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P-OQ0612-5291-E03 

3/7 

Operational 

Q u alification  (O Q

 

 

 

Automatic Polarimeter 

AP-300 

also offers heat-sensitive roll paper for long-term storage with limited fading. Contact 

ATAGO for details.   

 

 

6. Measurement 

 

1)

 

Make sure that the sample chamber is empty. Close the sample chamber cover. 

2)

 

Press the ZERO key. Zero-setting is initiated. 

3)

 

ZERO SET END is displayed. 

When a printer is connected, “ZERO SET END” will be printed.   

4)

 

Measure the  standard quartz control plate  and record the measured value on the 

measurement data recording chart.    (If a quartz control plate is not available measure a 

standard sucrose solution of 100 °Z and record the measured value on the measurement 

data recording chart.) 

5)

 

Repeat  step  4) a total of  four times. Record the measured values in  the measurement 

data recording chart. 

 

 

  7. Confirmation of Recorded Data 

 

    Check the measurement data of the Automatic Polarimeter AP-300. 

1)

 

Compare  the measurement values  recorded  in  the measurement data recording  chart 

with those printed by the printer. Check if they are consistent. 

2)

 

The AP-300 stores the measurement value of the last 30 measurements in the memory. If 

the  number of measurements exceeds 30, the newest measurement values will replace 

the oldest measurement values. 

3)

 

The measurement values stored in the memory can be recalled on the screen to compare 

with those in the measurement data recording chart. 

4)

 

The measurement values stored in the memory can also be exported and printed. 

 

The measurement values on record and those in the memory can be checked for consistency 

by the method described above. 

 

 

8. Operation Qualification Results Report 

 

1)

 

Fill out the Operation Qualification  test results report  with the measurement data 

obtained. 

2)

 

Calculate the average value and errors, and insert them in the report. 

3)

 

Assess the results, based on the judgment discretionary measurement standard. 

4)

 

Finally,  the  operator  and  an approved supervisor  will  sign the Operation 

Qualification test results report. 

 

 

Function Examination of Automatic Polarimeter AP-300 

 

Preface 

 

The Automatic Polarimeter AP-300 has various functions besides measuring angle of rotation. 

When zero-setting is attempted with a sample outside the range by –5 to +5 °, an error message is 

Содержание AP-300

Страница 1: ...tionary measurement standard Establish a set measurement standard for your samples taking the accuracy of the AP 300 into account Please refer to the product literature and or the instruction manual for the specifications features and measurement accuracy of the AP 300 These specifications are guaranteed at the time the AP 300 is shipped as a brand new product It is difficult to obtain an accuracy...

Страница 2: ...ailable prepare a standard sucrose solution of 100 Z Refer to below in a 200mm observation tube 3 Recording chart for measurement data How to make standard sucrose solution of 100 Z Put 26 000g of pure sucrose in a graduated cylinder and add distilled water to the pure sucrose until the total volume is 100ml 5 Preparation of Instrument 1 Turn on the power of the AP 300 The measurement screen appea...

Страница 3: ...Check if they are consistent 2 The AP 300 stores the measurement value of the last 30 measurements in the memory If the number of measurements exceeds 30 the newest measurement values will replace the oldest measurement values 3 The measurement values stored in the memory can be recalled on the screen to compare with those in the measurement data recording chart 4 The measurement values stored in ...

Страница 4: ...z control plate 34 Part number RE 72044 Quartz control plate 17 Part number RE 72043 Quartz control plate 8 Use a Quartz control plate whose angle is close to the angle of rotation usually measured 2 If a quartz control plate is not available fill a 200mm observation tube with a prepare a standard sucrose solution of 100 Z 3 Function Examination After a performance test in MODE 1 the measurement s...

Страница 5: ...key 5 The display returns to the SET UP MENU screen Press the QUIT key The display returns to the measurement screen 6 Set a standard Quartz control plate or a standard sucrose solution of 100 Z in the sample chamber 7 Close the sample chamber cover Press the START key 8 OUT OF RANGE will be displayed after measurement is completed TEMP ERROR 1 Press the SCALE key in the measurement screen to disp...

Страница 6: ...ress the MENU key in the measurement screen to display SET UP MENU 2 2 Select 7 SYSTEM LEVEL and press the ENTER key The SYSTEM LEVEL screen appears Make sure the SYSTEM LEVEL is 0 Press the QUIT key The screen returns to SET UP MENU 2 2 Press the QUIT key again to return to the measurement screen ...

Страница 7: ...st Average value Difference Judgment standard Accuracy Angle of rotation 0 03 2 Function Examination Functions Contents Switch function Power supply switch Key functions ZERO QUIT MENU SCALE START ENTER Arrow keys NUMERIC keypad Display functions Opening message Date and time Error messages ZERO SET END OUT OF RANGE TEMP ERROR Output functions Printer output RS 232C output check each box 3 Evaluat...

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