Pike FlexIR Hollow Waveguide Manual Download Page 5

 

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Installing the FlexIR HWG with MCT Detector  

 

Accessory Setup 

 

Turn off the power to the FTIR spectrometer. Connect the interface detector cable of the HWG 
accessory to the detector connector port of the spectrometer. Consult the FTIR manual for additional 
information regarding the detector connector port and the proper software settings to select an 
external detector.  
 
The base optics of the Mid-IR FlexIR HWG Accessory fits into the sample compartment of the FTIR 
spectrometer. The FlexIR HWG Accessory will include the baseplate mount for your FTIR spectrometer. 
Place the accessory into the sample compartment of your FTIR and secure any lock-down screws. 

 

MCT Liquid Nitrogen Filling and Stabilization 

 

Fill the MCT detector with liquid nitrogen using the funnel included with the accessory. 
 

WARNING:  

Wear safety goggles and protective clothing when handling liquid nitrogen. Exposure to 

liquid nitrogen will cause severe skin or eye injury. 

 
Pour a small amount of liquid nitrogen into the funnel and wait for it to drain into the Dewar of the 
detector. Add additional small amounts of liquid nitrogen until the detector is filled. Allow the detector 
to stabilize for about 10 minutes and then top it off with a final amount of liquid nitrogen to completely 
fill the liquid nitrogen Dewar. A lit green LED light indicates the Dewar contains liquid nitrogen and is 
beginning the detector cooling process or is sufficiently cooled. It is not an indication that the accessory 
is necessarily ready for use. Be sure to wait a 10 minute equilibrium time after the Dewar has been 
completely filled. Observing a stable interferogram is another indication that the HWG accessory is 
ready for measurements. An insufficiently cooled detector will produce a low and unsteady signal. The 
red LED light indicates the accessory is not ready for use. If the red LED is illuminated during use check 
that the detector Dewar is filled with liquid nitrogen.

 

 

Installing the HWG Probe 

 

 
The next step is to install the HWG probe. Insert the black probe connector end into the base optics and 
secure with hex screws provided with the accessory as shown on the following page.  

 
 
 
 
 

Summary of Contents for FlexIR Hollow Waveguide

Page 1: ...ocument contains confidential or proprietary information of PIKE Technologies Inc Neither this document nor the information herein is to be reproduced distributed used or disclosed either in whole or...

Page 2: ...ilization 3 Installing the HWG Probe 3 Aligning the FlexIR Accessory 4 Optimizing MCT Pre Amp Gain 6 Removing the FlexIR Accessory 6 Storage 6 ATR Probe 7 Zinc Selenide 7 Germanium 7 Diamond ZnSe Comp...

Page 3: ...oviding exceptional IR throughput The new hollow waveguides are very durable and free from the typical fracture problems encountered with polycrystalline and glass core fibers The highly reflective HW...

Page 4: ...hollow waveguide probes have a limited bend radius of 150 mm A smaller radius bend will break the probe Packing List FlexIR Manual FlexIR Hollow Waveguide Base HWG Probe or Probes PN 045 3000 PN 045...

Page 5: ...nt of liquid nitrogen into the funnel and wait for it to drain into the Dewar of the detector Add additional small amounts of liquid nitrogen until the detector is filled Allow the detector to stabili...

Page 6: ...probe tip be positioned gently touching the diffuse reference disk or a specular mirror embedded in the reference cap included with the probe respectively For an ATR probe no reference or mirror is r...

Page 7: ...ment of the input and output mirror two to three more times if increases in performance are observed to fully optimize the accessory The positioning of the MCT detector has been optimized for the spec...

Page 8: ...in should be adjusted to allow 50 of total energy counts or voltage registering on the detector To adjust the gain remove the gain cap from the front of the base optics Access the gain screw using a s...

Page 9: ...dditionally complexing agents such as ammonia and EDTA will erode its surface because of the formation of complexes The maximum temperature range for the ZnSe probe is ambient to 95 C Germanium German...

Page 10: ...n diffuse surfaces In collecting a background spectrum insert probe into provided reference cap If probe fits tightly or cannot bottom out on reference loosen set screw on side and insert probe cap Ti...

Page 11: ...pectrum of a coating on a smooth reflective surface coating on the outside of a soda can conducive to specular reflectance measurements The second sample featured a painted surface with diffuse reflec...

Page 12: ...ld be used when handling and using ATR crystals since some of the materials can be hazardous Speci cally zinc selenide is a heavy metal material and should be handled with this in mind If the crystal...

Page 13: ...wheeled bin is a clear reminder that the product must NOT be disposed with household waste It is the responsibility of the buyer to discard the product in accordance with Federal regional and local e...

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