Julabo SC 10000w Operating Manual Download Page 1 | Manualshive

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19.04.18

Operating Manual

SemiChill

Recirculating Coolers

Eco-Serie

SC 5000a

air cooled

SC 5000w

water cooled

SC 10000w

water cooled

EN

ERG E

NCY S

TO

P

N

O

T

-

A

U

S

OFF

ON

SC 10000

°C

10

30

60

130

180

220

ES

°C

Flo w

Cond.

1.951.4555-V11 04/18

www.calcert.com

[email protected]

1.800.544.2843

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5

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Summary of Contents for SC 10000w

Page 1: ...oolers Eco Serie SC 5000a air cooled SC 5000w water cooled SC 10000w water cooled EN ERGENCY STO P N O T A U S OFF ON SC 10000 C 10 30 60 130 180 220 ES C Flow Cond 1 951 4555 V11 04 18 www calcert com sales calcert com 1 800 544 2843 0 5 10 15 20 25 30 ...

Page 2: ...equirements of ISO 9001 and ISO 14001 Certificate Registration No 01 100044846 Unpacking and inspecting Unpack the circulator and accessories and inspect them for possible transport damage Damage should be reported to the responsible carrier railway or postal authority and a damage report should be requested These instructions must be followed fully for us to guarantee our full support of your cla...

Page 3: ...lanation of other notes 19 4 3 Safety instructions 20 5 Preparations 22 5 1 Installation 22 5 2 Connecting the external system 23 5 2 1 Tubing 24 5 2 2 Bath fluids 24 5 3 Filling 25 5 4 Draining 26 6 Operating procedures 27 6 1 Power connection 27 6 2 Switching on Start Stop 27 6 3 AUTOSTART ON OFF 28 7 Setting the temperatures 29 8 Safety installations warning functions 29 8 1 Excess temperature ...

Page 4: ...ity 38 9 5 Control parameters Xp Tv Tn 39 9 6 Reset 41 10 Troubleshooting guide Error messages 41 11 Electrical connections 43 12 Remote control 44 12 1 Setup for remote control 44 12 2 Communication with a PC or a superordinated data system 44 12 3 List of commands 45 12 4 Status messages 47 12 5 Error messages 47 13 JULABO Service Online remote diagnosis 48 14 Cleaning repairing the unit 49 www ...

Page 5: ...eratures to ensure an accurate temperature pattern at the selected spot in the bath over the full temperature range Electrical connections The serial interface RS232 allows modern process technology without additional interface The excess temperature protection conforming to IEC 61010 2 010 is a safety installation independent from the control circuit This protection can be indicated and set on th...

Page 6: ...same mains This unit is designed for operation in a controlled electromagnetic environment This means that transmitting devices e g cellular phones should not be used in the immediate vicinity Magnetic radiation may affect other devices with components sensitive to magnetic fields e g monitors We recommend maintaining a minimum distance of 1 m Permissible ambient temperature max 40 C min 5 C Permi...

Page 7: ... is switched off Do not dispose of the battery with household waste Depending on battery regulations in your country you may be obligated to return used or defective batteries to collection sites The product may be used with oil as bath fluid These oils fully or partially consist of mineral oil or synthetic oil For disposal follow the instructions in the material safety data sheets This unit conta...

Page 8: ...Operator responsibility Safety instructions 8 2 2 EC Declaration of Conformity www calcert com sales calcert com 1 800 544 2843 0 5 10 15 20 25 30 ...

Page 9: ...Recirculating Cooler 9 www calcert com sales calcert com 1 800 544 2843 0 5 10 15 20 25 30 ...

Page 10: ...months limited to a maximum of 10 000 working hours To apply for this extended warranty the user must register the unit on the JULABO web site indicating the serial no The extended warranty will apply from the date of JULABO GmbH s original invoice JULABO GmbH reserves the right to decide the validity of any warranty claim In case of faults arising either due to faulty materials or workmanship par...

Page 11: ...z 400 50 3 phases 400 50 3 phases Current cons without heater phase P3 P4 A 7 400 V 7 400 V Current cons with 5kW heater phase P3 P4 A 15 400 V 15 400 V Current consumption with 12kW heater phase P3 P4 A 30 400 V 30 400 V Mains power connection V Hz 208 230 V 3PPE 60Hz 208 230 60 3 phases 208 230 60 3 phases Current cons without heater phase P3 A 9 208 V 8 230 V Current cons without heater phase P...

Page 12: ... 365 440V 3PNPE 50Hz 400 50 3 phases Current consumption without heater phase P3 P4 A 11 400 V Current consumption 5 kW heater phase P3 P4 A 17 400 V Current consumption 12 kW heater phase P3 P4 A 31 400 V Mains power connection197 254 V 3PPE 60Hz V Hz 208 230 60 3 phases Current consumption without heater phase P3 A 15 208 V 16 230 V Current consumption without heater phase P4 A 17 208 V 17 230 V...

Page 13: ...3 P4 P3 P4 Flow rate max Lpm at 0 bar 30 40 33 43 Pressure max bar at 0 liter 1 8 2 5 3 5 4 4 Bath fluid Galden e g Fluorinert 3283 Pressure max bar at 0 liter 3 5 4 4 Notice If Galden or Fluorinert is used the the charge of the motor increases Wrong adjustment causes overheating and eventually destruction of the motor With the circulation pump P3 as well as P4 a maximum pump pressure stage PUMP 1...

Page 14: ... IEC 61 010 1 Use indoors only Altitude up to 2000 m normal zero Ambient temperature see Technical specifications Humidity Max relative humidity 80 for temperatures up to 31 C linear decrease down to 50 relative humidity at a temperature of 40 C Max mains voltage fluctuations of 10 are permissible Protection class according to IEC 60 529 IP 21 The unit corresponds to Class I Overvoltage category I...

Page 15: ...nature has the following duties x The operator must ensure that the equipment is checked at regular intervals for leaks x These intervals depend on the CO2 equivalent of the system This is calculated from the refrigerant fill volume and type of refrigerant The CO2 equivalent of your system is shown on the model plate x The operator undertakes to have maintenance repair service recovery and recycli...

Page 16: ... stainless steel x Chlorinated water will cause pitting corrosion in heat exchangers made of stainless steel x Due to their corrosive characteristics distilled water and deionized water are unsuitable and will cause corrosion of the bath x Due to its corrosive characteristics sea water is not suitable x Due to its microbiological bacterial components which settle in the heat exchanger untreated an...

Page 17: ...21 20 22 23 24 25 26 1 Mains power switch 2 Emergency stop switch 3 C 10 30 60 130 180 220 Adjustable excess temperature protection according to IEC 61010 2 010 4 Keypad Start stop key Key for selecting the working temperature Setpoint 1 2 3 Key for selecting the warning and safety values MENU button for selecting the menu functions Cursor keys left or right www calcert com sales calcert com 1 800...

Page 18: ...ble only air cooled recirculating cooler 12 RS232 Interface RS232 remote control via personal computer 19 2 Connectors for solenoid valve 230 V max 0 1 A No control voltage in the OFF condition 20 4 Safety cutouts Mains fuses 16 A with option H5 2 Safety cutouts Mains fuses 10 A 0 1 Motor protection circuit breaker for compressor motor 21 Mains power cable with plug 22 23 Pump connectors 3 4 NPT m...

Page 19: ...ase follow the documentation The danger is classified using a signal word Read and follow these important instructions Warning Describes a possibly highly dangerous situation If these instructions are not followed serious injury and danger to life could result Caution Describes a possibly dangerous situation If this is not avoided slight or minor injuries could result A warning of possible propert...

Page 20: ...the temperature of the bath fluid prior to draining e g by switching the unit on for a short moment x Use suitable connecting tubing x Avoid sharp bends in the tubing and maintain a sufficient distance from surrounding walls x Make sure that the tubing is securely attached x Regularly check the tubing for material defects e g for cracks x Never operate damaged or leaking units x Always turn off th...

Page 21: ...in operation moving machine parts etc x Do dangerous vapors or gases develop during heating Must the work be done in a fume hood x What to do when a dangerous substance was spilled on or in the unit Before starting to work obtain information concerning the substance and determine the method of decontamination Notice Check the safety installations at least twice a year x Excess temperature protecti...

Page 22: ... least 20 cm of open space on the front and rear venting grids x Do not set up the unit in the immediate vicinity of heat sources and do not expose to sun light x Before operating the unit after transport wait about one hour after installation This will allow any oil that has accumulated laterally during transport to flow back down thus ensuring that the compressor can develop its maximum capacity...

Page 23: ...zard For this reason solenoid valves for loop circuit or shut off valves can be integrated in the loop circuit LConnect the valve to the connector 19 Order No Description 8 980 705 Solenoid valve set 230V 50 60Hz x Unscrew the collar nut from the overflow connector 24 Connect a piece of tubing to the overflow connector and drain into a suitable vessel Order No 8 970 460 Barbed fitting for tubing 8...

Page 24: ...e tubing for material defects e g for cracks at least once a year x Preventive maintenance replace the tubing from time to time 5 2 2 Bath fluids Caution Carefully read the material safety data sheet of the bath fluid used particularly with regard to the fire point If a bath fluid with a fire point of d 65 C is used only supervised operation is possible Water The quality of water depends on local ...

Page 25: ...h fluids ATTENTION The maximum permissible viscosity is 30 mm2 s 5 3 Filling Notice Pay attention to the thermal expansion of bath oil during heating to avoid overflowing of the liquid Liquid level x Connect the tubing from the external system to the pump connectors and check for leaks x Check to make sure that the drain port 25 is closed x Remove the cap from the filling opening 9 x Fill the bath...

Page 26: ...nt for example Store and dispose of the used bath fluid according to the environmental protection laws 0 1 A x Turn the mains switch 1 off x Place a suitable vessel for accepting the used bath liquid underneath the drain x Unscrew the cup nut A from the drain port 25 and empty the unit completely x Close the drain port www calcert com sales calcert com 1 800 544 2843 0 5 10 15 20 25 30 ...

Page 27: ... X H X Version Switching on x Turn on the mains power switch 1 LThe unit performs a self test All segments of the 4 digit MULTI DISPLAY LED and all indicator lights will illuminate Then the order nomber Example 9501 051 03 P0H1 and the software version example n3 1 of the unit appears The display OFF or R OFF indicates the unit is ready to operate LThe recirculating cooler enters the operating mod...

Page 28: ...d by OFF or rOFF resp on the MULTI DISPLAY LED A complete shutdown of the main functional elements such as heater and circulation pump is effected simultaneously Should such a safety standard not be required the AUTOSTART function automatic start mode may be activated thus allowing the start of the circulator directly by pressing the mains power switch or using a timer Warning For supervised or un...

Page 29: ...ding to IEC 61010 2 010 and for the warning functions for high and low temperature and the conductivity limit are made in a menu that is called up with the key 8 1 Excess temperature protection C 10 30 60 130 180 220 This safety installation is independent of the control circuit When the temperature of the bath fluid has reached the safety temperature a complete shutdown of the heater cooling masc...

Page 30: ...ears Refill bath fluid 2 Switch in stage 2 recognizes a low fluid level If stage 2 of the low level protection device according to IEC 61010 2 010 is triggered a complete shutdown of the heater and circulating pump is effected A continuous alarm tone sounds and a message CODE 01 appears on the MULTI DISPLAY LED Turn off the unit with the mains switch refill bath fluid and turn the unit on again Im...

Page 31: ...unction to shutdown function 1 Press the key until the menu item or is displayed 2 Press enter to indicate the adjusted value on the MULTI DISPLAY LED digit blinks 3 Set value Use the cursor keys to move left or right on the display until the numeral you wish to change blinks Use the increase decrease arrows to change the selected numeral 0 1 2 3 9 4 Press enter to store the selected value Press t...

Page 32: ...for Setpoint 1 2 3 and also for t High and t Low see page 31 are automatically defered within the limit range 1 Press the key until the menu item or is displayed 2 Press enter to indicate the adjusted value on the MULTI DISPLAY LED digit blinks 3 Set value Use the cursor keys to move left or right on the display until the numeral you wish to change blinks Use the increase decrease arrows to change...

Page 33: ... a meassage appears on the MULTI DISPLAY LED t High t Low or x Setting Li 1 A complete shutdown of heater and circulating pump is effected An audible alarm continuous tone sounds and a message appears on the MULTI DISPLAY LED t High t Low or 1 Press the key until the menu item is displayed 2 Press enter to indicate the adjusted parameter on the MULTI DISPLAY LED digit blinks 3 Select the parameter...

Page 34: ...ned temperature value of the calibration point This value is automatically stored with Ctx and can be indicated for control purposes Ctx The Calibration value is determined with a temperature measuring device and stored under menu item Ctx Remote Baudrate Handshake Parity x Online communication with adjustable interface parameters XP Tn Tv x PID temperature control control parameters Reset x Facto...

Page 35: ...rculator and a defined measuring point in the bath tank because of physical properties Examples 1 point calibration C C T 1 T 3 point calibration C C T 1 T TT 1 Original curve Principle For ATC calibration in steady state the bath temperature at the location of the temperature sensor T M is determined at the respective adjusted working temperature This value is then set on the circulator in the me...

Page 36: ... 1 Calibration procedure Press and set the first temperature value under e g for example example 1st value 80 C 2 Wait until this temperature is maintained constant in the bath for about 5 minutes ATC status Factory setting YES 3 Call up the ATC menu Press the button until the menu item is displayed and press enter to switch to menu level 2 4 Adjusting menu item ATC Status Press enter and indicate...

Page 37: ...lue Press the button until the menu item is displayed and press enter to open the input window Read the value of TM on the temperature measuring device and enter the respective value Use the cursor keys to move left or right on the display until the numeral you wish to change blinks Use the increase decrease arrows to change the selected numeral 0 1 2 3 9 Press enter and the circulator also stores...

Page 38: ...ontrol via RS232 YES Continue Press to quit the menu The display changes from keypad control mode manual operation to remote control mode operation via personal computer 9 4 Interface Baud rate Handshake Parity Factory settings 4 8 kBauds 2 even Hardware handshake To allow communication of the circulator with a PC or a superordinated process control system take care the interface parameters of bot...

Page 39: ...rtional range Xp The proportional range is the range below the selected temperature value in which the control circuit reduces the heating power from 100 to 0 Setting range 1 9999 Resetting time Tn Integral component Compensation of the remaining control deviation due to proportional regulation An insufficient resetting time may cause instabilities to occur Excessive resetting time will unnecessar...

Page 40: ...ase arrows to change the selected numeral 0 1 2 3 9 4 Press enter to store the selected value Optimization instructions for the PID control parameters optimum setting C t The heat up curve reveals inappropriate control settings Inappropriate settings may produce the following heat up curves Xp too low C t Tv Tn too low C t Xp too high or Tv too high C t Tv Tn too high or Xp too high C t www calcer...

Page 41: ...in form of a code Warning without a complete shutdown of the unit The MULTI DISPLAY LED indicates the cause for the warning in form of a code and an acoustic signal sounds in regular intervals These messages appear every 10 seconds Press enter to quit the audible signal x The circulator is operated without bath fluid or the liquid level is insufficient Replenish the bath tank with the bath fluid x...

Page 42: ...rors x Error in A D converter x Excess temperature sensors defect x The excess temperature value lies below the working temperature setpoint Set the excess temperature to a higher value x Cable of the excess temperature sensor interrupted or short circuited x The early warning system for low level signals a critical fluid level Replenish the bath tank with the bath fluid After eliminating the malf...

Page 43: ...Pin assignments RS232 Pin 2 RxD Receive Data Pin 3 TxD Transmit Data Pin 5 0 V Signal GND Pin 7 RTS Request to send Pin 8 CTS Clear to send Pin 1 4 6 9 Reserved do not use Accessories Order No Description 8 980 073 RS232 interface cable 9 pol 9 pol 2 5 m 8 900 110 USB interface adapter cable Control connector Return flow safety device If the liquid levels in the recirculating cooler and the extern...

Page 44: ...culating cooler is now operated via the computer In general the computer master sends commands to the recirculating cooler slave The recirculating cooler sends data including error messages only when the computer sends a query In remote control mode After a power interruption the order to start and all values which have to be adjusted must be resent from the personal computer via the interface AUT...

Page 45: ...tpoint1 in_sp_00 Response from the circulator 55 5 LF 12 3 List of commands out commands Setting parameters or temperature values Command Parameter Response of circulator out_mode_05 0 Stop the unit R OFF out_mode_05 1 Start the unit out_sp_00 xxx xx Set working temperature t out_sp_03 xxx xx Set high temperature warning limit t High out_sp_04 xxx xx Set low temperature warning limit t Low out_sp_...

Page 46: ...sp_00 none Working temperature t 1 in_sp_03 none High temperature warning limit t High in_sp_04 none Low temperature warning limit t Low in_sp_07 none Pump pressure stage in_par_00 none Temperature difference between working sensor and safety sensor in_par_01 none Te Time constant of the external bath in_par_02 none Si Internal slope in_par_06 none Xp control parameter of the internal controller i...

Page 47: ...perature difference of more than 35 K 07 I2 C BUS ERROR Internal error when reading or writing the I2 C bus 08 INVALID COMMAND Invalid command 09 COMMAND NOT ALLOWED IN CURRENT OPERATING MODE Invalid command in current operating mode 10 VALUE TOO SMALL Entered value too small 11 VALUE TOO LARGE Entered value too large 12 TEMPERATURE MEASUREMENT ALARM Error in A D converter 13 WARNING VALUE EXCEEDS...

Page 48: ...possible in the conditions OFF R OFF or ALARM x Connect the circulator to the computer using an interface cable x Start the EasyBlackBox program The program asks for the port used COM1 and the baud rate of the unit You do not have this information on hand Simply try it out The program continues to send the request until the correct settings are made x Data is read out and shown on the monitor divi...

Page 49: ...sion water The recirculating cooler is designed for continuous operation under normal conditions Periodic maintenance is not required The tank should be filled only with a bath fluid recommended by JULABO To avoid contamination it is essential to change the bath fluid from time to time Repairs Before asking for a service technician or returning a JULABO instrument for repair please contact an auth...

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