Teledyne 3010MA Operating Instructions Manual Download

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Paramagnetic O2 Purity Analyzer

Teledyne Analytical Instruments

vii

6.2.2 Cross Interference

6.3 Oven and Temperature Controller

6.4 Sample System

6.5 Leak Checking the Analysis Unit

6.6 Initial Sensor Calibration

Appendix...................................................................................... 81

A-1 Model 3010MA Specifications

A-2 Recommended 2-Year Spare Parts List

A-3 Drawing List

Index............................................................................................. 85

Summary of Contents for 3010MA

Page 1: ...protective equipment may be required when servicing this instrument Hazardous voltages exist on certain components internally which may persist for a time even after the power is turned off and discon...

Page 2: ...s shape or weight of any parts in so far as such alterations do not adversely affect our warranty Important Notice This instrument provides measurement readings to its user and serves as a tool by whi...

Page 3: ...OT SURFACE WARNING This warning is specific to heated components within the instrument Failure to heed the warning could result in serious burns to skin and underlying tissue WARNING ELECTRICAL SHOCK...

Page 4: ...for a particular application or features and or options added per customer requests Please check the front of this manual for any additional information in the form of an Addendum which discusses spe...

Page 5: ...cessing 21 2 5 Temperature Control 22 Installation 25 3 1 Unpacking the Analyzer 25 3 2 Mounting the Analyzer 25 3 3 Rear Panel Connections Control Unit 28 3 3 1 Gas Connections Control Unit 28 3 3 2...

Page 6: ...creen 50 4 3 7 Display Sensor Output 50 4 4 The Zero and Span Functions 50 4 4 1 Span Cal 51 4 4 1 1 Auto Mode Spanning 51 4 4 1 2 Manual Mode Spanning 52 4 5 The Alarms Function 53 4 6 The Range Func...

Page 7: ...Cross Interference 71 6 3 Oven and Temperature Controller 74 6 4 Sample System 75 6 5 Leak Checking the Analysis Unit 78 6 6 Initial Sensor Calibration 78 Appendix 81 A 1 Model 3010MA Specifications 8...

Page 8: ...4 Range ID Relay Connections 33 Table 3 5 50 Pin Equipment Interface Connector 35 Table 3 6 Commands via RS 232 Input 37 Table 3 7 Required RS 232 Options 37 Table 4 1 Linear Analog Output 57 Table 4...

Page 9: ...f the Model 3010MA Control Unit 28 Figure 3 5 Equipment Interface Connector Pin Arrangement 30 Figure 3 6 Remote Valve Connections 34 Figure 3 7 FET Series Resistance 35 Figure 3 8 Analysis Unit Rear...

Page 10: ...ensor sample system and flowmeter Part I of this manual covers the Model 3010MA flush panel and or rack mount Control Unit The Analysis Unit is covered in Part II of this manual Typical Applications A...

Page 11: ...ally select the proper preset range within the 95 100 range of the sensor Manual override allows the user to lock onto a specific range of interest Two user adjustable concentration alarms and a syste...

Page 12: ...Part 1 Control Unit Model 3010MA Teledyne Analytical Instruments xii...

Page 13: ...Paramagnetic O2 Purity Analyzer Introduction Teledyne Analytical Instruments 13 OPERATING INSTRUCTIONS Model 3010MA Paramagnetic Oxygen Purity Analyzer Part I Control Unit...

Page 14: ...Part 1 Control Unit Model 3010MA Teledyne Analytical Instruments 14...

Page 15: ...perature controller Pressure compensation circuitry 24 VDC power supply for driving the Analysis Unit Digital meter readout and display circuit board Interface screen and circuit board 1 2 Front Panel...

Page 16: ...creen in a series If none remains returns to the Analyze screen Escape Moves VFD display back to the previous screen in a series If none remains returns to the Analyze screen Digital Meter Display The...

Page 17: ...he upper right corner of the panel is pressed all the way in with a narrow gauge tool Accessing the main circuit board requires unfastening the rear panel screws and sliding the unit out of the case 1...

Page 18: ...Outputs 0 1 Vdc concentration and 0 1 V dc range ID 4 20 mA concentration and optional 4 20 mA range ID Remote Span Zero Digital inputs for external control of analyzer calibration Calibration Contac...

Page 19: ...unt of oxygen present in the sample into an electrical signal It is a partial pressure device sensitive to both operating pressure vent pressure and temperature fluctuations The output from the sensor...

Page 20: ...Part 1 Control Unit Model 3010MA Teledyne Analytical Instruments 20 Figure 2 1 Block Diagram for Model 3010MA Control Unit Figure 2 2 Block Diagram for Model 3010MA Analysis Unit...

Page 21: ...ar Control unit With the exception of the paramagnetic sensor all of the system electronics are located in the Control Unit Figure 2 3 shows the location of the temperature controller and the main ele...

Page 22: ...me digital information is also sent to a 12 bit digital to analog converter that produces the 4 20 mA dc and the 0 1 V dc analog concentration signal outputs and the analog range ID outputs The microp...

Page 23: ...Paramagnetic O2 Purity Analyzer Operational Theory Teledyne Analytical Instruments 23 Figure 2 4 Block Diagram of the Model 3010MA Electronics...

Page 24: ...Part 1 Control Unit Model 3010MA Teledyne Analytical Instruments 24...

Page 25: ...ystem for operation Carefully unpack the analyzer and inspect it for damage Immediately report any damage to the shipping agent 3 2 Mounting the Analyzer The Model 3010MA is for indoor use in a genera...

Page 26: ...Part 1 Control Unit Model 3010MA Teledyne Analytical Instruments 26 Figure 3 1 Rack Mountable Control and Analysis Units...

Page 27: ...nics PCB s and temperature controller inside the instrument The door is spring loaded and will swing open when the button in the center of the latch upper right corner is pressed all the way in with a...

Page 28: ...l Unit 3 3 1 Gas Connections Control Unit The only gas connection made to the Control Unit is the pressure compensation line extending between the Analysis unit and the Control Unit A 1 8 inch tube fi...

Page 29: ...DBY SWITCH ON THE FRONT PANEL IS FOR SWITCHING POWER ON OR OFF TO THE DISPLAYS AND OUTPUTS ONLY The analyzer requires a 90 130 or 200 240 VAC 47 63 Hz power source A switch on the rear panel is used t...

Page 30: ...h Range 3 4 20 mA dc Range M option only Current increases linearly with increasing oxygen from 4 mA at 0 ppm to 20 mA at full scale Full scale 100 O2 for all ranges 4 4 20 mA dc Range ID This option...

Page 31: ...entration is below threshold Failsafe or non failsafe Latching or non latching Out defeated System Alarm Actuates when DC power supplied to circuits is unacceptable in one or more parameters Permanent...

Page 32: ...e appropriately Span Floating input 5 to 24 V input across the and pins puts the analyzer into the Span mode Either side may be grounded at the source of the signal 0 to 1 volt across the terminals al...

Page 33: ...until the CRC closes The CRC will quickly close 2 When the CRC closes remove the zero command 3 When CRC opens again send a span command until the CRC closes The CRC will quickly close 4 When the CRC...

Page 34: ...d valves as detailed below The remote valve connections are used as a method for directly controlling external sample zero span gas valves See Figure 3 6 Figure 3 6 Remote Valve Connections The voltag...

Page 35: ...Table 3 5 50 Pin Equipment Interface Connector Pin Function Pin Function 1 26 2 27 3 Range ID 4 20 mA floating 28 Threshold Alarm 1 Mov Contact 4 Range ID 4 20 mA floating 29 5 Range 4 20 mA floating...

Page 36: ...ote SAMPLE valve return Available by special option only 3 3 2 4 RS 232 PORT The digital signal output is a standard RS 232 serial communications port used to connect the analyzer to a computer termin...

Page 37: ...ng input Stops Starts any status message output from the RS 232 until st enter is sent again The RS 232 protocol allows some flexibility in its implementation Table 3 2 lists certain RS 232 values tha...

Page 38: ...ded in the Drawings section in the rear of this manual which contains a panel cutout diagram 3 5 Rear Panel Connections Analysis Unit The Rear Panel of the Analysis Unit is shown in Figure 3 8 The fol...

Page 39: ...also recommended that a 50 micron filter be installed in the sample line upstream from the restrictor to remove particulate matter that could otherwise clog the narrow passageways in the restrictor o...

Page 40: ...esidual water vapor or contaminants Note Purging can be accomplishedwith sample gas if the gas is dry If in doubt use an inert dry gas connected to the sample in port for purging Following the Self di...

Page 41: ...n latching failsafe etc Before you configure your 3010MA these default values are in effect Ranges LO 95 100 MED 96 100 HI 98 100 Auto Ranging ON Alarm Relays Defeated 90 HI Not failsafe Not latching...

Page 42: ...hierarchy of functions available to the operator via the function buttons Figure 4 1 Hierarchy of Functions Available on the Model 3010MA The six function buttons on the analyzer are Analyze This is...

Page 43: ...is described in greater detail in the following procedures The VFD screen text that accompanies each operation is reproduced at the appropriate point in the procedure in a Monospaced type style Pushb...

Page 44: ...to check the integrity of the power supply output boards and amplifiers Version Displays Manufacturer Model and Software Version of instrument 4 3 1 Setting the Display NOTE Contrast function is disab...

Page 45: ...Span Zero screen appears use the arrows to blink the Span or Zero OFF ON field Use arrows to set the OFF ON field to ON You can now turn these fields ON because there is a nonzero span interval defin...

Page 46: ...her or not a password has been previously installed T E T A I Enter PWD or A A A A A Enter PWD The screen prompts you to enter the current password If you are not using password protection press Enter...

Page 47: ...to change the password the password assignment screen appears T E T A I ENT To Proceed or A A A A A ENT To Proceed Enter the password using the arrow keys to move back and forth between the existing p...

Page 48: ...how which alarm it is 95 00 Anlz AL 1 NOTE If you log off the system using the logout function in the system menu you will now be required to re enter the password to gain access to Span Zero Alarm an...

Page 49: ...st during operation Press the System button to start the System function Contrast Auto Cal PSWD Logout More Use the arrow keys to blink More then press Enter Version Self Test Sensor Output Use the ar...

Page 50: ...e arrow keys again to move the blinking to the Cell Output function Press Enter The sensor output will then be displayed on the screen 4 4 The Zero and Span Functions The analyzer is calibrated using...

Page 51: ...ve readings from the sensor to determine when the output matches the span gas concentration Span calibration can also be performed manual mode where the operator determines when the span concentration...

Page 52: ...ss UP to permit modification Mod of span value Use the arrow keys to enter the oxygen concentration of the span gas you are using The arrows chose the digit and the arrows choose the value of the digi...

Page 53: ...he following four points 1 Which if any of the alarms are to be high alarms and which if any are to be low alarms Setting an alarm as HIGH triggers the alarm when the oxygen concentration rises above...

Page 54: ...1 is blinking AL 1 AL 2 Choose Alarm Set up alarm 1 by moving the blinking over to AL 1 using the arrow keys Then press Enter to move to the next screen AL 1 98 00 HI Dft N Fs N Ltch N Five parameter...

Page 55: ...ded the instrument will automatically shift to the next higher range If the concentration falls slightly below full scale of the next lower range the instrument will switch to that range A correspondi...

Page 56: ...itch from autoranging to fixed range analysis enter the range function by pressing the Range button on the front panel Use the arrow keys to move the blinking over AUTO Use the arrow keys to switch fr...

Page 57: ...r is equipped with two 0 1 V dc analog output terminals accessible on the back panel one concentration and one range ID The standard model also includes one isolated 4 20 mA dc current outputs for the...

Page 58: ...instrument is currently on especially when the analyzer is in the autoranging mode To provide an indication of the range a second pair of analog output terminals are used They generate a steady prese...

Page 59: ...lacing fuses and recalibration For recalibration see Section 4 4 The Zero and Span Functions WARNING SEE WARNINGS ON THE TITLE PAGE OF THIS MANUAL 5 2 Fuse Replacement The fuse compartment is located...

Page 60: ...n in Figure 5 1 American Fuses European Fuses Figure 5 2 Installing Fuses 5 3 System Self Diagnostic Test 1 Press the System button to enter the system mode 2 Use the arrow keys to move to More and pr...

Page 61: ...ARNINGS ON THE TITLE PAGE OF THIS MANUAL WARNING UNPLUG THE POWER CORD FROM THE POWER SOURCE PRIOR TO OPENING THE INSTRUMENT FOR MAINTENANCE OR CLEANING The 3010MA is comprised of the Control unit and...

Page 62: ...his picture See also the drawings located in the Drawings section at the back of this manual The Front Panel Display LED and display PCB as well as the temperature controller are accessible from the f...

Page 63: ...el Screws 5 5 Cleaning If the instrument is unmounted at the time of cleaning disconnect the instrument from the power source Close and latch the front panel access door Clean outside surfaces with a...

Page 64: ...Part 1 Control Unit Model 3010MA Teledyne Analytical Instruments 64...

Page 65: ...Paramagnetic O2 Purity Analyzer Analysis Unit Teledyne Analytical Instruments 65 OPERATING INSTRUCTIONS Model 3010MA Paramagnetic Oxygen Purity Analyzer Part II Analysis Unit...

Page 66: ...Part 2 Analysis Unit Model 3010MA Teledyne Analytical Instruments 66...

Page 67: ...tputs as a standard feature and linear across the entire analysis range The Model 3010MA uses a split architecture design with the Control Unit physically separate from the Analysis Unit to provide ad...

Page 68: ...t platinum wire is suspended in an inhomogneous magnetic field surrounded by sample gas This glass dumbbell is diamagnetic does not respond or only weakly responds to a magnetic influence and tends to...

Page 69: ...Paramagnetic O2 Purity Analyzer Analysis Unit Teledyne Analytical Instruments 69 Figure 6 1 Side view of Paramagnetic Sensor Figure 6 2 Front View of the Paramagnetic Sensor...

Page 70: ...e 6 2 is a drawing showing the side of the sensor Figure 6 3 shows the actual sensor and the location of the zero and span trimpots Figure 6 3 Sensor and Trimpot Identification The electrical intercon...

Page 71: ...rried out by the microprocessor as described in Part I Chapter 4 6 2 2 Cross Interference As mentioned previously the selectivity of the measuring system is based on the extraordinarily high magnetic...

Page 72: ...Part 2 Analysis Unit Model 3010MA Teledyne Analytical Instruments 72 Figure 6 4 15 Pin Sensor Cable and Pin Identification...

Page 73: ...nia NH3 0 26 Hydrogen Iodide HI 1 10 Argon Ar 0 22 Hydrogen Sulphide H2S 0 39 Bromine Br2 1 30 Iodine l2 2 40 1 2 Butadiene C4H6 0 49 Isobutane C4H10 1 11 1 3 Butadiene C4H6 0 49 Isopentane C5H12 1 49...

Page 74: ...used to provide thermal stability to the sensor assembly is comprised of dual 40 watt heaters powered by 115 or 230 V ac from the Control Unit The oven temperature is maintained at 40 C by a PID temp...

Page 75: ...the present reading and the baseline set during the last calibration The linear range of the uncorrected sensor output is 0 1 2 V dc For proper operation the raw output must be adjusted to 0 V dc at 9...

Page 76: ...ibration gas flowing through the system is monitored by a flowmeter downstream from the sensor The gases delivered to the instrument should be at constant pressure and have constant flow rates They mu...

Page 77: ...circuit in the Control Unit and is vented to atmospheric pressure at the Control Unit A bypass loop can be installed around the anaylsis unit to improve the overall response time of the instrument If...

Page 78: ...cial soap solution and pressurize the system using clean air nitrogen or other non toxic non flammable gas to 10 psig or less Apply the soap solution and watch for vigorous bubbling A certain amount o...

Page 79: ...oth the zero gas 95 O2 balance N2 and the span gas 100 O2 To perform the initial calibration 1 Assuming that the instrument is installed properly and gas line connections including sample in zero and...

Page 80: ...he span gas and open the valve to the zero gas Again adjust the flow to same flow that was used for the span gas Adjust the left trim screw on the sensor until the cell output reads 0 V dc 0 00 0 100...

Page 81: ...S 232 communications port Power 100 130 or 200 240 VAC at 47 63 Hz User selected on rear of control unit Operating Temperature 20 30 C Accuracy 0 045 O2 absolute at constant temperature once thermal e...

Page 82: ...Appendix Model 3010MA Teledyne Analytical Instruments 82 Approvals CE mark Area Classification General Purpose...

Page 83: ...Fuse 2 A 250 V 5 20 mm Slow Blow 2 F73 Ferrule 1 4 SS 2 F74 Ferrule 1 4 SS 2 N73 Nut 1 4 SS 1 R2533 Restrictor 1 V11 Union SS 1 4 1 S1307 Screwdriver 6 F1586 Thermal fuse 1 F1584 Blower fan NOTE Orde...

Page 84: ...Appendix Model 3010MA Teledyne Analytical Instruments 84 A 3 Drawing List D 71698 Outline Drawing B 71699 Piping Diagram A 4 19 inch Relay Rack Panel Mount...

Page 85: ...57 analyzer features x analyzer functions 42 Applications typical x arrow buttons 41 auto ranging xi auto cal See automatic calibration automatic calibration 43 44 51 automatic sequencing of gases 76...

Page 86: ...tion 28 gas connections analysis unit 38 hazardous voltage 62 heater out 17 initial sensor calibration 78 inputs calibration contact 18 digital 18 range id contacts 18 remote span zero 18 installation...

Page 87: ...span zero See inputs remote valve connections 34 restrictor 39 75 RFI protection xi ROM xi 21 RS 232 commands 37 RS 232 port xi 17 36 RTD 19 74 safety information iii sample in 17 sample system 62 76...

Page 88: ...power supply 21 access to 63 vent pressure 22 vent pressure changes 75 vent pressure sensitivity 79 version 44 view sensor output See display sensor output voltage amplifier 22 voltage output See ana...

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