Milli-Q IX 7003 User Manual Download

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REQUIREMENTS AND SPECIFICATIONS

Water specifications

Feed Water

The system has been designed to operate within feed water requirements:

Parameter

Value or range

Pressure

1 bar < P < 6 bar

Type of water

Potable tap water

Temperature

5 - 35°C (41 - 95°F)

Conductivity

< 2000 μS/cm @ 25° C

Dissolved CO

< 30 ppm

Free Chlorine

< 3 ppm

Fouling Index

< 10

4 <pH< 10

Maximum Total Organic Carbon (TOC)

< 2 ppm

LSI

< 0.3

Hardness as CaCO

< 300 ppm

Silica

< 30 ppm

PrePak - maximum total chlorine level

3 ppm for PRPKF00A1

PrePak - maximum Fouling Index

18 for PRPKF00A1

Pure (Type 2) Water: Elix Water

The Milli-Q

IX 7003/7005/7010/7015 system is intended to produce pure water that meets or

exceeds water quality specifications described by the organizations below:

Organization

Water quality / grade

European Pharmacopoeia

Purified water

U.S. Pharmacopoeia

Purified Water

Japanese Pharmacopoeia

Purified Water

Chinese Pharmacopoeia

Purified Water

ASTM

D1193

Type 2 water - Reagent water

ISO

3696

Grade 2 water

Chinese National Standard

GB 6682 Grade 2 water

JIS K 0557

A2 water

Summary of Contents for IX 7003

Page 1: ...User Manual Milli Q IX 7003 7005 7010 7015 ...

Page 2: ...History 14 Flow schematic 15 Troubleshooting 15 Contacts 16 SETTINGS MENU 17 Manager access password 19 System configuration 20 Accessories 22 Alarm configuration 23 Connectivity 24 Date Time Language 24 Units 25 MAINTENANCE MENU 26 Consumable installation wizards 27 Cleaning Sanitization 30 ech2 o UV lamps mercury free 30 Depressurization 31 SELF HELP GUIDE 32 Troubleshooting tips 32 Icons 34 REQ...

Page 3: ...the World Intended use The Milli Q IX 7003 7005 7010 7015 system is intended to produce pure type 2 water from a tap water source primarily for use in research and quality control in a variety of laboratories worldwide The product is designed to produce pure water with specific characteristics refer to the requirements and specifications section when it leaves the E POD unit provided that it is fe...

Page 4: ...iew of a Milli Q IX 7003 water purification unit with the front cover removed 8 Dispensing wheel 4 Accessories holder 9 POD base 5 Rear view of a Milli Q IX 7003 system with its hydraulic and electrical connec tions 10 Storage tank 50L capacity on the pho tograph Note The system can either have one IPAK Gard cartridge Milli Q IX 7003 7005 system or two Milli Q IX 7010 7015 system On the photograph...

Page 5: ...ll 2 Inlet strainer 18 Permeate 3 ways valve 3 Inlet solenoid valve 19 Elix EDI module 4 System feed pressure sensor 20 Pure water resistivity cell 5 IPAK Gard 1 or 2 depending on system type 21 Pure water 3 ways valve 6 Pressure regulator 22 ech2 o bactericidal lamp 7 Reverse osmosis RO reject capillary 23 Storage tank 25 50 or 100L 8 RO pump feed pressure sensor 24 Tank vent filter 9 RO recovery...

Page 6: ... the mercury free ech2 o automated sanitization module ASM lamp The tank vent filter maintains the consistent purity of stored water and provides effective protection against airborne contaminants The ech2 o ASM lamp further protects the integrity of the stored water with regular exposure to bactericidal UV light Throughout the distribution resistivity temperature and pressure are monitored Tank i...

Page 7: ... information Dispensing functions Alerts Alarms when generated by the system Dispense report when generated by the system Menu Consumables Information Settings Maintenance Login Go to Consumables Menu Go to Information Menu Go to Settings Menu Go to Maintenance Menu Go to Manager access ...

Page 8: ...enu or app level screen 1 minute of inactivity generates a time out back to the home screen When in a pop up level screen there is no time out therefore the user remains on this screen until the pop up is manually closed Important If multiple E POD units are installed and a pop up in the settings or maintenance menus is not closed dispensing will remain unavailable on all E POD units until the pop...

Page 9: ...ys displayed on the main screen Dispensing pure water in free flow mode There are several options to dispense pure water Manual Dispensing Full flow To start low flow dispensing turn the dis pense wheel one notch counter clockwise To start dispensing in full flow press the wheel once and quickly release Adjust flow rate Stop To increase the flow rate keep turning the wheel counter clockwise until ...

Page 10: ... button on the screen or the dispensing wheel to initiate the dispense 2 Select the unit 3 Select the desired volume and press OK to validate 4 Press the start button on the screen the dispense wheel or the foot pedal to start dispensing 5 The system will automatically stop once the input volume is dispensed Either press the stop button on the screen the dispense wheel or the foot pedal to stop di...

Page 11: ...n 2 Personalize assign a name or experiment number In the user ID field enter the content of your choice max 15 characters 3 Export Scan the QR code from a mobile device to instantly retrieve the report Click on the export button to save the report on a USB key 4 Automatic archiving The dispense report icon on the home screen will automatically disappear after 5 minutes of inactivity Each dispense...

Page 12: ...and there has been a certain time of user inactivity the screensaver will be displayed on the E POD touch screen Tap anywhere on the screen or initiate a manual dispense by pressing the dispenser wheel to exit the screensaver Home screen Status bar Home Menu ...

Page 13: ... Advice is provided in the information section to help the user troubleshoot If the issue is not resolved and depending upon the alert and alarm either select the Contact tab to find the technical support hotline number for further assistance or the Order tab containing ordering information when applicable To protect the system and user applications alarms of a serious nature will automatically st...

Page 14: ...lity are now available online www mymilliqconsumables com All cartridges have been designed to be easily replaced by a user A short cut is available to the replacement wizard by clicking on the replace pack button in the pop up Important Mercury free ech2 o UV lamps should not be replaced by users Contact the tech nical support hotline to organize a replacement visit Green no action required Yello...

Page 15: ...able lot number catalog number installation date The IPAK Gard and application POD paks information is automatically registered during their instal lation The tank vent filter comes with a RFID card enabling the transfer of the data into the system Go to page 29 Maintenance Consumables installation wizard for further information ...

Page 16: ...temperature Also included is the total volume dispensed during the day Dispensing events report Each row is a dispense operation It is an archive of all the dispense reports To export data or preview a graph 1 Select a time period of interest with a start and end date 2 A graph pre view of the last 30 records is available on the E POD screen 3 Export the report in ods open document source format t...

Page 17: ...low maintenance alert Red technical issue alarm Production flow schematic Distribution flow schematic Troubleshooting Access a diagnostic summary This app contains all the necessary information in one location for effective troubleshooting when in contact with the technical support hotline System information last service visit Water quality consumables installed dates Active alerts alarms auto tes...

Page 18: ... quickly help users identify the right contact for any questions or issues Technical support hotline Application specialist Field service engineer System manager Maintenance operator In case of troubleshooting Application enquiries or quote requirements Only in selected countries contact technical support Responsible for system configuration quality settings Responsible for maintaining the system ...

Page 19: ...ly Read only Periodic EDI rinsing period Read only Read only Tank configuration Tank capacity Read only Read only Tank refill setpoint Read only ech2o ASM lamp cycle start hour Read only Distribution configuration Lab close Recirculation Duration Read only Read only Safety flow stop Read only Production alarm configuration EDI resistivity Read only Permeate conductivity Read only RO ionic rejectio...

Page 20: ...Local network Read only Wi Fi configuration Read only Deactivation only Date Time Lan guage Time zone Date Time Read only Select language Read only Password System manager Units Resistivity Conductivity Read only Temperature Read only Storage tank Read only Temperature compensation mode Read only Pressure Read only ...

Page 21: ... after 1 hour of no activity Note By default this parameter is activated The default password is PASS If the system manager password is forgotten contact the technical support hotline Log off as a Manager 1 Press on the menu button 2 Press on Logout Modify system manager settings This can only be done when logged in as a manager In the Password app 1 Deactivate re activate the manager password thr...

Page 22: ... Safety flow stop A precautionary measure that stops a E POD unit dispensing after having continuously delivered water for a certain duration Adjust to the preferred time by using the arrows or click on the box to access the keypad This setting will not impact volumetric dispensing functions Screensaver This is the maximum duration of inactivity on a E POD unit before the screensaver starts 1 Acti...

Page 23: ...e secondary E POD unit E POD unit name This can be personalized Click on the text box and input up to a maximum of 8 characters Screen brightness Adjust to the preferred brightness from 1 to 7 using the arrows or click on the box to access the keypad and type in the value Sound volume Each E POD unit can emit a sound when alerts alarms are triggered This can be activated or deactivated using the s...

Page 24: ...ed to dispense water using the volumetric dispensing mode Washer Distribution kit This accessory will allow distributing water from a storage tank to washing machines It can be wall mounted Note A specific tank vent filter HF has to be used for such high flow rate application Alarm relay This accessory will allow to relay all or a selection of alarms to a remote device Select the alarm s that will...

Page 25: ...ak Gold 0 22μm sterile filter days 182 30 182 It is recommended to clean the inlet strainer once a year to avoid it becoming clogged Depend ing on the feed water and its particle concentration the inlet strainer clean frequency can be adapted Cartridges should be changed when the system alerts the user Two thresholds can be trig gered for the replacement of the IPAK Gard cartridge The first is the...

Page 26: ...ted device such as a laptop but must be done at the actual HMI screen Date Time Language Date Calendar date representations are shown in the ISO 8601 format 2018 11 06 YYYY MM DD YYYY indicates a four digit year MM indicates a two digit month of the year 01 through 12 DD indicates a two digit day of that month 01 through 31 Start by setting the year 1 Click on the month year title this displays mo...

Page 27: ...ted to 25 C The values are normalised The system firmware eliminates small fluctuations of temperature compensated resistivity or conductivity due to the fact that these two parameters are not measured exactly at the same time TC2 The actual temperature compensated resistivity or conductivity values are displayed In some operating conditions the feed water can be warmer or cooler than the water te...

Page 28: ...ess Available apps Note Dispensing in this menu is only available in the applicable wizards Maintenance screens Maintenance ongoing from the current facing E POD unit Note To unlock both E POD units from maintenance mode and regain access to dispensing functions click on Exit maintenance Maintenance ongoing from another E POD unit or from a remote location if External is indicated on the screen In...

Page 29: ...2 Follow the self guided wizard IPAK Gard 3 5 pretreatment pack IPAKGARA1 IPAK Gard 10 15 pretreatment pack IPAKGARA2 1 or 2 IPAK Gard cartridges depending on system type Note 1 When properly installed the blue side should face you with the e Sure symbol behind Note 2 If the sound has been activated it is normal to hear a buzzer when changing the consumables This is temporary and is only present w...

Page 30: ...s recommended to replace the tank vent filter when replacing the IPAK Gard cartridges Application POD Pak installation 1 Select Install consumables app and click on Application POD Pak installation 2 Select the POD Pak to be installed click on the Next button and follow the self guided wizard Do not over tighten the twist lock action when installing a new POD Pak 3 Rinsing must be performed manual...

Page 31: ...to lift it due to the presence of the ASM UVc LED You can register the vent filter details by selecting the Install consumables app and selecting the vent filter You can either manually type in or register the data by scanning the RFID card on the e Sure tag reader located on the handle of the E POD dispenser unit If you manually type in the data replace XXXXXXXXXXXX by the actual lot number of th...

Page 32: ...ng Follow the self guided wizard Contact your service representative for further information ech2 o UV lamps mercury free Contact the technical support hotline to organize a replacement visit It is highly recommended to have a qualified Milli Q field service representative to change the ech2 o UV lamps Replacement of the lamps involves removing the panels of the Milli Q system Hazardous UV light H...

Page 33: ...roduction depressurization The production depressurization is available by selecting the Depressurization app Simply press when turns into to keep using the system This temporarily stops production and all water processes To go back to tank full tank filling swipe down from the top of the touchscreen near E POD 1 and press Distribution depressurization The distribution depressurization is also ava...

Page 34: ...ays the capacitor will completely discharge When powering on again the system the time date settings will need to be reset see page 24 Information Date Time Language It takes about 45 minutes to recharge the capacitor Inaccurate volumetric dispensing Volumetric dispensing has been validated to work 5 precision Lab glassware precision can vary and to accommodate local needs a flow meter offset menu...

Page 35: ... production process M At the end make sure the icon is present on the top left corner of the screen A blinking icon indicates the tank is being filled A solid icon indicates a full tank Contact us If assistance is needed then get in contact with a local technical service representative The details can be found in the contacts app go to page 16 Information Contacts or visit our website www emdmilli...

Page 36: ...ispense 1 Alarm with number of active alarm s Alert Home Menu Storage tank System manager logged in Mass storage USB connected Ethernet LAN status connected Slider ON Slider OFF Back Calendar entry blinking Production Unit producing water solid Production Unit standby Production Unit blocked Production Unit maintenance Production Unit Maintenance exit Distribution depressurization exit ...

Page 37: ... Silica 30 ppm PrePak maximum total chlorine level 3 ppm for PRPKF00A1 PrePak maximum Fouling Index 18 for PRPKF00A1 Pure Type 2 Water Elix Water The Milli Q IX 7003 7005 7010 7015 system is intended to produce pure water that meets or exceeds water quality specifications described by the organizations below Organization Water quality grade European Pharmacopoeia Purified water U S Pharmacopoeia P...

Page 38: ...k 40 filter or Biopak filters when installed and used in a laminar flow hood Pyrogens endotoxins 0 005 EU mL with Biopak filter when installed and used in a laminar flow hood RNases 1 pg mL with Biopak filter DNases 5 pg mL with Biopak filter Proteases 0 15 µg mL with Biopak filter Production flow rate 3 L h for IX 7003 5 L h for IX 7005 10 L h for IX 7010 15 L h for IX 7015 The following specific...

Page 39: ...T0 50 60 Hz 10 300 VA 100 240 V 10 Environmental Specific environmental conditions have to be respected to ensure normal operation of the Milli Q system Location indoor use only Ambient operating temperature room temperature ranges from 4 C to 40 C Relative humidity room relative humidity conditions of 80 for a temperature up to 31 C decreasing linearly to a relative humidity of 50 at 40 C Altitud...

Page 40: ...with the EU RED directive and or FCC regulations Standard EU We certify that these Lab Water Systems are designed and manufactured in application of the following European Council directives DIRECTIVE 2014 53 EU OF THE EUROPEAN PARLIAMENT AND OF THE COUNCIL of 16 April 2014 on the harmonisation of the laws of the Member States relating to the making available on the market of radio equipment and r...

Page 41: ...culation after each dispense 30s Each hour 3 minutes of automatic recirculation 50 Weeks ON and 2 weeks OFF The produced water is dispensed on the E POD unit If the water system is in tank filling 5 hours a day Catalog Daily water produced L Daily amounts of dis penses Yearly energy con sumption kWh ZIX7003T0 15 10 309 ZIX7005T0 25 15 316 ZIX7010T0 50 20 333 ZIX7015T0 75 30 351 If the water system...

Page 42: ...Requirements and specifications 40 Dimensions and weights Water purification system 7003 7005 dimensions in mm Water purification system 7010 7015 dimensions in mm ...

Page 43: ...Requirements and specifications 41 E POD unit dimensions in mm Storage tank 25L 50 L 100 L dimensions in mm ...

Page 44: ...a dry system in its shipping container Consumables and accessories are not included Operating weight is defined as a wetted system with all its consumables but not any accessories Recycling Directive 2012 19 UE For European users only The symbol crossed bin on a product or its packaging indicates that the product should not be treated like household waste when discarded Instead the product should ...

Page 45: ... ZFC0NN5ST Accessories Name Catalog Number Water sensor ZWATSENA1 Foot pedal ZMQSFTSA1 e Sure dispenser tip ZFDISTPA1 Alarm relay cable ZMQ0ALCA1 Washer Distribution kit 230V Left ZWDK5L100 Washer Distribution kit 230V Right ZWDK5R100 Washer Distribution kit 115V Left ZWDK6L100 Washer Distribution kit 115V Right ZWDK6R100 Washer Distribution kit Adaptor ZWDKADPA1 Washer dist kit wall mounting brac...

Page 46: ...k IPAKGARA1 IPAK Gard 10 15 pretreatment pack IPAKGARA2 Ech2 o ASM Lamp ASMUVLPA1 Ech2 o Bactericidal Lamp ZIXUVLPA1 Vent filter HF for high flow applications TANKVH1A1 Vent filter TANKV01A1 Prepak filter pretreatment pack PRPK000A1 Note MILLI Q IX 7003 5 PURIFICATION KIT is composed of 1 IPAK Gard 3 5 pretreatment pack and 1 tank vent filter Milli Q IX 7010 15 PURIFICATION KIT is composed of 1 IP...

Page 47: ...ark names The initial M Millipore Milli Q E POD ech2 o IPAK Gard Millipak and Biopak are trademarks of Merck KGaA Darmstadt Germany Millipore SAS is an affiliate of Merck KGaA Darmstadt Germany QR Code is a registered trademark of DENSO WAVE INCORPORATED in Japan and other countries All other trademarks are trademarks of their respective manufacturers The Life Science Business of Merck KGaA Darmst...

Page 48: ...been tested by an independent and accredited company for compliance with EU directives related to safety and electromagnetic compatibility The declaration of conformity is available upon request The system has been manufactured using components and practices recommended by UL and has been cULus marked The registration and CB certificates can be verified at www members IECEE org In case of wall mou...

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