Radleys GreenHouse Instructions Manual Download Page 12

GreenHouse Blowdown Parallel Evaporation System

  Number of 

  Volume   

Vial  

   Evaporation

Solvent 

   Samples  

(ml)

Type

Time (min)

Methanol  

 24  

  2

        3.5ml Vial      

   20

Methanol  

  8 

    5    

         20ml Vial      

 22

Acetonitrile  

 24  

  2

        3.5ml Vial      

   20

Acetonitrile  

 24  

  2

 GreenHouse Tube  

   35

Water

   8   

  5  

       20ml Vial       

  157

DMF  

 24  

  2

        3.5ml Vial      

  138

DMF  

  8 

    5    

         20ml Vial       

  145

40˚C Base Temperature. Flowrate 10 l/min (8 well), 20 l/min (24 well)

Example Evaporation Times

GreenHouse with

Blowdown Head,

Standard

GreenHouse

Base and

GreenHouse

Reaction Block

GreenHouse with

Blowdown Head,

Standard

GreenHouse

Base, Base

Adapter and 24

Position Vial

Rack

GreenHouse with

Blowdown Head,

Standard

GreenHouse

Base, Base

Adapter and 8

Position Vial

Rack

GreenHouse with

Blowdown Head,

Standard

GreenHouse

Base, Base

Adapter and 24

Position MTP

GreenHouse with

Blowdown Head,

low profile Stand

Alone Base and

24 Position Vial

Rack

GreenHouse with

Blowdown Head,

low profile Stand

Alone Base and

8 Position Vial

Rack

GreenHouse with

Blowdown Head,

low profile Stand

Alone Base and

24 Position MTP

Examples 

of Blowdown 

Set-up 

Options

Page 11

Summary of Contents for GreenHouse

Page 1: ...down Parallel Evaporation System Your Local Distributor February 2023 Issue 5 Radleys Shire Hill Saffron Walden Essex CB11 3AZ United Kingdom Tel 44 0 1799 513320 Fax 44 0 1799 513283 Email sales radl...

Page 2: ...6 Set up Operation Page 7 Set up Operation continued Page 8 Set up Operation continued Page 9 Set up Operation continued Page 10 Temperature Control Page 11 Example Evaporation Times Examples of Blow...

Page 3: ...rays GreenHouse Blowdown Evaporator System is ideal for the evaporation of HPLC fractions in vials or micro titer plates Digitally controlled heating from a standard Carousel or IKA stirring hotplate...

Page 4: ...ing blowdown ALWAYS ENSURE that inert gas flow rate is within recommended limits Page 3 Warning Applies when there is a possibility of personal injury Important Note Alerts the user to important facts...

Page 5: ...9684 Blowdown Condenser RR99688 Blowdown 150ml Reservoir RR99658 System 17 GreenHouse Blowdown Complete Upgrade Comprising of the following RR99670 GreenHouse Blowdown Head RR99672 Long Blowdown Pin P...

Page 6: ...wdown Condenser RR99688 Blowdown 150ml Reservoir RR99691 AT01 Vial Rack 4 x 2 For 27 8mm OD Vials RR99692 AT02 Vial Rack 6 x 4 For 13mm OD Vials RR99693 AT03 Vial Rack 6 x 4 For 13 8mm OD Vials RR9969...

Page 7: ...ing giving them superior chemical resistance to most solvents and acids when compared with unplated aluminium or stainless steel They also contain Hastelloy springs and use a Kalrez fluoropolymer seal...

Page 8: ...can damage the threads Important Important Important Important Important Important Important Important Important Important Important Important Important Important Important Note Allow the Reaction Blo...

Page 9: ...tightening may damage the thread Do not use a spanner or wrench to tighten sealing knobs Important Important Important Important Important Important Important Important Important Important Important...

Page 10: ...reduced for thermally less stable compounds See page 13 for important information on pressure control Important Note If the tubes are more than half full use a slower flow rate increasing the flow rat...

Page 11: ...re to the desired level by following the instructions of RR98073 Fuzzy Logic Digital Temperature Controller The set temperature can be maintained to 0 5 C The maximum recommended operating temperature...

Page 12: ...ad Standard GreenHouse Base and GreenHouse Reaction Block GreenHouse with Blowdown Head Standard GreenHouse Base Base Adapter and 24 Position Vial Rack GreenHouse with Blowdown Head Standard GreenHous...

Page 13: ...Important Important Important Important Important Important Important Important Important Important Important Important Important AT01 AT05 AT06 AT03 AT02 Base Adapter with 8 position vial rack Base...

Page 14: ...portant Warning The Blowdown Head Safety Pressure Relief Valve and Gas Inlet Safety Pressure Relief Valve are designed to vent at nominally 4 to 6psi Therefore under normal and correct operation proce...

Page 15: ...with Silicone Rubber It is also more resistant to aromatic hydrocarbons Viton exhibits relatively good resistance to trifluoroacetic acid TFA and is the preferred gasket in this case Thermal Resistan...

Page 16: ......

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