YSI MultiLab 4010-1W Operating Manual Download

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Contents

MultiLab 4010-1W

ba76141e07

08/2018

4.4.5

Example 2 on navigation: Setting the date and time . . . . . . . . . . . . . . . . . . . . . . . . . 24

pH value. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

5.1

Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

5.1.1

Measuring the pH value . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

5.1.2

Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

5.2

pH calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

5.2.1

Why calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

5.2.2

When do you have to calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

5.2.3

Calibration procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

5.2.4

Carrying out automatic calibration (AutoCal)

. . . . . . . . . . . . . . . . . . . . . . . . . . 28

5.2.5

Carrying out manual calibration (ConCal) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

5.2.6

Calibration points . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

5.2.7

Calibration data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

5.2.8

Continuous measurement control (CMC function)

. . . . . . . . . . . . . . . . . . . . . . . . 37

5.2.9

QSC function (sensor quality control)

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

ORP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

6.1

Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

6.1.1

Measuring the ORP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

6.1.2

Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42

6.2

ORP calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

Dissolved oxygen . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

7.1

Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

7.1.1

Measuring D.O. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

7.1.2

Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

7.2

FDO Check (checking the FDO 4410) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

7.2.1

Why should you check the sensor? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

7.2.2

When should you check the sensor? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

7.2.3

Perform a FDO Check . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

7.2.4

Evaluation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48

7.3

Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

7.3.1

Why calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

7.3.2

When to calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

7.3.3

Calibration procedures. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

7.3.4

Calibration in water vapor-saturated air . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

7.3.5

Calibrating with

Comparison meas.

(e.g. Winkler titration) . . . . . . . . . . . . . . . . . . . . 50

7.3.6

Zero calibration

. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

7.3.7

Calibration data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Conductivity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

8.1

Measuring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

8.1.1

Measuring the conductivity . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

8.1.2

Measuring the temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57

8.2

Temperature compensation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57

8.3

Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

8.3.1

Why calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

8.3.2

When to calibrate? . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

8.3.3

Calibration procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

8.3.4

Determining the cell constant (calibration in the check- and calibration standard) . . 58

Summary of Contents for MultiLab 4010-1W

Page 1: ...OPERATING MANUAL ba76141e07 08 2018 MultiLab 4010 P 1 W DIGITAL METER FOR WIRELESS IDS SENSORS 4010P 1W 4010 1W 4010 1W 4010P 1W IDS WA IDS WA ...

Page 2: ... 4010 1W Contact YSI 1725 Brannum Lane Yellow Springs OH 45387 USA Tel 1 937 767 7241 800 765 4974 Email info ysi com Internet www ysi com Copyright 2018 Xylem Inc For the most recent version of the manual please visit www ysi com ...

Page 3: ...e operation 12 2 2 1 Authorized use 12 2 2 2 Requirements for safe operation 12 2 2 3 Unauthorized use 12 3 Commissioning 13 3 1 Scope of delivery 13 3 2 Power supply 13 3 3 Initial commissioning 13 3 3 1 Inserting the batteries 14 3 3 2 Connecting the power pack 15 3 3 3 Mounting the stand 15 4 Operation 16 4 1 General operating principles 16 4 1 1 Keypad 16 4 1 2 Display 17 4 1 3 Status informat...

Page 4: ...bration 43 7 Dissolved oxygen 44 7 1 Measuring 44 7 1 1 Measuring D O 44 7 1 2 Measuring the temperature 46 7 2 FDO Check checking the FDO 4410 47 7 2 1 Why should you check the sensor 47 7 2 2 When should you check the sensor 47 7 2 3 Perform a FDO Check 47 7 2 4 Evaluation 48 7 3 Calibration 49 7 3 1 Why calibrate 49 7 3 2 When to calibrate 49 7 3 3 Calibration procedures 49 7 3 4 Calibration in...

Page 5: ...ent settings 73 9 5 1 System 73 9 5 2 Data storage 74 9 5 3 Automatic Stability control 74 9 5 4 Automatic switch off function 74 9 5 5 Display illumination 75 9 6 Reset 75 9 6 1 Resetting the measurement settings 75 9 6 2 Resetting the system settings 77 10 Data storage 78 10 1 Manual data storage 78 10 2 Automatic data storage at intervals 79 10 3 Measurement data storage 81 10 3 1 Managing the ...

Page 6: ...14 3 Conductivity 94 14 4 General topics 95 15 Technical data 96 15 1 Measuring ranges resolution accuracy 96 15 2 General data 96 16 Firmware update 98 16 1 Firmware update for the meter MultiLab 4010 1W 98 16 2 Firmware Update for IDS Sensors 99 17 Glossary 100 18 Index 103 19 Appendix 106 19 1 Oxygen solubility table 106 19 2 DO Calibration values 108 19 3 Calculate the TDS Multiplier 109 20 Co...

Page 7: ...easurements quickly and reliably The MultiLab 4010 1W provides the maximum degree of operating comfort reliability and measuring certainty for all applications The MultiLab 4010 1W supports you in your work with the following functions Automatic sensor recognition CMC continuous measurement control QSC sensor quality control Electronic access control Data transmission via the USB interface USB B 1...

Page 8: ... sensors 1 3 1 IDS sensors IDS sensors support the automatic sensor recognition show only the settings relevant to the specific sensor in the setting menu process signals in the sensor digitally so that precise and interference free measurements are enabled even with long cables facilitate to assign a sensor to a measured parameter with differently colored couplings The information concerning the ...

Page 9: ...replace the sensor cable with an energy saving Bluetooth LE radio connection 1 3 3 Automatic sensor recognition The automatic sensor recognition for IDS sensors allows to operate an IDS sensor with different meters without recalibrating to assign measurement data to an IDS sensor Measurement datasets are always stored and output with the sensor name and sensor serial number to assign calibration d...

Page 10: ...matic sensor recognition a meter that supports the automatic sensor recognition e g MultiLab 4010 1W and a digital IDS sensor are required In digital IDS sensors sensor data are stored that clearly identify the sensor The sensor data are automatically taken over by the meter ...

Page 11: ...oods might be damaged if the actions mentioned are not taken 2 1 2 Safety signs on the meter Note all labels information signs and safety symbols on the meter and in the battery compartment A warning symbol triangle without text refers to safety information in this operating manual 2 1 3 Further documents providing safety information The following documents provide additional information which you...

Page 12: ...peration Note the following points for safe operation The meter may only be operated according to the authorized use specified above The meter may only be supplied with power by the energy sources mentioned in this operating manual The meter may only be operated under the environmental conditions mentioned in this operating manual The meter may only be opened if this is explicitly described in thi...

Page 13: ...iLab 4010 1W is supplied with power in the following ways Line power operation via the supplied power pack A sensor with stirrer can only be operated with line power Battery operation 4 batteries 1 5 V Mignon type AA USB operation via a connected USB B cable 3 3 Initial commissioning Perform the following activities Insert the supplied batteries For mains operation Connect the power pack If necess...

Page 14: ...ed 1 Open the battery compartment 1 on the underside of the meter 1 Battery compartment CAUTION Make sure that the poles of the batteries are positioned cor rectly The signs on the batteries must correspond to the signs in the battery compartment 2 Place four batteries type Mignon AA in the battery compartment 3 Close the battery compartment 1 4 Set the date and time see section 4 4 5 EXAMPLE 2 ON...

Page 15: ...line voltage at the operating site must lie within the input voltage range of the original power pack see section 15 2 GENERAL DATA page 96 CAUTION Use original power packs only see section 15 2 GENERAL DATA page 96 1 Connect the plug of the power pack to the socket for the power pack on the MultiLab 4010 1W 2 Connect the original power pack to an easily accessible power outlet 1 2 ...

Page 16: ...information on a sensor On Off Switches the meter on or off M Selects the measured parameter Quits the settings CAL CAL__ Calls up the calibration procedure Displays the calibration data STO STO_ Saves a measured value manually Opens the menu for the automatic save function RCL RCL__ Displays the manually stored measured values Displays the automatically stored measured values __ __ Menu control n...

Page 17: ... Sensor symbol calibration evaluation calibration interval 6 Measured temperature with unit 7 Status information meter 8 Softkeys and date time AR Stability control AutoRead is active HOLD Measured value is frozen AR key ZeroCal The zero point is calibrated Batteries are almost empty Data are automatically output to the USB B interface at intervals 3 2 1 4 5 6 8 HOLD AR 7 AutoCal TEC i 03 04 2013 ...

Page 18: ... ORP conductivity D O 2 USB B device interface 3 Stirrer interface for BOD sensor 4 Power pack 5 Service interface CAUTION Only connect sensors to the meter that cannot return any volt ages or currents that are not allowed SELV and current circuit with current limiting YSI IDS sensors and IDS adapters meet these requirements 1 In the measured value display Display the sensor data sensor name serie...

Page 19: ...The meter performs a self test 2 Connect the sensor The meter is ready to measure 1 Switch the meter off with On Off 25 0 7 007 pH C 0 14 More 4110 B09250001 pH resolution 0 001 mV resolution 0 1 Buffer YSI Calibration interval 7d Unit for slope mV pH QSC off Software version V 1 00 4110 B092500013 03 04 2013 08 00 Back 25 0 7 007 pH C 0 14 01 02 2014 08 00 i USB output ...

Page 20: ...nts The selection is done with the keys The current selection is dis played with a frame Submenus The name of the submenu is displayed at the upper edge of the frame Sub menus are opened by confirming with ENTER Example Operating mode Explanation Measuring The measurement data of the connected sensor are shown in the measured value display Calibration The course of a calibration with calibration i...

Page 21: ...ming with ENTER Example Display the Calibration record function Messages Information is marked by the i symbol It cannot be selected Example General Interface Clock function Service information Reset System 03 04 2013 08 00 Back Language Deutsch Audio signal off Illumination on Contrast 12 Shutoff time 1 h Temperature unit C Stability control on General 03 04 2013 08 00 Back Calibration record Cal...

Page 22: ...The instrument is in the setting mode 3 Select the System submenu with The current selection is displayed with a frame 4 Open the System submenu with ENTER Calibration record Calibration data storage Buffer YSI Single point calibration yes Calibration interval 7 d Unit for slope mV pH i 4 00 7 00 10 00 25 C pH 03 04 2013 08 00 Back 25 0 7 007 pH C 0 14 01 02 2014 08 00 i USB output System Data sto...

Page 23: ...tting with ENTER The meter switches to the measuring mode The selected language is active General Interface Clock function Service information Reset System 03 04 2013 08 00 Back Language Deutsch Audio signal off Illumination on Contrast 50 Shutoff time 1 h Temperature unit C Stability control on General 03 04 2013 08 00 Back Language Deutsch Audio signal off Illumination on Contrast 50 Shutoff tim...

Page 24: ...te time and date format The date format can be switched from the display of day month year dd mm yy to the display of month day year mm dd yy or mm dd yy The date and time are reset to default after a fall of the supply volt age empty batteries 1 In the measured value display Open the Storage config menu with ENTER__ The instrument is in the setting mode 2 Select and confirm the System Clock funct...

Page 25: ...with and ENTER The time is set 7 If necessary set the Date and Date format The setting is made similarly to that of the time 8 To make further settings switch to the next higher menu level with F1 or Switch to the measured value display with M The instrument is in the measuring mode ...

Page 26: ...ty control is switched off You can start the Stability control manually at any time irrespective of the set ting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CON TROL page 74 in the System menu To start the Stability control function manually the HOLD function must be enabled Hold function 1 Connect the IDS pH sensor to the meter The pH measuring window is displayed 2 If n...

Page 27: ... and the display of the mea sured parameter flashes The HOLD AR status indicator appears as soon as a stable measured value is recognized The progress bar disappears the display of the mea sured parameter stops flashing and there is a beep The current measurement data is output to the interface Measurement data meeting the stability control criterion is marked by AR You can prematurely terminate t...

Page 28: ...meter see section 9 1 2 BUFFER SETS FOR CALIBRATION page 64 Manual calibration ConCal Any buffer solutions can be used The nominal values of the buffer solutions are manually entered by the user during the calibration procedure 5 2 4 Carrying out automatic calibration AutoCal Make sure that in the menu for measurement and calibration settings in the menu pH ENTER Calibration Buffer the correct buf...

Page 29: ...ol The AR status indicator is displayed The measured parameter flashes 7 Wait for the end of the measurement with stability control beep HOLD AR status indicator or take over the calibrated value with ENTER The calibration display for the next buffer appears voltage display 8 If necessary finish the calibration procedure as a single point calibra tion with M The calibration record is displayed For...

Page 30: ...ol beep HOLD AR status indicator or take over the calibrated value with ENTER The calibration display for the next buffer appears voltage display 13 If necessary finish the calibration procedure as a two point calibration with M The calibration record is displayed pH 0 0 24 8 C AutoCal YSI 7 000 01 07 2011 08 00 AR Buffer mV 14 Thoroughly rinse the sensor with deionized water 15 Immerse the sensor...

Page 31: ... set has been measured Then the calibration record is dis played The calibration line is determined by linear regression If single point calibration was set in the menu the calibration proce dure is automatically finished with the measurement of buffer solu tion 1 and the calibration record is displayed 1 Connect the pH sensor to the meter The pH measuring window is displayed 2 Keep the buffer sol...

Page 32: ...e display 10 If necessary finish the calibration procedure as a single point calibration with M The calibration record is displayed For single point calibration the instrument uses the Nernst slope 59 2 mV pH at 25 C and determines the zero point of the IDS pH sensor pH 0 0 24 8 C ConCal 7 000 01 07 2011 08 00 Buffer mV AR pH 7 000 24 8 C ConCal 1 01 07 2011 08 00 Buffer 11 Thoroughly rinse the se...

Page 33: ... necessary finish the calibration procedure as a two point calibration with M The calibration record is displayed pH 4 035 24 8 C ConCal 2 01 07 2011 08 00 Buffer 18 Thoroughly rinse the sensor with deionized water 19 Immerse the sensor in the next buffer solution 20 Start the measurement with ENTER The measured value is checked for stability stability control The AR status indicator is displayed ...

Page 34: ... displayed or Continue calibrating using the next buffer with ENTER After the fifth buffer has been measured the calibration is automat ically finished Then the calibration record is displayed The calibration line is determined by linear regression Calibration Determined values Displayed calibration data 1 point Asymmetry Zero point Asymmetry Slope Nernst slope 59 2 mV pH at 25 C 2 point Asymmetry...

Page 35: ...ken into account The evaluation appears on the display and in the calibration record Menu item Setting function Explanation Calibration Calibration data stor age Display Displays the calibration records Further options Scroll through the calibration records with Output the displayed calibration record to the interface with F2 USB output Output all calibration records to the interface with F2__ USB...

Page 36: ...DS sensors you can optionally enable a more finely graded calibration evaluation QSC see section 5 2 9 QSC FUNCTION SENSOR QUALITY CONTROL page 38 Display Calibration record Zero point mV Slope mV pH 4010 1W Ser no 11292113 CALIBRATIONpH 01 02 2014 15 55 Ser no 10501234 YSI Buffer 1 4 00 Buffer 2 7 00 Buffer 3 10 00 Voltage 1 184 0 mV Voltage 2 3 0 mV Voltage 3 177 0 mV Temperatur 1 24 0 C Tempera...

Page 37: ... value needle 2 Marking lines for all nominal buffer values used with the last valid cali bration 3 Measuring range for which a valid calibration is available Measured values in this range are suitable for documentation 4 Measuring range for which no valid calibration is available shaded Measured values in this range are not suitable for documentation Calibrate the meter with buffers covering this...

Page 38: ...on with special QSC buffer solutions It covers the measuring range of the sensor pH 2 to pH 11 The QSC initial calibration determines the actual condi tion of the sensor and stores it as a reference in the sensor To meet the high requirements of a QSC initial calibration the QSC initial cali bration should optimally be carried out with the initial commissioning of the sensor 1 QSC scale The double...

Page 39: ...ial calibration very carefully It determines the reference value for the sensor This reference value cannot be overwritten or reset As soon as the QSC function was enabled it is not possible to return to the sensor evaluation with the sensor symbol 1 Prepare for calibration the meter sensor and the buffer solutions of the QSC Kit 2 Open the menu for measurement settings with ENTER 3 In the QSC men...

Page 40: ...d the buffer solutions of the QSC Kit 2 Open the menu for measurement settings with ENTER 3 In the QSC menu select Control calibration with The calibration display appears AutoCal QSC Kit is displayed as the buffer Exclusively use the QSC Kit for the QSC calibration If you use other buffers you will have no valid QSC control calibration 4 Start the measurement with ENTER Calibration with the buffe...

Page 41: ...on as the measured value is outside the stability range when the automatic Stability control is switched off You can start the Stability control manually at any time irrespective of the set ting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CON TROL page 74 in the System menu To start the Stability control function manually the HOLD function must be enabled IDS ORP sensors ...

Page 42: ...yed and the display of the mea sured parameter flashes The HOLD AR status indicator appears as soon as a stable measured value is recognized The progress bar disappears the display of the mea sured parameter stops flashing and there is a beep The current measurement data is output to the interface Measurement data meeting the stability control criterion is marked by AR You can prematurely terminat...

Page 43: ...ted temperature sensor is operated the tempera ture value is displayed and recorded together with the measured value 6 2 ORP calibration ORP electrodes are not calibrated You can however check ORP electrodes by measuring the ORP of a test solution and comparing the value with the nominal value ...

Page 44: ... FDO Check instead 7 1 Measuring 7 1 1 Measuring D O Selecting the displayed measured parameter You can switch between the following displays with M D O concentration mg l D O saturation A sensor with stirrer can only be operated while the meter is line powered 1 Connect the IDS D O sensor or a D O sensor with IDS adapter to the meter The D O measuring screen is displayed 2 If necessary select the...

Page 45: ...easurement signal The stability has a considerable impact on the reproduc ibility of measured values The measured parameter flashes on the display as soon as the measured value is outside the stability range when the automatic Stability control is switched off Irrespective of the setting for automatic Stability control see section 9 5 3 AUTOMATIC STABILITY CONTROL page 74 in the System menu you ca...

Page 46: ...atus indicator appears as soon as a stable measured value is recognized The progress bar disappears the display of the mea sured parameter stops flashing and there is a beep The current measurement data is output to the interface Measurement data meeting the stability control criterion is marked by AR You can prematurely terminate the Stability control function manu ally with ENTER at any time If ...

Page 47: ...e sensor cap is contaminated or at the end of its lifetime After the sensor cap was exchanged Routinely within the framework of the company quality assurance 7 2 3 Perform a FDO Check Proceed as follows to carry out the FDO Check 1 Connect the D O sensor to the meter 2 Place the D O sensor in the FDO Check check and storage vessel 3 Close the check and storage vessel FDO Check The sponge in the ch...

Page 48: ...ve D O saturation abbreviated saturation is 100 Therefore the validity scope is 98 102 The check resulted in a measured value of 99 3 The measurement error is within the specified validity scope No cleaning or user calibration is required 5 Start the measurement with ENTER The measured value is checked for stability stability control The AR status indicator is displayed The measured parameter flas...

Page 49: ...r ISO 5813 At the same time the relative slope is adapted to the comparison measurement by a correction multiplier When the correction multiplier is active the Factor indicator appears in the mea suring window 7 3 4 Calibration in water vapor saturated air For this calibration procedure the Comparison meas setting must be set to off in the Calibration menu As the calibration vessel use a BOD bottl...

Page 50: ...D O sensor into the calibration vessel 3 For FDO 4410 with the check and storage vessel FDO Check Close the check and storage vessel FDO Check Leave the sensor in the calibration vessel or check and storage vessel FDO 4410 long enough at least 15 minutes until the air is saturated with water vapor and the sensor has adapted to the ambient temperature 4 Start the calibration with CAL 5 Start the me...

Page 51: ...The AR status indicator is displayed The measured parameter flashes 5 Wait for the measurement with stability control to be finished beep HOLD AR status indicator 6 Using set the measured value to adjust the displayed value to the nominal value value of the comparison measurement Subse quently take over the adjustment with ENTER The meter switches to the measured value display The status display F...

Page 52: ... for this sensor 1 Connect the D O sensor to the meter 2 Place the D O sensor in a solution that does not contain any dissolved oxygen A solution not containing any dissolved oxygen can be prepared by dissolving approx 8 to 10 g sodium sulfite Na2SO3 in 500 ml tap water Carefully mix the solution It may take up to 60 minutes until the solution is free of oxygen 3 In the menu for measurement and ca...

Page 53: ...ue The zero point is calibrated The ZeroCal status indicator is displayed 7 Carry out a calibration see section 7 3 3 CALIBRATION PROCEDURES page 49 The calibration record is automatically transmitted to the interface after calibrating Menu item Setting function Explanation Calibration Calibration data stor age Display Displays the calibration records Further options Scroll through the calibration...

Page 54: ...was determined is compared to the characteristic curve of an ideal sen sor at similar environmental conditions relative slope S S Ssen sor Sideal sensor An ideal sensor has a slope of 1 Display Calibration record Relative slope S 0 94 1 06 S 0 92 0 94 or S 1 06 1 08 S 0 90 0 92 or S 1 08 1 10 Error Error S 0 90 or S 1 10 Error elimination see section 14 WHAT TO DO IF page 92 Display Calibration re...

Page 55: ...just this multiplier to meet your requirements in the range 0 40 1 00 The multiplier is set in the menu for the parameter TDS Stability control AutoRead HOLD function The stability control function AutoRead continually checks the stability of the measurement signal The stability has a considerable impact on the reproduc 1 Connect the conductivity sensor to the meter The conductivity measuring wind...

Page 56: ... Using ENTER activate the Stability control function manually The AR status indicator appears while the measured value is assessed as not stable A progress bar is displayed and the display of the measured parameter flashes The HOLD AR status indicator appears as soon as a stable measured value is recognized The progress bar disappears the display of the mea sured parameter stops flashing and there...

Page 57: ... methods Nonlinear temperature compensation nLF according to EN 27 888 Linear temperature compensation Lin with adjustable coefficient No temperature compensation off Application tips Select the following temperature compensations given in the table according to the respective test sample Measured parameter Time interval Stability in the time interval Conductivity ϰ 10 seconds ϰ better than 1 0 of...

Page 58: ...procedure for IDS conductivity sensors with a cell constant in the range 0 450 0 500 cm 1 Determining the cell constant Calibration with freely selectable check and calibration standard Comprehensive and flexible calibration procedure for all IDS conductivity sensors irrespective of the cell constant Which calibration procedures can be used depends on the conductivity sensor used The menu for meas...

Page 59: ...nt of the IDS sensor e g 4310 0 475 cm 1 For this calibration procedure the Type setting must be set to cal Proceed as follows to determine the cell constant 1 Connect the conductivity sensor to the meter 2 In the measured value display select the conductivity parameter with M 3 Start the calibration with CAL The cell constant that was calibrated last is displayed 4 Immerse the conductivity sensor...

Page 60: ...he cell constant 1 Connect the conductivity sensor to the meter 2 In the measured value display select the conductivity parameter with M 3 Open the menu for measurement settings with ENTER 4 Select the setting of the cell constant 4310 Menu Type man and Cell const man 4320 Menu Cell constant The current conductivity value is displayed in the status line 5 Set the suitable temperature compensation ...

Page 61: ...calibration record is automatically transmitted to the interface after calibrating Menu item Setting function Explanation Calibration Calibration data storage Display Displays the calibration records Further options Scroll through the calibration records with Output the displayed calibration record to the interface with F2 USB output Output all calibration records to the interface with F2__ USB ou...

Page 62: ...Conductivity MultiLab 4010 1W 62 ba76141e07 08 2018 Calibration record USB output CALIBRATION Cond 03 04 2013 07 43 33 4310 Ser no 09250033 Cell constant 0 476 1 cm 25 0 C Sensor ...

Page 63: ...see section 9 1 2 BUFFER SETS FOR CALIBRATION page 64 and section 5 2 PH CALIBRATION page 28 Calibration Single point calibration yes no Quick calibration with 1 buffer Calibration Calibration interval 1 7 999 d Calibration interval for the IDS pH sensor in days The meter reminds you to calibrate regularly by the flashing sensor symbol in the measuring screen Calibration Unit for slope mV pH Unit ...

Page 64: ...ution 0 1 1 Resolution of the mV display Reset Resets all sensor settings to the delivery condition see sec tion 9 6 1 RESETTING THE MEASUREMENT SETTINGS page 75 Menu item Possible setting Explanation No Buffer set pH values at 1 YSI 4 000 7 000 10 000 25 C 2 ConCal Any Any 3 NIST DIN DIN buffers according to DIN 19266 and NIST Traceable Buffers 1 679 4 006 6 865 9 180 12 454 25 C 4 TEC Technical ...

Page 65: ...1 995 4 005 7 002 9 208 25 C 13 Fisher 2 007 4 002 7 004 10 002 25 C 14 Fluka BS 4 006 6 984 8 957 25 C 15 Radiometer 1 678 4 005 7 000 9 180 25 C 16 Baker 4 006 6 991 10 008 25 C 17 Metrohm 3 996 7 003 8 999 25 C 18 Beckman 4 005 7 005 10 013 25 C 19 Hamilton Duracal 4 005 7 002 10 013 25 C 20 Precisa 3 996 7 003 8 999 25 C 21 Reagecon TEC 2 000 4 010 7 000 10 000 25 C No Buffer set pH values at ...

Page 66: ...g the calibra tion interval The calibration interval is set to 7 days in the factory You can change the interval 1 999 days 22 Reagecon 20 2 000 4 000 7 000 10 000 13 000 20 C 23 Reagecon 25 2 000 4 000 7 000 10 000 13 000 25 C 24 Chemsolute 2 000 4 000 7 000 10 000 20 C 25 USABlueBook 4 000 7 000 10 000 25 C The buffers are selected in the menu pH ENTER Calibration Buffer see section 9 1 1 SETTIN...

Page 67: ...asured value display and press the ENTER key After completing the settings switch to the measured value display with M The possible settings are individually displayed for each sensor Below the set ting menu is shown with all settings for all IDS D O sensors Default settings are printed in bold 3 Confirm the setting with ENTER 4 Quit the menu with M Menu item Possible setting Explanation mV resolu...

Page 68: ...fter exchanging the sensor cap For details see section 9 3 2 ENTER SENSOR CAP COEFFICIENTS PROOBOD page 69 Calibration Membrane cap only for 4100 Pro BOD 5010 with 4011 Adapter Black Yellow After exchanging the sensor cap select the cap type here FDO Check Start FDO Check only for FDO 4410 Starts the check with the FDO Check FDO Check Check interval only for FDO 4410 1 60 999 d Interval for the FD...

Page 69: ...or FDO 4410 30 300 s Response time of the signal filter in seconds A signal filter in the sensor reduces the limits of variation of the mea sured value The signal filter is characterized by the response time t90 This is the time after which 90 of a signal change is displayed DO Saturation local on off DO Saturation local is a proce dure that takes the local air pres sure into account for each satu...

Page 70: ...lt settings are printed in bold General setting menu for conductivity Menu item Possible setting Explanation Calibration Calibration record Displays the calibration record of the last calibration Calibration Calibration data stor age Display Displays the last calibration records max 10 Calibration Calibration data stor age Output to RS232 USB Outputs the calibration data stor age to the interface ...

Page 71: ...djustable cell con stant This menu item is only available when Type man is set The current conductivity value is displayed in the status line Temp comp TC Method nLF Lin off Procedure for temperature com pensation see section 8 2 TEM PERATURE COMPENSATION page 57 This setting is only available for the measured parameters con ductivity ϰ and resistivity ρ Temp comp TC Linear coeff 0 000 2 000 3 000...

Page 72: ... see section 8 2 TEM PERATURE COMPENSATION page 57 This setting is only available for the measured parameters conductivity ϰ and resistivity ρ Temp comp TC Linear coeff 0 000 2 000 3 000 K Coefficient of the linear tempera ture compensation This menu item is only available when the linear temperature com pensation is set Temp comp TC Reference temp 20 C 25 C Reference temperature This setting is o...

Page 73: ...ime 10 min 1h 24 h Adjusts the switch off time System General Tem perature unit C F Temperature unit degrees Celsius or degrees Fahrenheit All temperature values are displayed with the selected unit System General Air pressure unit mbar mmHg inHg Air pressure unit System General Stabil ity control on off Switches on or off the automatic stability control during measurement see section 9 5 3 AUTOMA...

Page 74: ...c switch off function in order to save the batteries see section 9 5 1 SYSTEM page 73 The automatic switchoff function switches off the meter if no key is pressed for an adjustable period The automatic switchoff function is not active if the power pack is connected if a USB B cable is connected if the Automatic data storage function is active or with automatic data trans mission System Clock funct...

Page 75: ... pH The following settings for pH measurements are reset to the default settings with the Reset function The sensor settings are reset under the Reset menu item in the menu for cali bration and measurement settings To open the settings display the required measured parameter in the measured value display and press the ENTER key The calibration data are reset to the default settings together with t...

Page 76: ...pen the settings display the required measured parameter in the measured value display and press the ENTER key Conductivity The following settings for conductivity measurements are reset to the default settings with the Reset function Setting Default settings mV resolution 0 1 Setting Default settings Calibration interval 180 d Measured parameter D O concentration mg l Salinity value 0 0 Salinity ...

Page 77: ...9 6 2 Resetting the system settings The following system settings can be reset to the default condition The resetting of the system settings is done in the menu Storage config System Reset To open the menu Storage config in the measured value display press the ENTER__ key Setting Default settings Language English Audio signal on Baud rate 4800 Baud Output format ASCII Decimal separator Contrast 50...

Page 78: ...the same time output to the interface When the storage is full When all storage locations are occupied it is not possible to continue storing Then you can e g transmit the stored data to a PC see section 10 3 1 MANAG ING THE MEASUREMENT DATA STORAGE page 81 and subsequently erase the data storage see section 10 3 2 ERASING THE MEASUREMENT DATA STORAGE page 82 1 Press the STO key shortly The menu f...

Page 79: ...cal display of the storage usage ID number 1 Interval 30 s Duration 180 min continue 0d03h00min 0 1d17h33min Automatic data storage 1 2 3 03 04 2013 08 00 Back Menu item Possible setting Explanation ID number 1 10000 ID number for the dataset series Interval 1 s 5 s 10 s 30 s 1 min 5 min 10 min 15 min 30 min 60 min Storage interval The lower limit of the storage interval can be restricted by the n...

Page 80: ... as follows to switch off the automatic data storage function before the adjusted storage duration has expired 1 Remaining storing duration 2 Graphical display of the storage duration If the automatic data storage function is activated only the follow ing keys are active M STO_ and On Off The other keys and the automatic switch off function are deactivated 25 0 7 007 pH C 0 14 0d03h00min 1 2 03 04...

Page 81: ...he settings are explained here using the manual data storage as an example The same settings and functions are available for the automatic data storage Menu item Setting function Explanation Data storage Manual data storage Display Displays all measurement data sets page by page Further options Scroll through the datasets with Output the displayed dataset to the interface with F2 USB output Quit t...

Page 82: ...ta storage see section 10 3 1 MANAGING THE MEASUREMENT DATA STORAGE page 81 10 3 3 Measurement dataset A complete dataset consists of Date time Meter name series number Sensor name series number ID number Manual data storage 3 of 64 03 04 2013 07 43 33 ID number 1 4110 B092500013 pH 7 000 24 8 C AR Sensor 03 04 2013 08 00 Back USB output 03 04 2013 07 43 33 4010 1W Ser no 09250023 ID number 2 4110...

Page 83: ... storing stable measured value Otherwise the AR dis play is missing Calibration evaluation 4 levels or no evaluation or QSC percentage 10 3 4 Storage locations The MultiLab 4010 1W meter has two measurement data storages The measured values recorded either manually or automatic are stored separately in individual measurement data storages Data storage Maximum number of datasets Manual data storage...

Page 84: ...the measurement data on the PC e g MultiLab Importer see CD ROM or Internet Installation of the USB driver Connecting a PC Adjusting the set tings for the data transmission 1 Insert the supplied installation CD in the CD drive of your PC or Download the USB driver from the Internet and unpack the files and folders 2 Start the driver installation 32 bits or 64 bits suitable for your operat ing syst...

Page 85: ...al Simultaneously with every automatic data storing process see section 10 2 AUTOMATIC DATA STORAGE AT INTER VALS page 79 Stored mea sured values Manual Displayed dataset with F2 USB out put after calling up from the data stor age All datasets with the Output to RS232 USB function see section 10 3 1 MANAGING THE MEASUREMENT DATA STORAGE page 81 calibration records Manual Calibration record with F2...

Page 86: ...7 08 2018 11 3 BOD Analyst Pro With the aid of the BOD Analyst Pro software you can administrate BOD measurement on the PC and automatically calculate the measured values More detailed information can be found in the BOD Analyst Pro operating manual ...

Page 87: ...nd ON OFF 3 Lever to open the paper compartment 4 Lid of the paper compartment 2 1 3 4 1 Connect the power pack to the MultiLab 4010P 1W The LED lights up green The printer is ready for operation or When the printer had been switched off LED flashing Switch on the printer with ON OFF The LED lights up green The printer is ready for operation If there is a USB B connection at the same time e g to a...

Page 88: ...1 Changing the roll of paper thermal paper Menu item Possible set ting Explanation System Printer Font size 12x20 8x16 7x16 Select the font size for the printer A print sample font of the printer to view the available font sizes can be output with ON OFF_ System Printer Print test page The printer prints the meter informa tion from the menu System Ser vice information The current printer settings ...

Page 89: ...cable from the meter Function store automatically at intervals with long intervals is switched on Switch off the function see section 10 2 AUTOMATIC DATA STORAGE AT INTERVALS page 79 No paper available Insert a roll of paper Cause Remedy Paper inserted the wrong way up Turn the roll of paper around and insert it with the other side upwards Cause Remedy The function store automatically at intervals...

Page 90: ... on maintenance You can operate the meter either with normal batteries or with rechargeable batteries Ni MH In order to charge the batteries an external charging device is required 1 Open the battery compartment 1 on the underside of the meter 1 Battery compartment CAUTION Make sure that the poles of the batteries are positioned cor rectly The signs on the batteries must correspond to the signs in...

Page 91: ...stem statutory in your country If you have any questions please contact your supplier 4 Set the date and time see section 4 4 5 EXAMPLE 2 ON NAVIGATION SETTING THE DATE AND TIME page 24 Dispose of used batteries according to the local regulations of your country End users within the European Union are obligated to return used batteries even ecologically compatible ones to a collection point set up...

Page 92: ... Air bubble in front of the junction Remove air bubble e g sway or stir the solution Cable broken Replace the sensor Gel electrolyte dried out Replace the sensor Cause Remedy IDS pH sensor The values determined for zero point and slope of the IDS pH sensor are outside the allowed limits Recalibrate Sensor soiled Clean the sensor Sensor broken Replace the sensor Buffer solutions The used buffer sol...

Page 93: ...pH sensor test sample Conductivity too low Use suitable IDS pH sensor Temperature too high Use suitable IDS pH sensor Organic liquids Use suitable IDS pH sensor Cause Remedy IDS pH sensor Sensor unsuitable Use suitable IDS sensor Temperature difference between buffer and test sample too great Adjust temperature of buffer or sam ple solutions Measurement procedure not suitable Follow special proced...

Page 94: ...e sensor cap Replace the sensor Calibration failed Recalibrate D O concentration during zero point calibration too high Immerse the sensor in an oxygen free solution More information and instructions on cleaning and exchange of sensors are given in the documentation of your sensor Cause Remedy Measured value outside the measuring range Use suitable IDS conductivity sensor Cause Remedy Sensor conta...

Page 95: ...teries almost empty Replace the batteries see section 13 1 MAINTENANCE page 90 Cause Remedy Operating condition undefined or EMC load unallowed Processor reset Press the ENTER and On Off key simultaneously Cause Remedy E g a question by the service department Switch on the meter Open the menu ENTER__ Stor age config System Service infor mation The instrument data are displayed or Connect the senso...

Page 96: ...ical safety Protective class III Test certificates CE Ambient conditions Storage 25 C 65 C Operation 5 C 55 C With the power pack connected 5 C 40 C Admissible relative humidity Yearly mean 75 30 days year 95 Other days 85 Power supply Batteries 4 x 1 5 V alkali manganese batteries type AA Operational life Approx 150 h Power pack Helmsman Industrial Co Ltd SEI0901100P Input 100 240 V 50 60 Hz 0 5 ...

Page 97: ...ate Adjustable 1200 2400 4800 9600 19200 Baud Data bits 8 Stop bits 2 Parity None Handshake RTS CTS Cable length max 3 m 9 843 feet Guidelines and norms used EMC EC directive 2014 30 EC EN 61326 1 EN 61000 3 2 EN 61000 3 3 FCC Class A Meter safety EC directive 2014 35 EC EN 61010 1 IP protection class EN 60529 ...

Page 98: ...E VERSION IS IN THE METER OR IDS SENSOR PAGE 95 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the meter or meter type the new data are displayed there 2 In the windows start menu open the update folder and start the firm ware update program for the meter 3 Using the USB interface cable connect the Multi...

Page 99: ... METER OR IDS SENSOR PAGE 95 1 Install the downloaded firmware update on a PC An update folder is created in the Windows start menu If an update folder already exists for the sensor or sensor type the new data are displayed there 2 In the windows start menu open the update folder and start the firm ware update program for the IDS sensor 3 Connect the IDS sensor to the MultiLab 4010 1W meter 4 Usin...

Page 100: ...y divided by the unit of the molality The practical pH value is the value of a pH measurement Potentiometry Name of a measuring technique The signal depending on the mea sured parameter of the electrode is the electrical potential The electri cal current remains constant Slope The slope of a linear calibration function Zero point The zero point of a pH combination electrode is the pH value at whic...

Page 101: ... T TRef D O saturation Short name for the relative D O saturation Relation of the D O partial pressure in the test sample to the D O partial pressure of air at the current air pressure Example 100 means that the test sample and the ambient air have the same D O partial pressure air and test sample are balanced Salinity The absolute salinity SA of seawater corresponds to the relationship of the mas...

Page 102: ...ll settings of a measuring system Resolution Smallest difference between two measured values that can be dis played by a meter Stability control AutoRead Function to control the measured value stability Standard solution The standard solution is a solution where the measured value is known by definition It is used to calibrate a measuring system Temperature function Name of a mathematical function...

Page 103: ...7 Firmware update 98 I Initial commissioning 13 Initialize 75 Interval for calibration 66 K Keys 16 M Measured value display 20 Measurement accuracy 66 Measurement data storage Storage locations 83 Measurement dataset 82 Measuring Conductivity 55 O2 44 ORP 41 pH 26 Menu for calibration and measurement settings O2 67 pH ORP 63 Menus navigation 20 Messages 21 P pH buffer sets 64 Printer 87 R Reset 7...

Page 104: ...Index MultiLab 4010 1W 104 ba76141e07 08 2018 Transmitting data 84 automatic 85 Manual 85 Transmitting measured values 84 Two point calibration pH 30 32 Z Zero point of pH electrode 28 ...

Page 105: ...MultiLab 4010 1W Index ba76141e07 08 2018 105 ...

Page 106: ...69 10 531 9 930 9 362 8 826 9 0 11 559 10 907 10 290 9 707 9 156 8 636 10 0 11 288 10 656 10 058 9 493 8 959 8 454 11 0 10 027 10 415 9 835 9 287 8 769 8 279 12 0 10 777 10 183 9 621 9 089 8 586 8 111 13 0 10 537 9 961 9 416 8 899 8 411 7 949 14 0 10 306 9 747 9 218 8 716 8 242 7 792 15 0 10 084 9 541 9 027 8 540 8 079 7 642 16 0 9 870 9 344 8 844 8 370 7 922 7 496 17 0 9 665 9 153 8 667 8 207 7 7...

Page 107: ... 5 842 5 576 5 321 5 078 41 0 6 312 6 026 5 753 5 493 5 243 5 005 42 0 6 213 5 934 5 667 5 411 5 167 4 993 43 0 6 116 5 843 5 581 5 331 5 091 4 861 44 0 6 021 5 753 5 497 5 252 5 017 4 793 45 0 5 927 5 665 5 414 5 174 4 944 4 724 46 0 5 835 5 578 5 333 5 097 4 872 4 656 47 0 5 744 5 493 5 252 5 021 4 801 4 589 48 0 5 654 5 408 5 172 4 947 4 730 4 523 49 0 5 565 5 324 5 094 4 872 4 660 4 457 50 0 5...

Page 108: ... 33 668 8 89 2 892 3496 1066 88 26 03 661 2 88 1 881 3804 1106 87 25 73 653 6 87 2 871 4115 1254 86 25 43 646 86 1 861 4430 1350 85 25 13 638 4 85 1 851 4747 1447 84 24 84 630 8 84 1 841 5067 1544 83 24 54 623 2 83 1 831 5391 1643 82 24 24 615 6 82 1 821 5717 1743 81 23 94 608 0 81 06 811 6047 1843 80 23 64 600 4 80 05 800 6381 1945 79 23 34 592 8 79 03 790 6717 2047 78 23 04 585 2 78 02 780 7058 ...

Page 109: ...the multiplier for a specific sample 1 Determine the specific conductance of a water sample from the site 2 Filter a portion of water from the site 3 Carefully measure a volume of the filtered water Completely evaporate to yield a dry solid 4 Accurately weight the remaining solid 5 Divide the weight of the solid in grams by the volume of water used in liters to yield the TDS value in g L for the s...

Page 110: ...Appendix MultiLab 4010 1W 110 ba76141e07 08 2018 ...

Page 111: ... returning a product for service include the Product Return form with cleaning certification The form must be completely filled out for an YSI Service Center to accept the instrument for service The Product Return form may be downloaded at www ysi com and clicking on the Support tab Telephone 800 897 4151 937 767 7241 Monday through Friday 8 00 AM to 5 00 PM ET Fax 937 767 1058 Email info ysi com ...

Page 112: ...Contact Information MultiLab 4010 1W 112 ba76141e07 08 2018 ...

Page 113: ......

Page 114: ...lyze and return water to the environment and we help people use water efficiently in their homes buildings factories and farms In more than 150 countries we have strong long standing relationships with customers who know us for our powerful combination of leading product brands and applications expertise backed by a legacy of innovation For more information on how Xylem can help you go to www xyle...

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