Ostec 4434-801-59962935-08 Operating Manual Download Page 19

 
 
 
 
 
 
 

 

 
 

15 

The last tab, 

Library

, is for setting the libraries for search. First, indicate the ones 

available on the computer or local network. To do so, click the 

Add 

button, find the library file 

folder, mark the files and click the 

Open

 button. The 

Delete

 button, on the contrary, excludes 

marked libraries from the list (however, they are not deleted from the drive and can be added 

later). Then mark the libraries in the list that will be used in your search (all items in the list 

are marked by default). To mark more than one line, press 

Ctrl

  or 

Shift

  (just like in the 

Explorer). The 

All

 button marks the whole list, and 

Inv.

 inverts your selection. The number of 

selected libraries and spectra in them is indicated in fields 

Lib.

 and 

Sp.

 Note that the list 

content coincides with the logical 

Libraries

 folder. When it is open in the list window, you can 

add, delete, mark individual libraries for search using context menu commands the same way. 

 

Viewing spectra 

Each open spectrum in the spectrum field (program window bottom) has its own 

sequence number and a curve color. By default, the first curve is black, the second is red, the 

third is dark green etc. The status bar at the window bottom each curve has a corresponding 

icon of the same color and number. Absent curves are marked with a dashed  line. The 

maximum number to display is 16 curves. You can change curve colors (and other properties) 

through the context menu by right clicking above the curve or its icon. All operations (search, 

edit) are usually performed on the first curve. The last open spectrum is marked as number 1, 

the previously opened spectra are numbered in an ascending order by adding one. Any curve 

can become number one if you click on it. You can also change the curve sequence by dragging 

them to a new position. If the position is occupied with another curve, they will exchange 

positions; if the position is empty, the curve will be duplicated. If you drop an icon outside the 

status bar, the spectrum will close. You can also close a spectrum through its context menu. 

The 

File

 toolbar can also be used to 

Close all spectra

 or 

Remove the last curve

 (i.e. the curve 

with the biggest number). On the contrary, the 

Remember curve

 command copies the first 

spectrum to the nearest vacant position. 

Deletion, however, does not apply to invisible curves. An invisible curve does not show 

up in the spectrum field and its presence is marked with a hashed icon. Double click the curve 

icon or use the menu to turn invisibility on or off. You can use this function to protect a 

spectrum against accidental deletion. 

You can zoom in or out spectral curves. To zoom in a curve fragment drag the cursor 

from the fragment top left to the bottom right corner with the left mouse button pressed. On 

button release, the rectangle drawn will fill the window (Fig. 7). Drag from left to right only, 

to expand your spectrum horizontally without changing the vertical scale. Similarly, move the 

cursor from top to bottom to expand your spectrum vertically. You can scroll a zoomed-in 

spectral image dragging it with the left mouse button or using the scroll bars. To return to a 

full-scale image, drag the cursor from right to left with the left mouse button pressed. 

 

 

Figure 7. Scaling curves with a mouse

 

 

Summary of Contents for 4434-801-59962935-08

Page 1: ...IROS 05 IR Fourier Spectrometer Operating Manual FSVE 443430 005RE 2020 Ostec Instruments Moscow...

Page 2: ...specialists who have read this manual are qualified to work on electrical devices up to 1 000 V and briefed on workplace safety rules The spectrometer involves operations with hazardous 220 V 50 Hz c...

Page 3: ...n 6 Device software installation 6 First run 7 Spectrum recording 7 Spectrum reading and copying 9 Spectrum identification 12 Viewing spectra 15 Spectrum editing 18 Calibration 19 Creating and editing...

Page 4: ......

Page 5: ...434 801 59962935 08 Please see spectrometer operating conditions in Table 1 Spectrometer s electromagnetic interference resistance complies with GOST 30804 6 1 2013 and radiated interference with GOST...

Page 6: ...ise ratio RMS in standard conditions in1 min at a resolution of 4 cm 1 in full bandwidth of 2000 2200 cm 1 40 000 Signal gain 1 2 4 8 Resolution 0 5 1 2 4 8 cm 1 Scanning speed spectra per minute For...

Page 7: ...1 Spectrometer optical scheme The inlet optical system 2 converts the IR source 1 radiant energy into a convergent annular beam and makes it focus on the inlet port of the interferometer 3 consisting...

Page 8: ...log to digital conversion is done at equal intervals of the optical path difference intervals The path difference reference scale is generated in a reference channel that consists of a HeNe laser the...

Page 9: ...t 2 the Scan light 3 peripheral equipment connection ports 4 sample compartment 5 MCT detector compartment cover 6 spectrum recording control buttons Note The photo displays the device in basic config...

Page 10: ...right sides The Power switch on the rear side of the device case near the 220 V power connector Device software installation First turn on the computer Run setup exe on the USB flash drive that comes...

Page 11: ...r icons there indicate scan errors Single errors can be caused by the device being pushed or shaken If errors keep occurring or the LED on the case stops blinking and the software window indicator loo...

Page 12: ...the beams reflected from an empty cell distort the spectrum Then click the Background Spectrum button or press Shift F9 The spectrum recording time is proportionate to the number of the scans and can...

Page 13: ...triangle to the right of the button and select you add on from the list Note that the scan number resolution and other recording settings apply to the current selection so switching to another add on...

Page 14: ...You can make any folder a home folder by opening it a clicking a context menu command Thus you can navigate the folder system on the disk through the list You can also open logical spectrum folders th...

Page 15: ...ial if you edit it the file is renamed As the Number field has the line number entering a number in this field results in the line under this number selected e g you can use this feature to get a spec...

Page 16: ...The Acceleration option involves all the CPU cores and multiplies the search speed almost by the number of the cores The Reset to initial values button restores the default values applicable to ordin...

Page 17: ...cating the number of each of them or the range using a hyphen e g C17 N3 5 02 Cl note that you do not have to use 1 Add to your formula if you want it to include any other elements except the listed o...

Page 18: ...ick the View button you can display them in advance Use the Compare button for comparison with the current spectrum and band coloring Use the Purge button to completely delete a peak list The From cur...

Page 19: ...rve The last open spectrum is marked as number 1 the previously opened spectra are numbered in an ascending order by adding one Any curve can become number one if you click on it You can also change t...

Page 20: ...ht Note that these variants do not affect the view if only one curve is open Sample spectra can be displayed both in the transmittance scale the quotient of two spectra current and background for each...

Page 21: ...he dependence of the spectrum current ordinate on the abscissa and vice versa Current X and Y are marked with dashed lines Their values are specified in the text fields at the graph edges You can use...

Page 22: ...it will change the base line or amplitude of the current spectrum in the area of the cursor moving If you magnify the curve images then your edits will be more accurate Plotting border lines involves...

Page 23: ...luted multiple times and recorded again Continue diluting until the peak of the substance to be identify appears on the spectrum For greater accuracy we recommend that you repeat the entire procedure...

Page 24: ...calculating concentration for that peak Consequently if a peak has graph a relevant concentration will show up near the peak height Creating and editing libraries As noted above spectrum libraries are...

Page 25: ...rogram If it does not help unplug and plug the USB cable back in Next turn off the device wait for a minute turn it on again and restart the program If it does not help restart the computer 2 Fault sc...

Page 26: ...rding settings set a different number where necessary If the channel number is correct check the sample compartment for foreign items or pollution 6 Fault software failure Manifestation the program do...

Page 27: ...ery two years Use the Calibration command in the Recording menu or the toolbar button The procedure is performed in the Master mode and consists of five steps Note that you may take measurements in an...

Page 28: ...equires a reference film and a comparison spectrum If you do not have them contact the spectrometer manufacturer or get a thin polystyrene layer ca 0 25 mm and record its spectrum and set the spectrum...

Page 29: ...n measuring precision are assessed at the next step This measurement is the most time consuming and can take a few minutes Its results are entered in the parameter list At the final step click the Rea...

Page 30: ...onditions are the same as the operating conditions Table 1 Place the spectrometer at least 10 cm away from the warehouse floor and walls and at least 50 cm from the heat sources Transportation and sto...

Page 31: ...measuring attenuated total reflection and specular diffuse reflection spectra It consists of a hold down 1 FTIR and SDR flange seats the seat shown covered with a plug flange 2 in Figure 12 The plug...

Page 32: ...remove the sample and clean the hold down tip and crystal surface with an alcohol or other solvent wetted cotton pad Liquid samples are placed at the FTIR element center in the form of a tiny drop do...

Page 33: ......

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