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Hanna Instruments HI 83200, Инструкция по эксплуатации

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30

31

• Remove the cuvette and add the content of one packet of HI 93716-0

DPD reagent. Replace the cap and shake gently for about 20 seconds to

dissolve most of the reagent.

• Reinsert the cuvette into the instrument.

• Press TIMER and the display will show the countdown prior to the

measurement or, alternatively, wait for 2 minutes and 30 seconds and

press READ. When the timer ends the meter will perform the reading.

• The instrument displays the results in mg/L of bromine.

INTERFERENCES

Interference may be caused by: Chlorine, Iodine, Ozone, Oxidized forms of Chromium and Manganese.
In case of water with hardness greater than 500 mg/L CaCO

3

, shake the sample for approximately 2

minutes after adding the reagent.
In case of water with alkalinity greater than 250 mg/L CaCO

3

 or acidity greater than 150 mg/L CaCO

3

,

the color of the sample may develop only partially, or may rapidly fade. To resolve this, neutralize the

sample with diluted HCl or NaOH.

CALCIUM

SPECIFICATIONS

Range

0 to 400 mg/L

Resolution

10 mg/L

Accuracy

±10 mg/L ±5% of reading

Light Source

Tungsten lamp with narrow band interference filter @ 466 nm

Method

Adaptation of the Oxalate method.

REQUIRED REAGENTS

Code

Description

Quantity

-

Buffer Reagent

4 drops

HI 93752

A

-0 Ca Calcium Buffer Reagent

7 mL

HI 93752BBBBB-0 Ca Calcium Oxalate Reagent

1 mL

REAGENT SETS

HI 937521-01

Reagents for 50 tests

HI 937521-03

Reagents for 150 tests

For other accessories see page 128.

MEASUREMENT PROCEDURE

Note: for sample preparation follow the IRRIGATION WATER (LR) procedure at page 17.
• Select the 

Calcium method using the procedure described in the Method Selection section (see page 12).

• Using the 5 mL syringe add exactly 3.00 mL of sample to the cuvette.

• Add 4 drops of Buffer Reagent.

• Use the pipette to fill the cuvette up to the 10 mL mark with

the HI 93752A-0 Calcium Buffer Reagent.

Calcium

3 mL of sample

Bromine

Содержание HI 83200

Страница 1: ...1 Instruction Manual HI 83200 Multiparameter Bench Photometer for Laboratories w w w h a n n a i n s t c o m This Instrument is in Compliance with the CE Directives...

Страница 2: ...y before using the instrument This manual will provide you with the necessary information for the correct use of the instrument If you need additional technical information do not hesitate to e mail u...

Страница 3: ...are optically identical to provide the same measurement conditions Most of methods use the same cuvette for both so it is important that measurements are taken at the same optical point The instrument...

Страница 4: ...elect method menu Press to move up in a menu or a help screen to increment a set value to access second level functions Press to move down in a menu or a help screen to decrement a set value to access...

Страница 5: ...mounts may cause interference they should be removed by treatment with active carbon and filtration Ensure the cuvette is filled correctly the liquid in the cuvette forms a convexity on the top the bo...

Страница 6: ...used more than once stability and storing conditions are described for each method in the related chapter INTERFERENCES In the method measurement section the most common interferences that may be pres...

Страница 7: ...all at once CHEMICAL FORM Chemical form conversion factors are pre programmed into the instrument and are method specific In order to view the displayed result in the desired chemical form press the o...

Страница 8: ...Disable When enabled a short beep is heard every time a key is pressed A long beep alert sounds when the pressed key is not active or an error is detected Press the functional key to enable disable th...

Страница 9: ...depending on the hardness level of water to be treated SAMPLE PREPARATION PROCEDURE Note If the water sample to be analyzed is very turbid let it stand in a beaker for a while until most of the solid...

Страница 10: ...of sample to the graduated cylinder using the 5 mL syringe twice Mix well using the spoon and then wait for 5 minutes Unscrew the filter assembly put a filter disc inside and close it Connect the fil...

Страница 11: ...HI 93712A 0 Ascorbic acid and mix until completely dissolved Add the content of one packet of HI 93712B 0 Aluminon reagent and mix until completely dissolved This is the sample Fill two cuvettes with...

Страница 12: ...d by Iron above 20 mg L Alkalinity above 1000 mg L Phosphate above 50 mg L Fluoride must be absent Aluminum SPECIFICATIONS Range 0 to 500 mg L as CaCO3 Resolution 5 mg L Precision 10 100 mg L Typical...

Страница 13: ...Ammonia MR method using the procedure described in the Method Selection section see page 12 Fill the cuvette with 10 mL of unreacted sample up to the mark and replace the cap Place the cuvette into th...

Страница 14: ...various aliphatic and aromatic amines Ammonia LR SPECIFICATIONS Range 0 00 to 3 00 mg L Resolution 0 01 mg L Accuracy 0 04 mg L 4 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lamp...

Страница 15: ...lder and close the lid Press ZERO key The display will show 0 0 when the meter is zeroed and ready for measurement 10 mL Remove the cuvette Add 4 drops of HI 93700A 0 First Reagent 6 drops for seawate...

Страница 16: ...may develop only partially or may rapidly fade To resolve this neutralize the sample with diluted HCl or NaOH CALCIUM SPECIFICATIONS Range 0 to 400 mg L Resolution 10 mg L Accuracy 10 mg L 5 of readin...

Страница 17: ...escribed in the Method Selection section see page 12 Fill the cuvette with 10 mL of unreacted sample up to the mark and replace the cap Place the cuvette into the holder and close the lid Free Chlorin...

Страница 18: ...key The meter will show 0 0 when the meter is zeroed and ready for measurement Remove the cuvette Powder reagents procedure Add the content of one packet of HI 93701 DPD reagent Replace the cap and sh...

Страница 19: ...strument x 3 x 3 x 1 Total Chlorine TOTAL CHLORINE SPECIFICATIONS Range 0 00 to 3 50 mg L Resolution 0 01 mg L Accuracy 0 03 mg L 3 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lam...

Страница 20: ...ark with the sample Add 0 5 mL of HI 93738A 0 Chlorine Dioxide Reagent to each cylinder 1 2 close them and invert several times to mix 2 25 ml 1 25 ml 1 2 1 2 Press TIMER and the display will show the...

Страница 21: ...t above 25 C 78 F agitation and exposure to light must be avoided INTERFERENCES Interferences may be caused by strong oxidants 10 mL 2 2 Chlorine Dioxide 1 Add the content of one packet of HI 93738B 0...

Страница 22: ...g L Accuracy 5 g L 4 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 525 nm Method Adaptation of the ASTM Manual of Water and Environmental Tech...

Страница 23: ...g L Accuracy 1 g L 4 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 525 nm Method Adaptation of the ASTM Manual of Water and Environmental Techn...

Страница 24: ...CU 10 mL 2 3 2 Color of Water COLOR OF WATER SPECIFICATIONS Range 0 to 500 PCU Platinum Cobalt Units Resolution 1 PCU Accuracy 10 PCU 5 of reading Typical EMC 1 PCU Deviation Light Source Tungsten lam...

Страница 25: ...5 00 mg L Resolution 0 01 mg L Accuracy 0 02 mg L 4 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the EPA meth...

Страница 26: ...0 to 1000 g L Resolution 1 g L Accuracy 10 g L 5 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the EPA method The r...

Страница 27: ...lts in mg L of cyanide Cyanide CYANIDE SPECIFICATIONS Range 0 000 to 0 200 mg L Resolution 0 001 mg L Accuracy 0 005 mg L 3 of reading Typical EMC Dev 0 001 mg L Light Source Tungsten lamp with narrow...

Страница 28: ...he cuvette into the holder and close the lid Press ZERO key The meter will show 0 0 when the meter is zeroed and ready for measurement Fill a graduated beaker up to the 25 mL mark with the sample add...

Страница 29: ...ethod using the procedure described in the Method Selection section see page 12 Add 2 mL of HI 93729 0 SPADNS Reagent to two cuvettes Fill one of the cuvettes with distilled water up to the mark repla...

Страница 30: ...0A 0 Calcium indicator solution and swirl to mix Add 0 5 mL of HI 93720B 0 Alkali solution and swirl to mix Use this solution to rinse 2 cuvettes before filling them up to the 10 mL mark 1 2 Press TIM...

Страница 31: ...sure that the beaker is clean and empty and inject 0 5 mL into the beaker Fill the beaker up to the 50 mL mark with hardness free water INTERFERENCES Interference may be caused by excessive amounts o...

Страница 32: ...EMC 0 02 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 525 nm Method Adaptation of the Standard Methods for the Examination of Water and Wastewater 18th edition EDTA...

Страница 33: ...lank function key to start adjusting the light level The display will show Blank Done when the meter is ready to take a zero measurement Fill a second cuvette with 10 mL of unreacted sample up to the...

Страница 34: ...k and replace the cap Place the cuvette into the holder and close the lid Press ZERO key The display will show 0 0 when the meter is zeroed and ready for measurement Remove the cap and add the content...

Страница 35: ...er and close the lid Press ZERO key The display will show 0 0 the meter is zeroed and ready for measurement Remove the cuvette and add the content of one packet of HI 93721 0 reagent Replace the cap a...

Страница 36: ...see page 12 Fill one graduated mixing cylinder up to the 25 mL mark with deionized water Add the content of one packet of HI 93746 0 TPTZ reagent close the cylinder and shake vigorously for 30 seconds...

Страница 37: ...hen the meter is zeroed and ready for measurement Remove the cuvette Fill another graduated mixing cylinder up to the 25 mL mark with the sample Add the content of one packet of HI 93746 0 TPTZ reagen...

Страница 38: ...g Light Source Tungsten lamp with narrow band interference filter 466 nm Method Adaptation of the Calmagite method REQUIRED REAGENTS Code Description Quantity HI 93752A A A A A 0 Mg Magnesium Buffer R...

Страница 39: ...mg L 3 of reading Typical EMC 0 1 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 525 nm Method Adaptation of the Standard Methods for the Examination of Water and Waste...

Страница 40: ...L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the PAN Method The reaction between manganese and the reagents causes an orange tint in the samp...

Страница 41: ...ple up to the mark and replace the cap Place the cuvette into the holder and close the lid Press ZERO key The display will show 0 0 when the meter is zeroed and ready for measurement Manganese LR Pres...

Страница 42: ...strument Molybdenum Press TIMER and the display will show the countdown prior to the measurement or alternatively wait for five minutes and press READ When the timer ends the meter will perform the re...

Страница 43: ...he reaction between nickel and the reagent causes a blue tint in the sample REQUIRED REAGENTS Code Description Quantity HI 93726 0 Powder reagent 1 packet REAGENT SETS HI 93726 01 Reagents for 100 tes...

Страница 44: ...cal EMC 0 001 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the PAN method The reaction between nickel and the reagents causes an orange ti...

Страница 45: ...cedure described in the Method Selection section see page 12 Using the pipette fill the cuvette with 6 ml of sample up to half of its height and replace the cap Place the cuvette into the holder and c...

Страница 46: ...f one packet of HI 93708 0 reagent Replace the cap and shake gently until completely dissolved 10 mL Nitrate Replace the cap and immediately shake vigorously up and down for exactly 10 seconds Continu...

Страница 47: ...ark with 10 mL of unreacted sample up to the mark and replace the cap Place the cuvette into the holder and close the lid Press ZERO key The display will show 0 0 when the meter is zeroed and ready fo...

Страница 48: ...93732B 0 Add more sample to fill the bottle completely Replace the cap again and ensure that a part of the sample spills over This is to make sure that no air bubbles have been trapped inside which co...

Страница 49: ...e ozone concentration in mg L mg L O3 value A value B STANDARD MEASUREMENT PROCEDURE Select the Ozone method using the procedure described in the Method Selection section see page 12 Fill the cuvette...

Страница 50: ...L CaCO3 will not reliably develop the full amount of color or it may rapidly fade To resolve this neutralize the sample with diluted HCl In case of water with hardness greater than 500 mg L CaCO3 sha...

Страница 51: ...scription Quantity HI 93710 0 Phenol Red Indicator 5 drops REAGENT SETS HI 93710 01 Reagents for 100 pH tests HI 93710 03 Reagents for 300 pH tests For other accessories see page 128 MEASUREMENT PROCE...

Страница 52: ...H RANGE SPECIFICATIONS Range 0 0 to 30 0 mg L Resolution 0 1 mg L Accuracy 1 mg L 4 of reading Typical EMC Dev 0 1 mg L Light Source Tungsten lamp with narrow band interference filter 525 nm Method Ad...

Страница 53: ...cy 0 04 mg L 4 of reading Typical EMC Dev 0 01 mg L Light Source Tungsten lamp with narrow band interference filter 610 nm Method Adaptation of the Ascorbic Acid method The reaction between phosphate...

Страница 54: ...orus PHOSPHORUS SPECIFICATIONS Range 0 0 to 15 0 mg L Resolution 0 1 mg L Accuracy 0 3 mg L 4 of reading Typical EMC Dev 0 2 mg L Light Source Tungsten lamp with narrow band interference filter 525 nm...

Страница 55: ...page 110 Potassium HR Potassium HR POTASSIUM HIGH RANGE SPECIFICATIONS Range 20 to 200 mg L Resolution 5 mg L Accuracy 30 mg L 7 of reading Typical EMC 5 mg L Deviation Light Source Tungsten lamp with...

Страница 56: ...rocedure described in the Method Selection section see page 12 Fill the cuvette with 10 mL of sample up to the mark Add six drops of HI 93750A 0 replace the cap and swirl the solution Place the cuvett...

Страница 57: ...6 drops of HI 93750A 0 Potassium Reagent re place the cap and swirl the solution Place the cuvette into the holder and close the lid 10 mL x 6 Press ZERO key The display will show 0 0 when the meter i...

Страница 58: ...000 ppm Silica SILICA SPECIFICATIONS Range 0 00 to 2 00 mg L Resolution 0 01 mg L Accuracy 0 03 mg L 3 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lamp with narrow band interferen...

Страница 59: ...asurement Alternatively wait for exactly 3 minutes and press READ When the timer ends the meter will perform the reading The instrument displays concentration in mg L of silica SiO2 Press the or to ac...

Страница 60: ...mg L Accuracy 0 005 mg L 10 of reading Typical EMC 0 001 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the PAN method The reaction between...

Страница 61: ...will show 0 0 when the meter is zeroed and ready for measurement Remove the cuvette Sulfate 10 mL SULFATE Silver Press ZERO key The display will show 0 0 when the meter is zeroed and ready for measure...

Страница 62: ...mark with the sample Add the content of one packet of HI 93731A 0 Zinc reagent close the cylinder and invert several times to mix until completely dissolved Fill one cuvette with 10 mL of the reacted...

Страница 63: ...y be caused by Aluminum above 6 mg L Cadmium above 0 5 mg L Copper above 5 mg L Iron above 7 mg L Manganese above 5 mg L Nickel above 5 mg L Zinc Place the cap and insert the cuvette into the instrume...

Страница 64: ...hyde Iodine 0 0 to 12 5 mg L DPD Iron HR 0 00 to 5 00 mg L Phenantroline Iron LR 0 to 400 g L TPTZ Magnesium 0 to 150 mg L Calmagite Manganese HR 0 0 to 20 0 mg L Periodate Oxidation Manganese LR 0 to...

Страница 65: ...ts HI 93750 01 100 potassium HR tests HI 93750 03 300 potassium HR tests HI 93751 01 100 sulfate tests HI 93751 03 300 sulfate tests ACCESSORIES REAGENT SETS HI 93700 01 100 ammonia LR tests HI 93700...

Страница 66: ...leaflets contact your dealer or the Hanna Customer Service Center nearest to you To find the Hanna Office in your vicinity check our home page at www hannainst com RecommendationsforUsers Before using...

Страница 67: ...567 e mail sales hanna co jp Korea Tel 02 2278 5147 Fax 02 2264 1729 e mail mccoyhan chollian net Malaysia Tel 603 5638 9940 Fax 603 5638 9829 e mail hannamal tm net my Norway Tel 23 3811 00 Fax 23 38...

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