perkakas dari kaca untuk laboratorium Ada sebuah kenop penguncian untuk mengunci atau membuka kunci perangkat penguncian Jika muncul tanda merah maka perangk...

Страница 136: ...ipasang tidak dengan benar daya tali Velcro yang kuat bisa menyebabkan tekanan di dalam kaca yang pada gilirannya bisa menyebabkan kerusakan pada kondensor kaca Setelah kondensor dipasang dudukan dipa...

Страница 137: ...ngan sekrup 4 4 4 2 4 4 13 Sambungan selang 4 4 4 2 4 4 14 Manipol 1 1 1 15 Penutup 1 16 Kartrid 1 17 Ring dislotkan 1 18 Washer 1 1 1 1 1 19 O ring 1 20 Steker vacuum tinggi 1 1 Catatan Tabung PTFE 5...

Страница 138: ...dalam bracket yang disediakan untuk tujuan ini dan sambungkan selang vacuum ke katup Sambungkan RV 10 4002 Operasi RV 10 auto Tidak diperlukan katup tambahan untuk operasi normal vacuum dengan pompa...

Страница 139: ...en sor tersambung dengan benar Penyulingan otomatis tidak dapat dilakukan jika selang inlet dan outlet air tidak dipasang sesuai dengan instruksi dan ilustrasi karena ini akan menyebabkan pembacaan su...

Страница 140: ...kat tersambung ke sebuah komputer dan bahwa perangkat se dang dikendalikan oleh komputer Program dikendali kan Simbol ini berarti bahwa perangkat sedang dikendalikan oleh sebuah program Rotasi Simbol...

Страница 141: ...me Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Density Boiling point Name Bath temperature Efficiency Enthalpy i factor Formula Rotation speed Heat capacity Dens...

Страница 142: ...e Delete Edit Edit Insert Insert Rotation Speed Rotation Speed Delete Delete hh mm ss hh mm ss Rotation Speed limit Interval mode Minimum 5 rpm Ccw Interval Maximum 300 rpm Cw Activate Value 00 10 Val...

Страница 143: ...e update info Pump max 100 Rot speed min 5 rpm Operating hours 0 hours hPa g White Torr Logic version Display version Pressure max 1100 mbar Pressure min 1 mbar Pump min 0 Rot speed max 300 rpm Pressu...

Страница 144: ...yang diukur berada di bawah nilai ambang yaitu segera sesudah larutan disuling seluruhnya Drying Pengeringan Selisih suhu air pendingin tidak dipantau jika opsi ini diaktifkan mis penggunaan dalam pro...

Страница 145: ...nam pilkan opsi diaktifkan Display Tampilan Pada menu Timer pengguna dapat menetapkan bahwa timer ditampilkan pada tampilan layar aktif Sebuah centang yang men ampilkan opsi diaktifkan Calculator Kalk...

Страница 146: ...gai Simpan rangkaian penyulingan sebagi sebuah program Edit Mengedit parameter program yang dipilih Mulai mengedit parameter program yang dipilih dengan menekan opsi menu Edit dengan kenop mulai berhe...

Страница 147: ...Pengguna bisa mengatur suhu yang berbeda ke nol ketika tidak ada likuifaksi uap air Penyesuaian suhu yang benar akan mem bantu mode penyulingan otomatis untuk menghidupkan dan menghentikan penyulingan...

Страница 148: ...n tidak boleh diisi lebih dari setengah volumenya Pengisian otomatis Sebelum mengisi bejana penguapan kon troler vacuum digunakan untuk mengatur alat dari kaca ke te kanan sasaran Sekarang isi bejana...

Страница 149: ...perintah Pada umumnya perintah dikirim dari komputer Master ke per angkat lab Slave Perangkat lab hanya mengirim sesuai permintaan komputer Bah kan indikasi yang salah tidak dapat dikirim secara spont...

Страница 150: ...terangan suku cadang lihat www ika com Versi software Perbaikan Mohon hanya kirimkan perangkat yang sudah dibersih kan untuk perbaikan dan juga yang bebas dari bahan ba han yang mungkin menimbulkan ba...

Страница 151: ...k pemanas tidak memanas Digunakan larutan dengan titik didih ekstrem Periksa bak pemanas Penyulingan larutan hanya secara manu al Kesalahan pembuan gam Analisis gradasi tekanan tidak menunjukkan adany...

Страница 152: ...Peralatan yang salah digunakan untuk berkomunikasi dengan kontrol RV 10 Koneksi tidak stabil Periksa pengaturan LWS Periksa alat alat PC Periksa Koneksi Kesalahan komunikasi bak pemanas Komunikasi de...

Страница 153: ...n pada suhu konstan Vacuum akurasi penyesuaian mbar histeresis Kontrol vacuum dua posisi mbar 1 Kontrol kecepatan vacuum atur nilai 100 mbar 1 Kontrol kecepatan vacuum atur nilai 100 mbar Kisaran peng...

Страница 154: ...0 coated RV 10 3 non coated RV 10 30 coated RV 10 2 non coated RV 10 20 coated RV 10 4 non coated RV 10 40 coated 7 8 6 4 5 18 14 12 4x 13 4x 11 1 2 10 15 16 17 19 6 5 18 4 13 2x 12 2x 2 10 11 1 Drawi...

Страница 155: ...155 18 4 5 14 20 6 13 4x 12 4x 8 7 11 1 2 10 7 8 6 13 4x 12 4x 20 14 18 4 5 11 1 2 10 RV 10 5 non coated RV 10 50 coated RV 10 6 non coated RV 10 60 coated...

Страница 156: ...er out Vacuum pump Water in 1 9 3 9 3 4 3 6 4 10 3 9 3 4 8 6 6 Water Vacuum Water RV 10 2 non coated RV 10 20 coated 1 9 3 6 9 3 6 4 8 3 6 4 10 3 6 9 3 8 4 1 9 3 6 9 3 6 8 4 3 9 3 6 3 6 4 8 10 4 RV 10...

Страница 157: ...ntrol RV 10 auto Water out Vacuum pump Water in 1 9 3 9 3 4 3 6 4 10 3 9 3 4 8 6 6 1 9 3 6 9 3 6 4 8 3 6 4 10 3 6 9 3 8 4 Vacuum Water Water RV 10 4 non coated RV 10 40 coated 8 4 9 3 6 4 10 8 4 3 9 8...

Страница 158: ...p Water in 1 9 3 9 3 4 3 6 4 10 3 9 3 4 8 6 6 1 9 3 6 9 3 6 8 3 6 4 10 3 6 9 3 8 4 Vacuum Water Water RV 10 6 non coated RV 10 60 coated 1 9 3 6 9 3 8 4 3 6 6 4 4 3 8 6 10 3 9 RV 10 control RV 10 auto...

Страница 159: ...O atm press 1 2 Dichloroethylene trans C2 H2 CI2 751 Diisopropylether C6 H14 O 375 Dioxane C4 H8 O2 107 Dimethylformamide DMF C3 H7 NO 11 Ethanol C2 H6 O 175 Ethylacetate C4 H8 O2 240 Ethylmethylketo...

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