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JEROME

J605

Hydrogen Sulfide Analyzer

Operation Manual

PROPRIETARY RIGHTS NOTICE

This manual contains valuable information and material developed by Arizona Instrument LLC

for use with the Jerome

J605 Hydrogen Sulfide Analyzer. No part of this manual can be

reproduced or transmitted in any form or by any means, electronic, mechanical or otherwise. This

includes photocopying and recording or in connection with any information storage or retrieval

system without the express written permission of Arizona Instrument LLC.



Resisorb

is a registered trademark of Avantor Performance Materials.

Tygon

is a registered trademark of Saint-Gobain Performance Plastics Corporation.

Acrodisc

is a registered trademark of Pall Corporation.

Windows

is a registered trademark of Microsoft Corporation in the United States and other

countries.

Содержание JEROME J605

Страница 1: ...05 HYDROGEN SULFIDE ANALYZER June 2013 Firmware v1 2X ARIZONA INSTRUMENT LLC 3375 N Delaware Street Chandler AZ 85225 USA 800 528 7411 602 470 1414 f 602 281 1745 www azic com Email General azi azic com International intl azic com Customer Service support azic com ...

Страница 2: ... electronic mechanical or otherwise This includes photocopying and recording or in connection with any information storage or retrieval system without the express written permission of Arizona Instrument LLC ALL RIGHTS RESERVED Copyright 2010 2013 Arizona Instrument LLC Resisorb is a registered trademark of Avantor Performance Materials Tygon is a registered trademark of Saint Gobain Performance P...

Страница 3: ...30 4 20mA Output 30 6 MAINTENANCE 32 Preventive Maintenance Calendar 32 Flow System 33 25 inch Fritware Filter 33 Internal Filters 34 Replacing the Battery Pack 35 7 CALIBRATION 36 Factory Calibration Service 36 Verification of Functionality and Quality Control 36 8 J605 TROUBLESHOOTING 37 Potential Interferences 39 9 ACCESSORIES MAINTENANCE PARTS 40 Spare Parts Accessories 42 10 APPENDIX A USB HY...

Страница 4: ...pments are available from AZI Pack the Jerome instrument only in a Jerome shipping container AZI WILL NOT BE RESPONSIBLE FOR SHIPPING DAMAGE IF YOU RETURN THE INSTRUMENT IMPROPERLY PACKAGED OR SHIPPED YOU SHOULD INSURE IT FOR FULL VALUE Check for any damage and confirm receipt of all parts on your packing list Contact Arizona Instrument Customer Service at 800 528 7411 or 602 470 1414 if you have ...

Страница 5: ...the end of the handle of the J605 to start a sampling cycle When the instrument measures hydrogen sulfide the 0 000 ppm or 0 00 ppb display will be replaced with a value To ensure the input to the instrument contains no hydrogen sulfide or mercaptans install a Zero Air Filter AZI P N Z2600 3905 in the intake of the instrument The Zero Air Filter cleans the air sample and should produce sample read...

Страница 6: ...zic com for assistance J605 Features Accurate analysis of hydrogen sulfide concentrations in seconds 3 inch 9 cm backlit display showing everything you need to be confident in the instrument including 5 8 inch 1 6 cm tall character readout battery charge indicator and sensor saturation percentage Microprocessor ensures a linear response throughout the entire range of the sensor Inherently stable g...

Страница 7: ...itoring Waste water treatment facilities Quality control Scrubber efficiency testing Accuracy check for other hydrogen sulfide monitors and control systems Hydrogen sulfide source detection Leak detection Portable hydrogen sulfide detection The Jerome J605 is operated from the internal 12V battery For charging the battery an external AC power supply charger is included ...

Страница 8: ...ting fuse Internal battery pack Rechargeable nickel metal hydride NiMH Operating environment 0 C to 40 C non condensing non explosive Case construction Aluminum powder coated Dimensions 11 in L x 6 in W x 6 5 in H 28 cm L x 16 cm W x 17 cm H Weight 5 4 pounds 2 5 kilograms Digital meter display 3 inch 9 cm backlit liquid crystal display LCD Data storage capacity 20 000 samples Output Digital USB s...

Страница 9: ...the SAMPLE button is pressed an internal pump pulls ambient air over the gold film sensor for a precise period of time The gold film sensor adsorbs the hydrogen sulfide and the instrument determines the amount adsorbed and displays the measured concentration of hydrogen sulfide in parts per million ppm or parts per billion ppb depending on the Range in use During normal sampling in Range 1 or 2 th...

Страница 10: ...ilm With use the sensor becomes saturated and needs to be cleaned This is accomplished by a manually activated 45 minute sensor regeneration cycle which removes the hydrogen sulfide from the sensor The bypass solenoid closes during the sensor regeneration cycle causing the air to pass through the scrubber filter providing clean air for the regeneration process The closed loop film heat cycle ensur...

Страница 11: ...t will equalize temperatures faster to allow accurate analysis to begin sooner For maximum accuracy wait 15 seconds between samples to allow the sensor to restabilize The Zero Air Filter can also be used to identify contamination within the instrument If the readings do not reduce to near 0 000 ppm with the filter installed contamination should be suspected If the readings do drop to near 0 000 pp...

Страница 12: ...ta on page 29 If the USB icon is not present this option is not activated Contact your AZI Sales Representative for details on the USB option RANGE Indicates in which Range the J605 is set to sample 0 1 2 or A Auto range as set in the SAMPLE menu See Range in SAMPLE menu on page 15 AUTO SAMPLING INDICATOR Indicates if the J605 is set to sample automatically at regular intervals as set in Sample Mo...

Страница 13: ... USB TYPE A PORTS The USB Type A ports are used to connect a USB printer or USB memory drive for printing or saving sample data or to connect a USB keyboard for menu navigation or data entry The two ports are identical and either can be used For more information see DATA menu on page 18 USB TYPE B PORT The USB Type B port is used to connect the J605 directly to the USB port of a computer using the...

Страница 14: ... 800 528 7411 or 602 470 1414 Page 14 of 57 J605 User Interface Main Menu Structure NOTE The main menu also contains a selection labeled Factory This option is for AZI factory use only and is not accessible by the end user ...

Страница 15: ...ge prior to sampling 0 1 or 2 If the expected H2S concentration is not known Auto ranging can be used instead and the J605 will test each sample in each range before displaying the concentration Using Auto ranging results in longer test times however accuracy is not affected The selected range also determines what units the J605 will use to display the results The three ranges and their default di...

Страница 16: ...midnight or noon 12 00 2 00 4 00 6 00 8 00 10 00 etc SET LOCATION NAME Up to 80 unique location presets are available using the J605 This feature is useful if sampling is done in multiple locations and there is a need to record which readings came from which locations Use the and arrows to scroll through the list of 80 presets until the location to be edited is highlighted Press ENTER START to beg...

Страница 17: ...ger or the external battery pack must be plugged into the back of the instrument before a regeneration can be performed The following options are available from the REGEN menu REGEN NOW Connect external power to the instrument before performing a regeneration Highlighting REGEN NOW and pressing ENTER START will immediately start the sensor regeneration process Do not disconnect external power duri...

Страница 18: ...enty thousand 20 000 data points On instruments that have the USB Communications option in addition to viewing the sample data on the instrument data can be retrieved from the instrument in one of three ways 1 SEND TO PC 2 SAVE TO USB MEMORY DRIVE 3 PRINT DIRECTLY TO AN AZI APPROVED PRINTER AZI P N Y990 0098 The presence of the USB icon on the main screen indicates that the Communications option h...

Страница 19: ...t PC has been configured connect the included USB A to B cable AZI P N 200 0165 between the USB TYPE B PORT on the back panel of the J605 and the USB PORT of the target computer and launch HyperTerminal On the J605 with SEND TO PC highlighted press ENTER START and all of the stored data on the J605 will be transmitted to the target computer as a comma delimited text file See Retrieving Data on pag...

Страница 20: ...se the A and B buttons to switch between the high and low alarm settings by pressing A to select the high alarm or B to select the low alarm Once the alarm level has been set press ENTER START to select the highlighted alarm level as the current alarm level to be used Upon returning to the SET ALARM LEVELS screen there will be asterisk next to the currently selected alarm level either high or low ...

Страница 21: ... blank instead of indicating pass or fail After viewing each result press any key except I O or ESC to move to the next diagnostic check I O should not be used during the diagnostics because I O will power off the instrument and ESC should only be used when specifically indicated by the instrument When testing the keypad follow the on screen prompts to press each of the keys in turn The J605 will ...

Страница 22: ...p before beginning the next step Perform sensor regeneration Refer to Sensor Regeneration on page 23 for the procedure Ensure the instrument has been powered on for at least five 5 minutes prior to sampling Use the Zero Air Filter to equilibrate the instrument to ambient air temperature Install the Zero Air Filter in the instrument s intake Sample repeatedly every 15 seconds until the readings sta...

Страница 23: ... RIGHT arrow button to select Regen from the menu Press the ENTER START button on the keypad to select Regen Now from the Regen menu The instrument will begin a 45 minute regeneration cycle indicated by Regeneration in Progress on the display Do not interrupt this cycle If any error message appears on the display see the J605 TROUBLESHOOTING section beginning on page 37 The LCD screen displays Reg...

Страница 24: ...emains displayed until the next sample is taken The digital meter automatically re zeroes at the start of each sample When the sensor is completely saturated the digital meter displays Sensor Regeneration Required when sampling is attempted No further operation is possible until a sensor regeneration is performed Refer to the Sensor Regeneration procedure on page 23 Press the I O button to turn th...

Страница 25: ... Screen press to enter the Main Menu From the Main Menu select the Sample menu Scroll through the Sample menu to Survey Mode Press ENTER START to select Survey Mode and begin sampling The instrument performs a 4 second purge of the flow system and then begins survey mode sampling The display updates the measured concentrations at the end of each sample cycle NOTE Approximately 100 samples at 0 5 p...

Страница 26: ...ty minutes If the J605 is reading low levels of hydrogen sulfide in Survey or Auto Sampling mode it will continue to sample until the battery runs out However if the J605 is reading high levels of hydrogen sulfide in Survey mode when the sensor reaches saturation a message will appear indicating that sensor regeneration is required and twenty minutes later the instrument will automatically power o...

Страница 27: ...ctions After charging disconnect the battery before returning the instrument to storage Again the time and date will need to be reset if the battery is reconnected so the instrument can be put into service Sample data is stored in non volatile memory and will not be lost or affected when the battery is disconnected or replaced External Battery Power An optional external battery pack AZI P N 990 02...

Страница 28: ...not recharge the J605 s internal battery pack In order to use the external battery pack or the car accessory cable the J605 s internal battery pack must be installed in the instrument If the internal battery pack is disconnected or removed neither of these accessories will be able to provide power to the instrument To order either of these accessories or for additional information call AZI Custome...

Страница 29: ...like this example Jerome Model J605 0001 Serial Number 605 00019 Date 01 OCT 2010 11 03 22 Gas H2S dd MMM yyyy hh mm ss Reading Units Temp C Type Location 01 OCT 2010 09 07 05 4 65 ppb 26 12 S LAB 01 OCT 2010 09 07 32 4 68 ppb 26 12 S LAB 01 OCT 2010 09 07 59 4 79 ppb 26 12 S LAB 01 OCT 2010 09 18 30 5 37 ppb 27 87 M LAB 01 OCT 2010 09 20 12 5 31 ppb 28 06 M LAB 01 OCT 2010 09 28 42 5 26 ppb 27 93...

Страница 30: ...r higher Current levels between 4 and 20 mA correspond to H2S readings between 3 ppb and 10 ppm on a proportional scale as determined by this equation 2 current in mA 4 x10 H S Concentration Detected ppm 16 When the J605 is powered off either manually or automatically the output current will drop to 3 5mA to indicate this condition However if the J605 is operating with the internal battery disconn...

Страница 31: ... example the 5 522mA current level displayed above would correspond to an H2S concentration of 951 ppm After configuring your system the J605 Diagnostics feature can be used to test your setup When the 4 20mA test portion of the diagnostics is reached the instrument will output current levels of 4 8 12 16 and 20mA and the current level displayed on the J605 should match the readout of your 4 20mA ...

Страница 32: ... needed Page 33 Change internal filters and tubing1 After 6 months of use or as needed Page 34 Replace Zero Air Filter1 Annually N A Factory calibration Annually Page 36 Functional check Monthly or as needed Appendix B Page 55 Replace battery Annually or as needed The battery pack contains NiMH batteries Please dispose of properly Page 35 FUSE The J605 utilizes an auto resetting fuse that does not...

Страница 33: ...lace the 25 inch fritware filter once each week or as needed In dusty environments the fritware filter may need to be replaced as often as once a day Replacement 25 inch fritware filters are available from AZI Consumable Sales at 800 528 7411 or 602 470 1414 Remove the two 2 side screws from the intake end of the instrument and open the case Gently pull the inner portion of the intake out of the i...

Страница 34: ...l AZI Customer Service at 800 528 7411 602 470 1414 or e mail support azic com for a copy of the Resisorb MSDS or for other questions Replace the old filters with new filters oriented as shown in the diagram above Push the Tygon tubing as far as it will go onto the filter fittings Push the filters into the mounting clips Remove any crimps or twists in the tubing and ensure that tubing connections ...

Страница 35: ...Disconnect the battery connector to detach the old battery Install the new battery by connecting it to the battery connector and sliding it into the J605 Tuck the cabling into the gap between the battery and the case Replace the battery panel and secure with the four 4 screws removed above Dispose of the old nickel metal hydride NiMH battery in accordance with state and federal regulations After b...

Страница 36: ...ing authorization call AZI Customer Service at 800 528 7411 or 602 470 1414 or visit our website at www azic com Verification of Functionality and Quality Control The Functional Test Module AZI P N Z2600 0918 or Z2600 0930 is used to determine if your instrument is functioning correctly between recommended annual factory calibrations It allows you to have complete confidence in the sample results ...

Страница 37: ...and crimps in the Tygon tubing Obstructed intake or exhaust Clogged intake filter Periodically check the Tygon tubing in the instrument Refer to page 34 Verify ports are not obstructed Change intake fritware filter Refer to page 33 High erratic results Internal hydrogen sulfide contamination 1 Install the Zero Air Filter in the intake Press the SAMPLE button After three samples at 15 sec intervals...

Страница 38: ...supply charger to instrument Memory Failure Call AZI Customer Service at 800 528 7411 or 602 470 1414 Sensor Failure Sensor A D Failure Call AZI Customer Service at 800 528 7411 or 602 470 1414 Data Memory Full Data memory full Save and then delete data See Retrieving Data on page 29 Incomplete Regen Check battery AC power supply External power was interrupted before regeneration could complete Re...

Страница 39: ...at water vapor condensation on the gold film can cause irreparable harm to the sensor and must be avoided However the following compounds may cause the gold film sensor to respond Chlorine Ammonia NO2 Most mercaptans organic sulfur compounds or thiols Special filters designed to remove chlorine or ammonia gas are available from Arizona Instrument and may be ordered as Chlorine Filter AZI P N Z2600...

Страница 40: ...Communications Package Instruments See pictures beginning on page 42 1400 2002 Probe 1400 3010 Tubing Adapter 1 4 to 1 8 2600 3039 Filter Fritware 0 25 1 pack of 20 fritware filters Z2600 3905 Filter Zero Air Filter 4000 1025 AC power supply charger 6000 4003 Line Cord 115 VAC USA and Canada alternate 200 0003 Line Cord 220 240 VAC England alternate 200 0008 Line Cord 220 240 VAC Europe Z2600 0918...

Страница 41: ...905 Filter Zero Air Filter 600 0279 Filter LFS Scrubber Filter Z2600 3930 Filter Scrubber Filter 600 0281 Filter LFD Scrubber Filter 2600 3061 Filter Acrodisc Filter 25mm 990 0217 Hard Side Carry Case Includes a molded case with die cut foam rubber inserts to hold the Jerome J605 and accessories 990 0220 Soft Side Carry Case Includes a shoulder strap for easy carrying a clear plastic window over t...

Страница 42: ...stomer Service 800 528 7411 or 602 470 1414 Page 42 of 57 Spare Parts Accessories 4000 1025 AC Power Supply Charger 200 0143 Battery Pack Assembly 200 0170 Car Accessory Cable 990 0225 10 to 1 Dilution Module ...

Страница 43: ...y Pack 2600 3061 Filter Acrodisc Filter 990 0183 Filter Ammonia Filter Z2600 3940 Filter Chlorine Filter 2600 3039 Filter Fritware 25 inch pack of 20 600 0281 Filter LFD Scrubber Filter 600 0279 Filter LFS Scrubber Filter Z2600 3930 Filter Scrubber filter Z2600 3905 Filter Zero Air Filter ...

Страница 44: ...VAC Line Cord Europe 1400 2002 Probe 1300 0031 Reducer 1 8 x 3 16 1400 3010 Tubing adapter 345 0050 Tygon tubing 1 8 I D 1 foot 2500 3002 Tygon tubing 1 16 I D 1 foot 200 0165 USB Communication Cable Type A to Type B 990 0230 USB Keyboard For current prices and delivery information call AZI Customer Service at 800 528 7411 or 602 470 1414 ...

Страница 45: ...file from the Support tab at http www azic com and save it to your desktop If you received these instructions and the driver in an email save the attached file AZI_USB_Driver zip to your desktop Once the driver file AZI_USB_Driver zip is on your desktop 1 Launch the AZI Driver Installer wizard Double click the file to open it Drag the Driver Install directory from the zip file to the desktop Doubl...

Страница 46: ...ay one or more messages indicating that the driver has not passed Windows Logo Testing This driver being installed is a generic Communications Port driver that is part of Windows usbser sys so it is safe to ignore this warning Click Continue Anyway to install the driver 4 Click Finish ...

Страница 47: ...and automatically start the New Hardware wizard The following pictures and descriptions correspond to a Windows XP installation If using Windows Vista or Windows 7 this process is abbreviated and requires minimal user interaction Watch for the two info balloons to appear and then proceed to page 50 6 If the following dialog box appears DO NOT connect to Windows Update to get the driver Select No n...

Страница 48: ...tically and click Next 8 Windows may display a message indicating that the driver has not passed Windows Logo Testing This driver being installed is a generic Communications Port driver that is part of Windows usbser sys so it is safe to ignore this warning Click Continue Anyway to install the driver ...

Страница 49: ...ZI Customer Service 800 528 7411 or 602 470 1414 Page 49 of 57 9 Windows will copy a file and finish the wizard Click Finish 10 Windows will then indicate that the driver has been successfully installed ...

Страница 50: ...art All Programs Accessories Communications HyperTerminal If prompted to make HyperTerminal the default telnet application click No 3 When prompted for a name for this connection enter J605 and click OK The pictures that follow are from setup for a J405 However the installation and usage are exactly the same whether using a J605 or a J405 4 If HyperTerminal has not been run previously on the targe...

Страница 51: ...will be displayed Find the last dropdown list in the dialog box labeled Connect using Select the last COM port from the list and click OK 6 Next HyperTerminal will prompt for Port Settings These settings do not apply to USB ports so the default values do not need to be changed Continue by clicking OK ...

Страница 52: ...411 or 602 470 1414 Page 52 of 57 7 A blank HyperTerminal screen will be displayed On the status bar in the lower left hand corner it should say Connected 8 Select Capture Text from the Transfer menu on the main HyperTerminal window ...

Страница 53: ...data to It is recommended that the data be saved to either the Desktop or My Documents 10 Go to the J605 and navigate to the DATA menu then highlight Send to PC and press ENTER START 11 You should see your data scrolling in the HyperTerminal window If you do not see anything in the HyperTerminal window go to step 13 ...

Страница 54: ...le menu click Properties c You will see the same window as in step 4 above Try selecting a different COM port and continue from step 4 Keep trying each COM port in the list If you have tried all of them and still cannot receive data from the J605 try re installing the USB driver If that does not solve the problem call AZI Customer Service at 800 528 7411 or 602 470 1414 or email support azic com S...

Страница 55: ...the J605 The H2S flows over the gold film sensor of the Jerome analyzer which then measures the concentration of the gas The flow rate and temperature of the H2S release are factory set to provide a concentration of approximately 0 250 ppm 250 ppb 20 Z2600 0918 or 0 030 ppm 30 ppb 20 Z2600 0930 The user then compares the reading on the Jerome analyzer with the known concentration from the module I...

Страница 56: ...uct has been subjected to environmental or stress testing by buyer or any third party without written approval of seller prior to such testing Further no warranty shall be enforceable if the alleged defect is found to have occurred because of misuse neglect improper installation repair alteration accident or improper return handling procedure by buyer Discontinued product is warranted only for a c...

Страница 57: ...in Performance Plastics Corporation Acrodisc is a registered trademark of Pall Corporation Windows is a registered trademark of Microsoft Corporation in the United States and other countries Arizona Instrument LLC Jerome J605 Hydrogen Sulfide Analyzer Operation Manual Part Number 700 0108 E June 2013 If you have any questions regarding the operation of this instrument please call our toll free num...

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