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PN 350-0453000-02 

 

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Use of ATR HWG Probe to Investigate Defects in Tape 

 

ATR is an ideal probe to investigate defects on adhesive tape. In this example a background was 
collected while the ATR probe was clean. The sample spectrum was then collected after adhering the 
tape sample to the ATR crystal. The resulting spectrum is shown in Figure 8. Other applications for the 
ATR accessory include reaction monitoring, skin analysis, and small spot defects.   
 
 

 

 

 

 

Figure 8:  Spectrum of transparent tape (adhesive side) collected with the ZnSe ATR probe

 

 

Precautions 

 

SAFETY 

 

Caution should be used when handling and using ATR crystals since some of the materials can be 

hazardous. Specifically, zinc selenide is a heavy metal material and should be handled with this in mind. 

If the crystal is broken or pulverized, the dust may be harmful by inhalation, ingestion, or skin 
absorption.  

 

HWG Probe Assembly Handling 

 

Hollow waveguide assemblies are fragile. Do not bend past their minimum bend radius of 150 mm. Do 
not expose probes to shock. Do not drop as they may get damaged. Do 

not fl

ex or stress the probe and 

waveguide interface. Use caution when analyzing powder samples with diffuse and specular reflectance 
probes. Stay within the prescribed temperature limit for each probe.   

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Summary of Contents for FlexIR Hollow Waveguide

Page 1: ...ocument contains confidential or proprietary information of PIKE Technologies Inc Neither this document nor the information herein is to be reproduced distributed used or disclosed either in whole or...

Page 2: ...ilization 3 Installing the HWG Probe 3 Aligning the FlexIR Accessory 4 Optimizing MCT Pre Amp Gain 6 Removing the FlexIR Accessory 6 Storage 6 ATR Probe 7 Zinc Selenide 7 Germanium 7 Diamond ZnSe Comp...

Page 3: ...oviding exceptional IR throughput The new hollow waveguides are very durable and free from the typical fracture problems encountered with polycrystalline and glass core fibers The highly reflective HW...

Page 4: ...hollow waveguide probes have a limited bend radius of 150 mm A smaller radius bend will break the probe Packing List FlexIR Manual FlexIR Hollow Waveguide Base HWG Probe or Probes PN 045 3000 PN 045...

Page 5: ...nt of liquid nitrogen into the funnel and wait for it to drain into the Dewar of the detector Add additional small amounts of liquid nitrogen until the detector is filled Allow the detector to stabili...

Page 6: ...probe tip be positioned gently touching the diffuse reference disk or a specular mirror embedded in the reference cap included with the probe respectively For an ATR probe no reference or mirror is r...

Page 7: ...ment of the input and output mirror two to three more times if increases in performance are observed to fully optimize the accessory The positioning of the MCT detector has been optimized for the spec...

Page 8: ...in should be adjusted to allow 50 of total energy counts or voltage registering on the detector To adjust the gain remove the gain cap from the front of the base optics Access the gain screw using a s...

Page 9: ...dditionally complexing agents such as ammonia and EDTA will erode its surface because of the formation of complexes The maximum temperature range for the ZnSe probe is ambient to 95 C Germanium German...

Page 10: ...n diffuse surfaces In collecting a background spectrum insert probe into provided reference cap If probe fits tightly or cannot bottom out on reference loosen set screw on side and insert probe cap Ti...

Page 11: ...pectrum of a coating on a smooth reflective surface coating on the outside of a soda can conducive to specular reflectance measurements The second sample featured a painted surface with diffuse reflec...

Page 12: ...ld be used when handling and using ATR crystals since some of the materials can be hazardous Speci cally zinc selenide is a heavy metal material and should be handled with this in mind If the crystal...

Page 13: ...wheeled bin is a clear reminder that the product must NOT be disposed with household waste It is the responsibility of the buyer to discard the product in accordance with Federal regional and local e...

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