DataApex Shimadzu GC2014C APC/AFC Скачать руководство пользователя страница 20 | Manualshive

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4 Using the control module

Clarity Controls

16

4.2.7 Gradients

Menu Path:

Instrument -> Method -> GC Control

Fig. 13 Method Setup - GC - Gradients

This tab displays the temperature gradient as set on the

Method Setup - GC - Oven/Zones

tab.

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Содержание Shimadzu GC2014C APC/AFC

Страница 1: ...trols Shimadzu GC 2014C GC ENG Code Rev M113 26C Date 13 5 2008 Phone 420 251 013 400 DataApex Ltd 2008 Fax 420 251 013 401 Podohradska 1 clarity dataapex com 155 00 Prague 5 www dataapex com The Czec...

Страница 2: ...emarks of DataApex Ltd Microsoft and WindowsTM are trademarks of Microsoft Corporation DataApex reserves the right to make changes to manuals without prior notice Updated manuals can be downloaded fro...

Страница 3: ...14C setup communication 3 3 3 Clarity Configuration 4 4 Using the control module 6 4 1 Hardware Configuration 6 4 2 Method Setup GC 7 4 2 1 Oven Zones 7 4 2 2 INJ 1 2 8 4 2 3 DET 1 4 9 4 2 4 Time Even...

Страница 4: ...VE orange capital italics marks the state of the station or its part Administrator green italics refers to a value or text inserted into a field The bold text is sometimes also used for important part...

Страница 5: ...erial line Fig 1 Shimadzu GC 2014C with AOC 20i autosampler Shimadzu GC 2014C control module provides the means for the direct control of the Shimadzu GC 2014C chromatograph It allows a limited contro...

Страница 6: ...n the PC Modern computers usually have only 1 if any serial COM port installed To use more devices requiring the port the MultiCOM adapter p n MC01 is available Serial cross DB9F DB9F cable p n SK01 C...

Страница 7: ...iring is described in the picture Fig 2 Serial cross cable DB9F DB9F 3 2 Shimadzu GC 2014C setup communication The GC must be fully configured prior to connecting to Clarity No special settings have t...

Страница 8: ...onfiguration In the System Configuration dialog press the Add button to invoke the Available Control Modules dialog Fig 3 Available Control Modules Select the Shimadzu GC 2014C in the GC section and p...

Страница 9: ...ed against the settings of the GC and in case they are not the same the warning message is issued and no control is possible Switch to the Signals tab for more details see the Shimadzu GC 2014C Setup...

Страница 10: ...etting of the GC control method 4 1 Hardware Configuration Menu Path Instrument Method GC Control GC Status Fig 6 Hardware Configuration This dialog is invoked by pressing the GC Status button in the...

Страница 11: ...it range between 400 and 470 C Equilibry Time Time that the GC needs to reach the temperature equilibrium after the temperature program gets to the set initial temperature This time is used to distrib...

Страница 12: ...ead from GC it serves for the information purposes only 4 2 2 INJ 1 2 Menu Path Instrument Method GC Control Fig 8 Method Setup GC INJ 1 This tab governs the settings concerning the injection port of...

Страница 13: ...rameters for a detector configured in the Shimadzu GC 2014C Setup dialog Particular fields may vary according to the type of the detector set On Off Switches the detector on and off The detector switc...

Страница 14: ...larity or vice versa polarity Range Applies on the analog detector signal before its processing to the digital data directly in the Shimadzu GC 2014C This value serves for the compensation of the over...

Страница 15: ...ere applicable setting temperatures to detector injector auxiliary zones etc To delete a row simply delete the value in the Time column on that row The table should be filled with the Time of the even...

Страница 16: ...n the Time Events table Event Operation Performs an event operation defined by the event code These codes may be used as a positive number or negative number in which case the opposite of the operatio...

Страница 17: ...e number of method runs doesn t have any meaning for Clarity as the method is usually sent after each injection thus resetting the counter after each injection For more details consult Shimadzu manual...

Страница 18: ...tograph will do nothing when the analysis is completed Set Off after analysis The chromatograph performs the System Off function check Shimadzu GC 2014C manual for more details This function is useful...

Страница 19: ...the leakage of possibly dangerous gasses hydrogen into the laboratory environment Zero at ready When checked the chromatograph performs the autozero action after it becomes READY Auto flame ON When c...

Страница 20: ...control module Clarity Controls 16 4 2 7 Gradients Menu Path Instrument Method GC Control Fig 13 Method Setup GC Gradients This tab displays the temperature gradient as set on the Method Setup GC Ove...

Страница 21: ...to set the particular Sampling Rate on the appropriate tab This sampling rate in fact states the frequency of the data sending from the Shimadzu GC 2014C detector to Clarity it has nothing to do with...

Страница 22: ...n oven Besides that it also shows the run time of the analysis System On Allows to switch the chromatograph on It starts the temperature program in the column oven detectors and injectors System Off S...

Страница 23: ...Autodetect function because these settings are checked against those in the GC when opening the Instrument window If they don t match the control is not possible The only parts of the dialog that can...

Страница 24: ...log Piping tab Fig 17 Shimadzu GC 2014C Setup Piping Car 1 3 Allows to set the possible operation modes for carrier gasses For Shimadzu GC 2014C chromatographs without automatic flow control function...

Страница 25: ...ount Defines the number of signals that will be transferred to the Clarity These signals correspond to Clarity detectors and will have their own sub tabs in the Method Setup Acquisition dialog if conf...

Страница 26: ...the default names of particular temperature zones as set in the Shimadzu GC 2014C chromatograph Names Allows to set desired names for particular temperature zones By default these names are the same...

Страница 27: ...Shimadzu GC 2014C Setup Line Config This tab shows the position of particular components on the analytical lines in the chromatograph Up to four independent lines may be configured All settings on thi...

Страница 28: ...from all major windows Fig 21 Shimadzu GC 2014C report preview All chromatograph specific settings e g temperatures set to particular temperature zones are reported as a part of the data displayed by...

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