BAS LC-4C, Инструкция по эксплуатации

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Table 3.1
Parts of the assembled LC-44 Amperometric Detector (refer to Figures 3.1–3.4).
Ref. # Description
1 LC-4C Amperometric Detector
2 CC-5 Flowcell Compartment
3 Injection Valve (installed only in the BAS 480 liquid chromatographs, but available from BAS for installation by customers
who wish to upgrade their detectors and use them as the basis for an LC system)
4 Utility Panel (this is removed when the unit is upgraded for cartridge column temperature control, model LC-22C/23C)
5 Optional Preheater Module (120 V/60 Hz or 240 V/50 Hz)
6 Optional LC-22C Temperature Controller for Detector Preheater Module or Cartridge Column Heater Temperature Control
(120 V/60 Hz or 240 V/50 Hz)
7 Stainless Steel Auxiliary Electrode
8 Reference Electrode Retainer (packaged in detector accessories box)
9 Working Electrode Clamp and backing plate (packaged in detector accessories box)
10 Single Electrode Cable (dual electrode cable has two working electrode leads)
11 Generator Electrode Lead
12 Power Cord/Fuse location on LC-4C Controller
13 Dual Working Electrode Block (glassy carbon is standard)
14 Reference Electrode (pkg. of 3 RE-4 Ag/AgCl/gel reference electrodes is provided in detector accessories box)
15 TG-2M Electrode Gasket (4 of these translucent gaskets are in the same small box with the electrode jumper and foam
sheets)
16 Dual Electrode Jumper (use is optional) (packaged with the electrode gaskets)
17 PTFE Inlet Tubing, 0.25-mm i.d. (not shown; packaged with detector accessories) (not used with cell preheater)
18 20-
µ
L Loop (not provided with detector purchases, BAS 480 ONLY)
19 PEEK Fingertight Nut (cell outlet)
20 Valve to column inlet tube (already prepared with correct end fittings, not provided with detector purchases,
BAS 480 ONLY)
21 PEEK Fingertight Nut for column to cell inlet tubing
22 Inlet Tubing, Stainless Steel (for preheater) or Teflon (without preheater, #17)
23 Analytical Column, 100
×
3.0 mm, 3
µ
m ODS (BAS P/N MF-8954) (not provided if only detector is purchased)
24 Column End Fittings (not provided with detector purchases, BAS 480 ONLY)
25 Connecting Tube from PM-80 Pump to Injection Valve (when installed)
26 PTFE Outlet Tubing (0.5-mm i.d.) (note the small piece of larger tubing located midway on the tube, used to secure the
tubing in a notch on the right side of the cell compartment; unless the tubing is secured in the notch,
it may be pinched closed when top is lowered; see #30)
27 Notch in cabinet for tubing connection from pump
28 Notch in cabinet to allow use of longer columns (e.g., conventional 25 cm columns) which will extend outside the CC-5
cabinet
29 Notch in cabinet for cell outlet tube (be sure to press the portion of tube with a thicker, Tygon sheath into this slot)
30 Output cable to chart recorder
31 Optional ground connector
Section 3. Installation
6
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