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9

ZTKS0172 / Z31964 / 04

1

Introduction

1.1

General Information

This manual contains important information about the handling of the supplied magnet
system used for NMR spectroscopy and its components. The compliance with all safety
and handling instructions, the applicable local accident prevention and general safety
regulations are necessary for safe work.

This manual is part of the product. It must be kept nearby the magnet system and free
access must be ensured at any time. Read the manual carefully before handling the
magnet system or its components.

1.2

Limitation of Liability

The information in this manual will take into account the current state of the technology.

The manufacturer assumes no liability for damages resulting from:

•

non-compliance with the instructions and all applicable documentation,

•

use for purposes not intended,

•

not sufficiently approved persons,

•

arbitrary changes or modifications and

•

use of not approved spare parts or accessories.

1.3

Customer Service

Technical support is provided by Bruker Service via telephone or e-mail. For contact
information see

of this document.

1.4

Warranty

The warranty terms can be found in the sales documents of the magnet system and in
the Terms and Conditions of Bruker BioSpin AG.

1.5

Copyright

No part of this publication may be reproduced, stored in a retrieval system, or transmit-
ted, in any form or by any means without the prior consent of the publisher. Product
names used are trademarks or registered trademarks of their respective holders.

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Содержание 500'89 Ascend Aeon

Страница 1: ...Version Innovation with Integrity 500 89 Ascend 04 User Manual NMR ...

Страница 2: ...marks of their respective holders This manual was written by Renate Petry July 26 2018 Bruker Corporation Faellanden Switzerland ZTKS0172 Z31964 04 For further technical assistance on the NMR Magnet System please do not hesitate to contact your nearest BRUKER dealer or contact us directly at BRUKER BioSpin AG Industriestrasse 26 CH 8117 Faellanden Switzerland Phone 41 44 825 91 11 FAX 41 44 825 96...

Страница 3: ...fety Devices 16 2 4 4 Spare Parts 16 2 4 5 Signs and Labels 17 2 4 6 Technical Risks 17 2 5 Personal Protective Equipment 23 2 6 Description of Signs and Labels 24 2 7 Safety Devices 25 2 8 Behavior in Danger and Emergency Situations 27 2 9 Fire Department Notification 27 3 Transportation 29 3 1 Safety 29 3 2 Packaging 29 3 2 1 Disposal 30 3 3 Transport Inspection 30 3 4 Transportation by Fork Lif...

Страница 4: ...4 Maintenance free Components 56 8 Disassembling 57 9 Technical Data MS 500 89 Ascend 59 9 1 Environmental Conditions 59 9 2 Identification Plate 59 9 3 Dimensions 60 9 3 1 Weights 60 9 3 2 Dimensions for Transportation 60 9 3 3 Dimensions Cryostat 61 9 4 Safety Valves 64 9 5 Nitrogen Level Sensor 65 9 6 Helium Level Sensor 66 9 7 Temperature Sensors 67 9 8 Technical Data Magnet 69 9 9 Fringe Fiel...

Страница 5: ...d Currents 79 9 21 Current Lead 81 9 21 1 Wiring Diagram Magnet 82 9 21 2 Wiring Diagram Magnet Control and Shims 83 9 21 3 Wiring Diagram Magnet Diagnostic and Temperature Sensors 84 9 21 4 Shorting Plug 85 9 22 Nitrogen Refill Report 86 9 23 Helium Refill Report 88 Appendix A 91 A 1 Warning Signs 91 A 2 Figures 93 A 3 Tables 95 A 4 Index 97 ...

Страница 6: ...6 ZTKS0172 Z31964 04 Table of Contents ...

Страница 7: ...rasse 26 CH 8117 Faellanden Switzerland Phone 41 44 825 91 11 Fax 41 44 825 96 96 http www bruker com E mail 2nd level support bbio bruker com Please refer to the Model No Serial No and Internal Order No in all correspondence regarding the NMR system or components thereof ...

Страница 8: ...8 ZTKS0172 Z31964 04 Contact ...

Страница 9: ... of the technology The manufacturer assumes no liability for damages resulting from non compliance with the instructions and all applicable documentation use for purposes not intended not sufficiently approved persons arbitrary changes or modifications and use of not approved spare parts or accessories 1 3 Customer Service Technical support is provided by Bruker Service via telephone or e mail For...

Страница 10: ... The isolators in the magnet stand absorb floor vibrations Different heights and isolators are available optionally The nitrogen turrets 4 connected with the nitrogen flow system 7 and the heat exchangers 5 are the interface to the nitrogen vessel The nitrogen fill in turret is marked with a green label The helium turrets 6 9 connected with the helium flow system 8 are the interface of the helium ...

Страница 11: ...onnel As a result of professional training by Bruker Service Personnel experience and knowledge of applicable regulations these persons are qualified to perform the specific tasks on the magnet system and its components assigned to them in this manual Approved Customer Personnel are qualified to identify possible hazards and risks associated with the tasks assigned to them and to perform all possi...

Страница 12: ...truction plates The customer has to ensure the intended use of the magnet system The customer has to inform the local fire brigade about the special risks of the magnet system and how to react in the event of an incident The customer must clearly define the responsibilities for operation and maintenance The customer must ensure that all employees working with the magnet system have read and unders...

Страница 13: ...r serious injury This signal word is limited to the most extreme situations This is the consequence of not following the warning 1 This is the safety condition This is the safety instruction WARNING WARNING Indicates a hazardous situation that if not avoided could result in death or serious injury This is the consequence of not following the warning 1 This is the safety condition This is the safet...

Страница 14: ... safety condition This is a safety instruction SAFETY INSTRUCTIONS SAFETY INSTRUCTIONS are used for control flow and shutdowns in the event of an error or emergency This is the consequence of not following the safety instructions 1 This is a safety condition This is a safety instruction This symbol highlights useful tips and recommendations as well as information designed to ensure efficient and s...

Страница 15: ...ust only be carried out by approved persons with applicable qualifications The necessary qualifications are specified in the beginning of the relevant chapter In case of doubt contact Bruker Service Contact information see page 7 of this document WARNING Risk of damage to life and limb by incorrect use of the magnet system Incorrect use of the magnet system can lead to life threatening situations ...

Страница 16: ...devices Do not remove safety devices Check the operational reliability of the safety devices before working on the magnet system WARNING Risk of injury and property damage from using incorrect or defective spare parts and accessories Incorrect or defective spare parts can cause serious injuries They may cause damaging malfunctioning and the destruction of the magnet system Only use original equipm...

Страница 17: ...health Duration of exposure 8 h day above the limit of 200 mT can cause damage to health Ferromagnetic tools in the magnetic field are significantly hazardous Disks and electronic devices may be damaged Mark the magnetic field of more than 0 5 mT 5 Gauss before start up Keep people with active medical implants away from the 0 5 mT 5 Gauss area The permanent workplace of employees must be outside t...

Страница 18: ...nic agents are extremely cold Contact with liquid or gaseous cryogenic agents will lead to cold burns Contact with the eyes may cause blindness Refer to Warning Low Temperature on page 20 Only use cryogenic agents in well ventilated rooms In case of doubt ask Bruker Service Wear an oxygen monitor on the body during service and maintenance work Prevent any skin contact with liquid or gaseous cryoge...

Страница 19: ...stat and further equipment The helium or the nitrogen vessel of the cryostat may get sealed off due to ice formation inside the helium or the nitrogen turrets in case of non compliance with the instruction given in this manual This may lead to overpressure and damage of the helium or the nitrogen vessel Manipulations of components with gas under pressure may lead to injury and property damage In c...

Страница 20: ...ure sensitive components such as O rings from contact with liquid cryogenic agents WARNING Risk of injury from spontaneous ignition and explosion caused by liquid oxygen Pure oxygen condenses on extremely cold metal pieces Together with oil it may ignite spontaneously In case of fire the pure oxygen may cause an explosion Do not smoke near the magnet system Do not use open flames near the magnet s...

Страница 21: ...tem on your own WARNING Risk of damage to life and limb caused by heavy weights Lifting heavy weights is life threatening due to falling or moving parts Do not stay or work under a lifted magnet system All lifting equipment in use must be approved to carry the weight Do not use damaged lifting equipment Do not use lifting equipment without updated check tag Lifting only with approved qualification...

Страница 22: ...e boxes in an upright position Do not tilt the boxes Prevent crossing thresholds even if they are only a few millimeters high Clean the transportation way before moving the box Unpack shortly before assembling The cryostat or further equipment must be protected from rain and other bad weather conditions during transportation Exclusively move the cryostat in its original box Do not remove the tight...

Страница 23: ...ontact with extremely cold liquids or surfaces and for protection from injury caused by rough edges Protective Clothes Used to protect the body from injury caused by contact with extremely cold liquids or surfaces and for protection from wounds Safety Shoes Used to protect the feet from injury from falling of heavy objects An anti slip sole protects from injury caused by slipping and falling on sl...

Страница 24: ... to enter these areas Prohibition sign No watches or electronic devices Watches and electronic devices may be damaged in the identified area of 0 5 mT 5 Gauss Prohibition sign No credit cards or other magnetic memory Credit cards and magnetic memory may be damaged in the identified area of 0 5 mT 5 Gauss Prohibition sign Do not touch Do not block Do not touch or block the identified area Hazard wa...

Страница 25: ...the magnet system is equipped with the following safety devices Figure 2 1 Safety devices of the cryostat with 2 helium turrets 1 Drop off plate 2 One way valve of the nitrogen vessel 3 Safety valve of the nitrogen vessel 4 One way valve of the helium vessel 5 Quench valves ...

Страница 26: ...e of an accidental overpressure in the nitrogen vessel the safety valve will release the pressure smoothly Drop off Plate The drop off plate 1 is a safety device of the RT vessel If the vacuum breaks the drop off plate will open In case of an accidental overpressure in the RT vessel the drop off plate will release the pressure smoothly One way Valves The one way valves of the nitrogen flow system ...

Страница 27: ...Burns Help the injured persons to lie down comfortably in a warm room Loosen all clothing which could prevent blood circulation in the injured area Pour large quantities of warm water over the affected parts Cover the wound with dry and sterile gauze In case of contact of liquid cryogenic agents with the eyes rinse thoroughly with clean water Call for medical assistance 2 9 Fire Department Notific...

Страница 28: ...28 ZTKS0172 Z31964 04 Safety ...

Страница 29: ...ctions in this chapter and to inform these persons before 3 2 Packaging WARNING Heavy Weights see page 21 CAUTION Transportation see page 22 Figure 3 1 Packaging without surrounding panels The cryostat is supplied in a wooden box on a pallet It is secured inside with straps against tilting and moving Accessories such as the flow systems level sensors and bore tubes are in the side compartment of t...

Страница 30: ...s Shock Watch Tilt Watch on the boxes show if the boxes were kicked or tilted during transportation Checks Shock Watch Follow instructions on the label Tilt Watch Follow instructions on the label In case of damage Accept delivery with reservation Make a documentation of all observable damage and add it to the transportation documents Start complaint process Contact Bruker Service before installati...

Страница 31: ... view 1 Check the route of transport for the minimal height and width 2 Check sufficient floor capacity on the route of transport In case of doubt ask a stress analyst 3 Check sufficient carrying capacity while using an elevator 4 Position the forks between the bars of the box as shown in the figure Make sure the side towards the operator is the one with the labels on it Figure 3 3 Transportation ...

Страница 32: ...ked eyelets as attachment points for the lifting equipment 2 Use all eyelets for the lifting equipment Figure 3 5 Instruction label for lifting equipment 3 Follow the instructions on the label on top of the cryostat This label gives important information about correct attachment and transportation 4 Check for correct fastening of the lifting equipment before lifting the cryostat 5 Make sure that a...

Страница 33: ...s in a closed dry and dust free room Store the boxes upright Do not tilt the boxes Do not unpack the supplied boxes Prevent mechanical vibrations to the boxes Storage temperature 5 40 C Storage humidity less than 50 23 C 3 7 Disposal For disposal after the life cycle please contact Bruker Service for further information For contact information see page 7 of this document ...

Страница 34: ...34 ZTKS0172 Z31964 04 Transportation ...

Страница 35: ...35 ZTKS0172 Z31964 04 4 Assembling Approved Persons Bruker Service only ...

Страница 36: ...36 ZTKS0172 Z31964 04 Assembling ...

Страница 37: ... Z31964 04 5 Operation 5 1 Safety Approved Persons Bruker Service Approved Customer Personnel WARNING Magnetic Field see page 17 Cryogenic Agents see page 18 Electricity see page 18 Gas under Pressure see page 19 ...

Страница 38: ...with a magnet stand with pneumatic isolators Set the magnet stand into operation by switching the pneumatic controller to UP position Figure 5 2 Stop the magnet stand For any work at the magnet system like maintenance or refill of cryogenic agents stop the magnet stand by switching the pneumatic controller to DOWN position ...

Страница 39: ...page 7 of this manual 6 1 Safety Only approved persons should perform the troubleshooting tasks They are outlined in this chapter Bruker Service Approved Customer Personnel Personal protective equipment Protective goggles Protective gloves Protective clothes Safety shoes WARNING Magnetic Fields see page 17 Cryogenic Agents see page 18 Electricity see page 18 Gas under Pressure see page 19 Spontane...

Страница 40: ...cess Approved Customer Personnel Indicator Possible reason Solution Performed by Ceiling height too low for assembling on magnet stand Site does not meet the required conditions Choose another site that meets the required conditions Bruker Service Ceiling height too low for inserting the Helium Level Sensor Site does not meet the required conditions Insert the Helium Level Sensor before mounting t...

Страница 41: ...lve the drop off plate the reduction and sealing flanges the bottom plate a Bruker Service Defective pumping unit or pumping line Check pumping unit and pumping line A vacuum of at least 10 6 mbar must be reached while the sealing plug is closed Replace if necessary Bruker Service Room temperature bore has scratches or dust on the sealing surfaces Check sealing surfaces on the RT bore No scratches...

Страница 42: ...ckly Transfer pressure too high Stop cooling Adjust correct transfer pressure Bruker Service Vacuum in RT vessel does not reach 5 x 10 5 mbar within 48 hours O rings are leaky Check and clean O rings and slots If necessary replace the O rings for the vacuum valve the drop off plate the reduction and sealing flanges the bottom plate a Bruker Service O rings are frozen due to contact with liquid nit...

Страница 43: ...efully remove all liquid nitrogen using the precooling tube 3 Use the dipstick to check that the helium vessel is empty no liquid nitrogen or frozen nitrogen Bruker Service After some intervals of flushing it is not possible to reach a vacuum in the range of 1 mbar The globes in the quench valves are not fitting correctly in the O rings and thus the quench valves are leaky 1 Stop pumping 2 Remove ...

Страница 44: ...eck that the helium vessel is empty no liquid nitrogen or frozen nitrogen Bruker Service Transfer of liquid helium does not start The transportation dewar is empty Refill or replace transporta tion dewar Bruker Service The transfer pressure in the transportation dewar is too low Increase the transfer pressure Bruker Service The transportation dewar is leaky no transfer pressure is built up Check t...

Страница 45: ...rret between Helium Level Sensor and connector Bruker Service The Helium Level Sensor is defective Check the Helium Level Sensor using the 0 calibration plug Bruker Service The helium level does not reach 100 after cooling Empty transpor tation dewar helium transfer stopped Refill or replace transporta tion dewar Bruker Service The Helium Level Sensor is disturbed by the transfer line s extension ...

Страница 46: ... it can be inserted correctly into the connector Bruker Service Main coil heater test fails Power supply defective Replace the power supply Bruker Service Connector or cables defective Clean connectors or replace cables if necessary Bruker Service Setting of sense voltage fails The main coil heater switch is OFF The main coil switch is not opened Switch the main coil heater to ON and check the mai...

Страница 47: ...ng for the warm helium gas to remove small ice spots from the connector Bruker Service The magnet system quenches Loss of superconductivity See After a Quench on page 54 Bruker Service The helium level was too low for energizing cycling shimming de energizing or sweeping See After a Quench on page 54 Bruker Service The power supply is defective The main current is oscillating Replace the power sup...

Страница 48: ... wrong position Change the switch position Bruker Service Shims do not affect the NMR signal Shim heater current is not correct The shim switches are not opened Set the shim heater current to the specified value See Energizing Assign ment and Currents on page 76 Bruker Service Magnet system does not reach specification Magnetic material inside RT bore tube Carefully clean the RT bore tube Bruker S...

Страница 49: ...les in loose S or U shapes Approved Customer Personnel If the problem is still not solved contact Bruker Service Approved Customer Personnel Magnet system is touching the magnet stand Check the level adjust if necessary Approved Customer Personnel Piston of the isolator is not centered or is touching its casing Align magnet stand Bruker Service T safety bracket is touching the pillar Align magnet ...

Страница 50: ... is not level Stop the pneumatic isolators Check the level of the cryostat Bruker Service Defective leveling valve Replace leveling valve or isolator Bruker Service Defective membrane of an isolator Replace leveling valve or isolator Bruker Service The movement of the magnet stand is not smooth Piston is not centered or is touching its casing Align magnet stand Bruker Service Audible loss of gas D...

Страница 51: ...re than 600 mm from the top of the helium turrets Bruker Service The helium boil off is too high The Helium Level Sensor is in service mode or has been used too often Switch off Helium Level Sen sor Reduce frequency of helium level measurement during measuring of the helium level an amount of helium boils off due to the heat input of the Helium Level Sensor Approved Customer Personnel The atmosphe...

Страница 52: ...out of MICS is false Helium Level Sensor defective Contact Bruker Service immediately Approved Customer Personnel Helium level at constant level no change during days Helium Level Sensor defective Contact Bruker Service immediately Approved Customer Personnel WARNING Low Temperature Helium level warning out of MICS is false Helium Level Sensor defective Replace Helium Level Sensor see chapter Repl...

Страница 53: ...l cable to the current lead and to the Power Supply correctly Bruker Service The switch Main Coil OFF Shim Coil is not on the Shim Coil position Switch Main Coil OFF Shim Coil on the Shim Coil position Bruker Service High helium flow after breaking vacuum Remaining cryogenic agents in the vessels Remove liquid cryogenic agents Bruker Service Vacuum still remains after 12 hours Vacuum valve is clos...

Страница 54: ...n the correct position 4 Remove probe and shim system to prevent formation of ice on the shim system 5 Start the refill with liquid helium as soon as possible 6 Contact Bruker Service immediately Figure 6 1 Magnet system during a quench A quench is the very fast de energizing of the magnet by loss of its superconductivity The stored magnetic energy is converted into heat which promotes rapid evapo...

Страница 55: ...l Personal protective equipment Protective goggles Protective gloves Safety shoes 7 2 Cleaning Clean the RT vessel of the magnet system and the magnet stand with a dry or slightly damp cloth Only use water and neutral detergents Do not use volatile cleaning solvents WARNING Magnetic Field see page 17 Cryogenic Agents see page 18 Electricity see page 18 Gas under Pressure see page 19 Low Temperatur...

Страница 56: ...is case contact Bruker Service Approved Customer Personnel weekly Cryostat Check the nitrogen level Refill liquid nitrogen if necessary Follow the safety instructions of the supplied manual Refilling Procedure Z31326 Weekly refill of liquid nitrogen is recommended Record the filling session A record of changes in the estimated consumption may be used to identify problems In this case contact Bruke...

Страница 57: ...57 ZTKS0172 Z31964 04 8 Disassembling Approved Persons Bruker Service only ...

Страница 58: ...58 ZTKS0172 Z31964 04 Disassembling ...

Страница 59: ...et System Identifier Type Magnet Identifier Serial Number Year of Construction Cryostat Identifier Specification Helium Vessel Specification Nitrogen Vessel Specification Vacuum Chamber Weight empty and completely filled including magnet stand Value Unit Minimum surrounding temperature 7 C Maximum surrounding temperature 38 C Maximum relative humidity up to 31 C 80 Maximum relative humidity betwee...

Страница 60: ...kg Operational weight completely filled with magnet stand 847 kg Weight magnet stand 118 kg Weight magnet stand ready for transportation including box 184 kg Weight magnet system empty ready for transportation including box and transportation locks 743 kg Table 9 2 Weight of the magnet system L x D x H Unit Box with magnet system 114 x 93 x 199 cm3 Box with magnet stand 79 x 76 x 149 cm3 Table 9 3...

Страница 61: ...61 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 3 3 Dimensions Cryostat Front View Figure 9 1 Dimensions of the cryostat front view ...

Страница 62: ...t for transportation 1604 mm H3 Height Cryostat bottom plate to flow system 1763 mm S Height Magnet Stand floor to bottom plate 950 mm M1 Distance magnetic center to bottom flange calculated Refer to Table 9 17 on page 77 for the measured distance of the magnetic center to bottom flange MCB 416 mm M2 Distance magnetic center to top flange calculated Refer to Table 9 17 on page 77 for the measured ...

Страница 63: ... Top View 1 Keep at least an additional free space of 1 5 m around the magnet system for service Figure 9 2 Dimensions of the cryostat top view Cryostat Dimensions Value Unit W1 1236 mm W2 1116 mm D3 1 1375 mm Table 9 5 Dimensions of the cryostat top view ...

Страница 64: ...en vessel 2 Safety valve of the nitrogen vessel 3 One way valve of the helium vessel 4 Quench valve Opening pressure mbar psi One way valve of the nitrogen vessel 10 0 15 Safety valve of the nitrogen vessel 140 2 One way valve of the helium vessel 15 0 2 Quench valve 180 2 6 Table 9 6 Opening pressure of the safety valves of the magnet system ...

Страница 65: ...hts display the nitrogen level see Figure 9 4 Nitrogen Level Sensor Material No Value Unit Level Sensor Type Z122404 12 1126 860 D325 Diameter 12 mm Overall length 1126 mm Active length 860 mm Table 9 7 Nitrogen level sensor Figure 9 4 Nitrogen level sensor Nitrogen Level at more than 90 70 90 50 70 30 50 10 30 Schedule Refill less than 10 Refill immediately ...

Страница 66: ...e helium fill in turret Helium Level Sensor Material No Value Unit Level Sensor Type Z58103 1500 874 D37X Overall length 1500 mm Active length 874 mm Calibration 0 Calibration resistor Z53168 violet 177 Ω Calibration 100 Calibration resistor Z28628 black 15 Ω Table 9 8 Helium level sensor Figure 9 5 Helium level sensor ...

Страница 67: ...ng cooling down and warming up the magnet system PT 100 Sensor Measure the resistance with a maximum current of 1 mA Temperature Unit Resistance Unit Room Temperature 293 K 107 8 Ω 273 K 100 0 Ω 250 K 91 0 Ω 200 K 71 1 Ω 150 K 50 9 Ω 100 K 30 0 Ω Liquid Nitrogen 77 K 20 1 Ω Table 9 9 Characteristic values of PT 100 sensor Figure 9 6 Characteristic curve of PT 100 sensor ...

Страница 68: ...ximum current of 0 1 mA Temperature Unit Resistance Unit Room Temperature 300 K 220 Ω Liquid Nitrogen 77 K 265 Ω 40 K 300 Ω 20 K 350 Ω 10 K 420 Ω 8 K 450 Ω 6 K 500 Ω 5 K 540 Ω Liquid Helium 4 2 K 575 Ω Table 9 10 Characteristic values of IBT carbon sensor Figure 9 7 Characteristic curve of IBT carbon sensor ...

Страница 69: ...ergized Persistent Mode In the persistent mode the current flows exclusively within the magnet The circuit has no connection to the outside The magnetic field cannot be switched off Technical Data Magnet Value Unit Proton frequency 500 MHz Central field 11 74 T Coil inductance 42 94 H Magnetic energy 736 6 kJ Maximum drift rate 0 01 ppm h 5 0 Hz h Table 9 11 Specification of the magnet T h i s p a...

Страница 70: ...5 0 mT 0 50 m 0 88 m 3 0 mT 0 54 m 0 97 m 1 0 mT 0 62 m 1 21 m 0 5 5 Gauss mT 0 70 m 1 40 m 0 2 mT 0 92 m 1 73 m 0 1 mT 1 17 m 2 07 m 0 05 mT 1 52 m 2 49 m max magnetic field B0 at access point 314 mT max field gradient dB dz at access point 4 7 T m Table 9 12 Fringe field data of the magnet system at maximum field T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d...

Страница 71: ... Helium needed for cool down 300 l Helium needed for energizing cryo shimming and quench reserve 300 l Table 9 13 Cryogenic agents consumption during installation Cryogenic Agents Value Unit Nitrogen vessel total volume 134 l Nitrogen refill volume 104 l Nitrogen evaporation rate 270 ml h Nitrogen hold time1 16 days Helium vessel total volume 90 l Helium refill volume 68 l Helium evaporation rate ...

Страница 72: ...l Graph Figure 9 9 Nitrogen level graph 1 HYHOJUDSK 0 86 5HSRUW 9HULILHG QG 5HOHDVHG 3 PP OLWUHV WRS RI 1 YHVVHO PLQLPXP DOORZHG OHYHO RI QLWURJHQ OHYHO VHQVRU RI QLWURJHQ OHYHO VHQVRU T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a ...

Страница 73: ...re 9 10 Helium level graph H HYHOJUDSK 0 86 5HSRUW 9HULILHG QG 5HOHDVHG 3 PP OLWUHV WRS RI KHOLXP YHVVHO PLQLPXP OHYHO GXULQJ HQHUJL LQJ PLQLPXP DOORZHG OHYHO WRS RI FRLO RI KHOLXP OHYHO VHQVRU T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a ...

Страница 74: ... Con SHIM Shim Coils Ω From To PIN C D E F PIN S 10 PIN Con SHIM 19 PIN Con CONTROL Shim Coil to Heater common Ω From To PIN T High current Con 19 PIN Con CONTROL High Current to Sense Ω From To High current Con High current Con Main Coil Ω From To PIN U High current Con 19 PIN Con CONTROL High Current to Sense Ω From To PIN F PIN S 19 PIN Con CONTROL 19 PIN Con CONTROL Z Heater Ω From To PIN T PI...

Страница 75: ...ents Value Unit Main heater current mA Shim heater current mA Table 9 16 Heater currents Shim Switch Heater Operation Z0 not heated Z1 automatic Z2 permanent Z3 automatic X automatic Y automatic XZ automatic YZ automatic XY automatic X2 Y2 automatic Table 9 17 Shim switch heater operation T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a ...

Страница 76: ...0 148 17 to 175 95 500 175 95 to 185 21 200 Overshoot 0 22 of final current 185 21 Final current to 185 62 Overshoot 50 10 minutes break at overshoot current 185 62 Overshoot to 185 21 Final current 50 Total energizing time min 143 Rate of current ramp down with magnet in persistent mode A min 20 Mandatory wait time between energizing and shimming h 18 Table 9 18 Energizing assignment and currents...

Страница 77: ... from bottom flange MCB 416 mm Shimsystem Offset SO see Figure 9 11 and refer to the supplied Test Protocol AST mm Table 9 19 Magnetic center Figure 9 11 Magnetic center and shimsystem offset SO MC Magnetic Center MCT Magnetic Center from Top Flange MCB Magnetic Center from Bottom Flange SO Shimsystem Offset T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a ...

Страница 78: ...nts Value Unit Shim current rate A min Z1 Shim current A Z2 Shim current A Z3 Shim current A X Shim current A Y Shim current A XZ Shim current A YZ Shim current A XY Shim current A X2 Y2 Shim current A Frequency change due to cycling kHz Date and Signature Table 9 20 Cycling assignment and shim currents T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a ...

Страница 79: ...current A XZ Shim current A YZ Shim current A XY Shim current A X2 Y2 Shim current A Shimsystem Offset design value Refer to the supplied Test Protocol AST mm Shimsystem Offset Customer Site value mm Date and Signature Table 9 21 Cryo shim currents Deenergizing Currents A Sense Voltage mV Remarks Bruker Test Site 185 21 to 175 95 200 175 95 to 148 17 500 148 17 to 0 1500 Total deenergizing time mi...

Страница 80: ...80 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend This page is intentionally left blank T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a ...

Страница 81: ...81 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 21 Current Lead Figure 9 12 Current lead 55 pin ...

Страница 82: ...82 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 21 1 Wiring Diagram Magnet Figure 9 13 Wiring diagram magnet ...

Страница 83: ...83 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 21 2 Wiring Diagram Magnet Control and Shims Figure 9 14 Wiring diagram magnet control and shims ...

Страница 84: ...84 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 21 3 Wiring Diagram Magnet Diagnostic and Temperature Sensors Figure 9 15 Wiring diagram magnet diagnostic and temperature sensors ...

Страница 85: ...emoval of the current lead After inserting the shorting plug the current flows through the shorting plug and no longer through the current lead and the power supply 1 Shorting Plug Tool for fitting and removing the shorting plug 2 Shorting Plug 3 Shorting Plug view from pin side Figure 9 16 Shorting plug 55 pins ...

Страница 86: ...86 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 22 Nitrogen Refill Report Nitrogen level before refill Nitrogen level after refill Refill Volume l Date Time Signature ...

Страница 87: ...87 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend Table continued Nitrogen level before refill Nitrogen level after refill Refill Volume l Date Time Signature ...

Страница 88: ...88 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend 9 23 Helium Refill Report Helium level before refill Helium level after refill Refill Volume l Date Time Signature ...

Страница 89: ...89 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend Table continued Helium level before refill Helium level after refill Refill Volume l Date Time Signature ...

Страница 90: ...90 ZTKS0172 Z31964 04 Technical Data MS 500 89 Ascend ...

Страница 91: ...eavy Weights 21 Intended Use 15 Key Word and Symbol 13 Low Temperatures 20 Magnetic Field 17 Persons 15 Quench 19 Safety Devices 16 Signs and Labels 17 Slippage 20 Spare Parts 16 Spontaneous Ignition and Explosion 20 Caution Incorrect Transportation 22 Key Word and Symbol 13 Notice Key Word and Symbol 14 S Safety Instructions Key Word and Symbol 14 ...

Страница 92: ...92 ZTKS0172 Z31964 04 Warning Signs ...

Страница 93: ...nch 54 Figure 9 1 Dimensions of the cryostat front view 61 Figure 9 2 Dimensions of the cryostat top view 63 Figure 9 3 Safety valves of the cryostat 64 Figure 9 4 Nitrogen level sensor 65 Figure 9 5 Helium level sensor 66 Figure 9 6 Characteristic curve of PT 100 sensor 67 Figure 9 7 Characteristic curve of IBT carbon sensor 68 Figure 9 8 Fringe field plot of the magnet system at maximum field 70...

Страница 94: ...94 ZTKS0172 Z31964 04 List of Figures ...

Страница 95: ...ensor 65 Table 9 8 Helium level sensor 66 Table 9 9 Characteristic values of PT 100 sensor 67 Table 9 10 Characteristic values of IBT carbon sensor 68 Table 9 11 Specification of the magnet 69 Table 9 12 Fringe field data of the magnet system at maximum field 70 Table 9 13 Cryogenic agents consumption during installation 71 Table 9 14 Cryogenic agents 71 Table 9 15 Resistance at room temperature 7...

Страница 96: ...96 ZTKS0172 Z31964 04 List of Tables ...

Страница 97: ...66 I IBT Carbon Resistor 68 Identification Plate 59 Intended Use 15 L Liability 9 Low Temperatures 20 M Magnetic Center 77 Magnetic Field 17 O One way Valves 26 P Persistent Mode 69 Portable Oxygen Monitor 23 Protective Clothes 23 Protective Gloves 23 Protective Goggles 23 PT 100 Sensor 67 Q Quench 19 54 Quench Valve 26 R Rescue Equipment 27 S Safety Devices 25 Safety Shoes 23 Safety Valve 26 Shim...

Страница 98: ...98 ZTKS0172 Z31964 04 Index ...

Страница 99: ...First release 01 September 2012 Update and released fringe field data and related directives 02 February 2013 Update Magnetic Center 03 June 2013 New layout front and rear page 04 August 2018 Update of chapter Technical Data magnet design C New calculation of Nitrogen minimum allowed level ...

Страница 100: ...Bruker Corporation info bruker com www bruker com Order No Z31964 ...

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