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Hanna Instruments HI98198 OPDO, Instruction Manual, Page: 32 / 60

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Hanna Instruments HI98198 OPDO Instruction Manual Download Page 32

32

CALIBRA

TION

The probe has a built-in temperature sensor and the thermal transfer is made via the stainless steel 
contact located on the probe body. The contact point must be fully immersed in solution and in 
thermal equilibrium with the solution measured during calibration. The greater the difference between 
the temperatures at which the probe was stored and the temperature of the sample, the longer it 
will take to reach thermal equilibrium. When the probe is connected to the meter and the meter 
is powered, the temperature is displayed. Observe when temperature is stable before conducting a 
temperature calibration. A reference thermometer with 0.1 °C (or better) accuracy is suggested.

Note:

 Calibration data for temperature is stored in the probe memory.

Procedure

Remove the protective shield from probe. Place 

HI764113 

probe and the reference thermometer into 

a stirred container of water. Ensure the temperature contact on the probe is submerged in the water. 
Observe the temperature on display until it stops changing (this may take several minutes).
Press 

CAL

 from any measure mode (DO, BOD, OUR

 

or SOUR). The calibration menu will be displayed.

Press 

Temp

 to select the temperature calibration.

Use the   /   keys to set the calibration point values to that of the reference thermometer. When 
available, 

CFM

 will appear on the display.

Press 

CFM

 to complete the calibration.

To clear the user temperature calibration at any time, press 

CAL

 from any measure mode (DO, BOD, 

OUR

 

or SOUR). The calibration menu will be displayed. Press the 

Temp

 functional key then 

Clear

. The 

previous user calibration has been removed and the factory calibration restored.
Press 

ESC

 button at any time to escape from the calibration without changing values.

”CAL DUE” will be displayed and a probe calibration must follow.

Summary of Contents for HI98198 OPDO

Page 1: ...INSTRUCTION MANUAL HI98198 opdo Optical Dissolved Oxygen Meter ...

Page 2: ...osing a Hanna Instruments product Please read this instruction manual carefully before using this meter This manual will provide you with the necessary information for correct use of this meter as well as a precise idea of its versatility If you need additional technical information do not hesitate to e mail us at tech hannainst comorviewourworldwidecontactlistatwww hannainst com Dear Customer ...

Page 3: ...ION 26 9 2 PRESSURE CALIBRATION 30 9 3 TEMPERATURE CALIBRATION 31 10 GOOD LABORATORY PRACTICE GLP 33 11 MEASUREMENT 34 12 LOGGING 35 12 1 LOGGING THE CURRENT DATA 35 12 2 VIEW LOGGED DATA 35 13 RETRIEVING DATA 37 13 1 METER TO PC 37 13 2 METER TO USB DRIVE 37 14 DO MEASUREMENT 39 15 BOD MEASUREMENT 40 16 OUR MEASUREMENT 45 17 BATTERY REPLACEMENT 50 18 PROBE MAINTENANCE 51 19 TROUBLESHOOTING GUIDE ...

Page 4: ...ensor protectiveshieldand4m 13 4 cable HI764113 1 Smart Cap with o ring HI7040 Bicomponent Zero Oxygen Solution Calibration storage vessel 100 mL plastic beaker 2 pcs 6 g sachet with silicone grease Syringe Lens wipe 1 pc 1 5V AA batteries 4 pcs Instrument quality certificate Probe quality certificate DO Smart Cap quality certificate USB Type A to C cable Instruction manual Note Save all packing m...

Page 5: ...l calibration in mg L or saturation using a reference method for calibration value A dedicated HELP key for assistance anytime A user selectable Calibration due warning A dedicated GLP key that includes at last 5 calibrations with time date calibration points as well as barometric pressure temperature and salinity setting AutoEnd freezes the next stable measurement value on the display Log on dema...

Page 6: ...d Laboratory Practice information 7 CAL key to enter exit calibration menu 8 SETUP key to enter exit Setup menu 9 RCL key to enter exit view logged data mode RCL means RECALL 10 MODE key to switch between DO BOD OUR and SOUR applications 11 RANGE key to change between saturation or concentration in DO measurement mode 12 HELP key to enter exit contextual help 13 ESC key to leave current mode exit ...

Page 7: ... using a value entered by the user in saturation or mg L Temperature Calibration Single point anywhere within temperature range Pressure Calibration Single point anywhere within pressure range Temperature Compensation Automatic from 5 0 to 50 0 C 23 0 to 122 0 F Pressure Compensation Automatic from 420 to 850 mmHg Salinity Compensation Automatic from 0 to 70 PSU manually set DO Probe HI764113 Opti...

Page 8: ...nd 20 m 65 6 ft options Probe guard 316 Stainless Steel Temperature Measurement Thermistor Pressure 20 m 29 PSI Probe Dimensions with Guard 174 X 25 mm 6 8 X 1 Response Time t95 45 seconds Probe Weight with Guard 400 g 14 2 oz 4 m 13 1 ft cable length Probe Ingress Protection Rating IP68 Sensor type Optical Luminescence Quenching Origin Assembled in USA ...

Page 9: ... lifetime of the luminescence The lifetime of the luminescence is measured by a photodetector and is used to calculate the dissolved oxygen concentration This is in turn reported by the meter as a saturation or mg L reading of Dissolved Oxygen The major components of the probe include a blue LED for excitation a red LED that is used as a reference light and a photodetector The Smart Cap is locked ...

Page 10: ...ROBE COMPONENTS 1 Strain relief 2 ABS Probe body 3 Temperature Sensor 4 O ring Seal 5 Optical window 6 Alignment key 7 Smart Cap 8 RFID Tag 9 Embedded O2 sensitive luminophore with black protective layer 10 Protective shield ...

Page 11: ... guard from probe body if it was installed Use care not to leave fingerprints on the optical window 2 Remove the syringe plunger cut top off supplied sachet with silicone grease and empty contents into the syringe Using the syringe sparingly lubricate the o ring with a thin film of the supplied grease Avoid getting any kind of grease or fingerprints onto the optical window 3 Remove the HI764113 1 ...

Page 12: ...properly installed on the probe No conditioning period is required when using a HI764113 DO probe Store the HI764113 probe in the HI98198 carrying case when not in use For frequent use and short term storage it is recommended to remove the stainless steel guard and replace with the storage vessel that has a small amount of deionized water The probe can also be stored with the stainless steel guard...

Page 13: ...ample min delta DO The minimum diff between the start and the end DO val 0 00 to 50 00 mg L 0 00 mg L Sample min end DO The minimum end DO value 0 00 to 50 00 mg L 0 00 mg L Seed min delta DO The minimum diff between the start and the end DO val 0 00 to 50 00 mg L 0 00 mg L Seed min end DO The minimum end DO value 0 00 to 50 00 mg L 0 00 mg L OUR Configuration Min time The minimum time for the OUR...

Page 14: ... Enabled or Disabled Disabled Autodelete BOD start data Automatically delete BOD start data after BOD compute Enabled or Disabled Disabled Backlight Backlight Level 1 to 7 4 Contrast Contrast Level 0 to 20 10 Auto Light off Time backlight remains ON 1 5 10 30 minutes 1 Auto Power off Time until meter is powered OFF Disabled or 5 10 30 60 minutes 30 Date Time 01 01 2006 to 12 31 2099 00 00 to 23 59...

Page 15: ...mprove the accuracy during calibration and measurement Enter the salinity value to be close to the known salt level of the sample Seawater typically has a salinity of 35 and the oxygen solubility is 18 less as compared to fresh water at 25 C By entering the approximate salinity value the calibration and subsequent concentration measurement will be compensated to display the correct oxygen concentr...

Page 16: ...onvert and display pressure measurements in user selected units Automatic and Manual Pressure will utilize these units To change the pressure measurement unit highlight Pressure unit and press Modify Using keys highlight the desired pressure measurement unit Press Accept to confirm or ESC to exit without saving Temperature Unit Option C or F The HI98198 has the ability to convert and display tempe...

Page 17: ...every time the meter is calibrated and the CAL DUE status is triggered when the meter detects a calibration time out The CAL DUE tags will start blinking to warn the user that the meter should be recalibrated If the calibration timeout is changed e g to 20 days then the timer will be immediately reset Notes Before the DO calibration is cleared default values loaded the display always shows the CAL...

Page 18: ...l DO value for a sample If the final DO value is less than this value the meter will show a warning message when evaluating the BOD Range 0 00 to 50 00 mg L Seed min DO the minimum acceptable difference between the initial and final DO values for a seed sample If the difference is less than this value the meter will show a warning message when evaluating the BOD Range 0 00 to 50 00 mg L Seed min e...

Page 19: ...the test cannot be started Range 0 01 to 50 00 mg L Min end DO the minimum accepted DO value at the end of the test If the DO reading at the end of the OUR test is less than this value a warning message will be displayed Range 0 00 to 50 00 mg L Total volume the volume of the diluted mixture Range 0 1 to 300 0 mL Sample volume the volume of sample in the diluted mixture Range 0 1 to 300 0 mL SOUR ...

Page 20: ...art DO the minimum accepted DO value for starting the SOUR test If the DO reading is less than this value the test cannot be started Range 0 01 to 50 00 mg L Min end DO the minimum accepted DO value at the end of the test If the DO reading at the end of the SOUR test is less than this value a warning message will be displayed Range 0 00 to 50 00 mg L Total volume the volume of the diluted mixture ...

Page 21: ...nitial data records that were used in BOD result evaluation entering View initial BOD data mode Backlight Option 1 to 7 The display backlight can be adjusted to increase visibility in various lighting environments To adjust the backlight highlight Backlight and press Modify Use keys to change intensity then press Accept to confirm Press ESC to leave without changing Contrast Option 0 to 20 The dis...

Page 22: ...tomatically To change the duration highlight Auto Light OFF then press the desired functional key to change the option The backlight display setting should be set to the shortest time to preserve the battery life Auto Power OFF Option Disabled 5 10 30 or 60 minutes This selection can be used to preserve the battery life in the event that the meter is accidentally left on Highlight Auto Power OFF P...

Page 23: ...phasized values Press Accept to confirm the new settings or ESC to leave without changing Time Format Option AM PM or 24 hours Your desired time format may be selected in this parameter Highlight Time Format from Setup menu Press functional key to change the option Date Format Option DD MM YYYY MM DD YYYY YYYY MM DD YYYY MM DD Mon DD YYYY DD Mon YYYY YYY Mon DD Your desired date format may be sele...

Page 24: ...from the Setup menu and press the desired virtual key to make selection Beep On Option Enable or Disable This option allows the user to turn an acoustic warning signal on or off If enabled a short tone will occur to signal a condition is correct key press calibration or a long tone will occur when an incorrect key is pressed Disabling will silence audible signals Instrument ID Option 0000 to 9999 ...

Page 25: ...version pressure calibration date meter serial number as well as the battery capacity Highlight the Meter Info then press Select Probe Info This parameter displays probe and Smart Cap information Press Select to view cap information Press Next to view the Cap information Press Prev to return to first screen Press ESC to return to Setup Press ESC two times to return to Measurement ...

Page 26: ...atory tissue 5 Discard zero oxygen solution in an appropriate manner after use do not return to bottle Follow local disposal regulations 6 Confirm all water droplets have been removed from the cap surface as well as the temperature element before performing the calibration procedure in water saturated air Calibration of the HI764113 optical dissolved oxygen probe may be performed several different...

Page 27: ...por will become pressurized If using water verify the probe Smart Cap has not been moistened Wait a minimum of 15 minutes for the air to become saturated with water vapor Calibrating the probe over a large water surface such as a lake or aeration basin used in wastewater treatment should also suffice Air saturated water can be produced by bubbling air into a water sample for a prolonged period The...

Page 28: ...er and wait for the probe and sample to reach thermal equilibrium Press CAL The calibration menu will be displayed Press DO to select the DO calibration The meter will automatically recognize the 100 saturated standard or equivalent mg L The DO calibration screen will be displayed and the standard 100 saturation or 8 26 mg L depending on the currently selected measuring unit will be automatically ...

Page 29: ...elected When the reading is stable within the acceptable range the CFM functional key is displayed Press CFM to confirm the calibration point Remove probe from the standard and rinse it off completely in running water to remove all traces of zero standard Blot any water off the cap with a lint free tissue Suspend the probe into the water saturated air container and wait for the probe and sample to...

Page 30: ...Press CFM to confirm the calibration point The meter will return to the measurement screen and the probe will store the calibration data 9 2 PRESSURE CALIBRATION The HI98198 meter incorporates a pressure transducer that accurately tracks local barometric pressure Oxygen partial pressure is influenced by the local barometric pressure as dictated by Henry s Law The HI98198 automatically compensates ...

Page 31: ... the calibration data CAL DUE will be displayed and a probe calibration must follow To clear the pressure calibration and restore the factory one press CAL from any measure mode DO BOD OUR or SOUR The calibration menu will be displayed Press the Pressure functional key and then Clear The user calibration will be removed and the factory calibration restored Press ESC key at any time to exit the cal...

Page 32: ... shield from probe Place HI764113 probe and the reference thermometer into a stirred container of water Ensure the temperature contact on the probe is submerged in the water Observe the temperature on display until it stops changing this may take several minutes Press CAL from any measure mode DO BOD OUR or SOUR The calibration menu will be displayed Press Temp to select the temperature calibratio...

Page 33: ...Data from the last 5 DO calibrations are stored automatically after a successful calibration To view the last calibration data press GLP when the meter is in the DO BOD OUR or SOUR measurement mode The last calibration will appear at the top of the list The meter will display GLP data related to the calibration including calibration standards salinity pressure and temperature Use to scroll through...

Page 34: ...centration measurement is calculated for oxygen dissolved in water and is based upon air saturated water If measuring other fluids not water the mg L measurements will be in error In those cases the saturated reading should be used AutoEnd AutoEnd allows the user to display a measurement with a hold function This is useful when you are taking a measurement in a location where it might be difficult...

Page 35: ...urement press LOG key The meter will display for a couple of seconds the record number and the amount of free space in If the maximum number of stored measurements is achieved the Log space is full message will be displayed for a few seconds when LOG key is pressed Enter RCL mode and delete records in order to free log space 12 2 VIEW LOGGED DATA Press RCL to retrieve the stored data while in the ...

Page 36: ... Press CFM to delete record Press More to view more information of the selected record Press Pg Down to see additional information To export data to an USB drive or PC see the next sections If there is no logged data the meter will display No Records DO recall ...

Page 37: ...and can be opened with any text editor or spreadsheet program Field separator may be set as comma or semicolon depending upon region preferences see SETUP Note Western Europe ISO 88859 1 character set and English language are suggested settings Other files may be visible depending upon computer settings All files stored will appear in this folder Adjust Font or column width appropriately 13 2 METE...

Page 38: ...irmation of overwriting the existing file The message File exists OverWrite Press CFM for overwriting the existing file Note Do not remove the USB Flash Drive during the file transfer If the USB is not found the following screen will appear Try reseating USB drive and pressing Export again ...

Page 39: ...cordance with sampling protocols 5 When measuring across a temperature gradient i e the car is hot and the waters cool allow the probe to come thermal equilibrium with the water being sampled 6 The HI98198 with HI764113 have been designed for dissolved oxygen water quality measurements in urban and natural waters It may be used for discrete spot sampling using the meters Log on Demand function The...

Page 40: ...s The loss of dissolved oxygen in the sample once corrections have been made for the degree of dilution is called the BOD5 Before measuring BOD remember to set the BOD configuration from the Setup menu BOD Procedure DAY 0 CAL DO Go to Setup and configure BOD configuration parameter which sets up expected sample and seed concentrations Determine if you wish to save all BOD data or automatically del...

Page 41: ...en a new record is saved the meter will display a message indicating the remaining free BOD initial data space in Repeat procedure with additional samples Rinse off probe between samples Place the probe into the BOD sample and allow the measurement to stabilize The sample should be well mixed Follow all standard operating procedures Press Add new and complete BOD Parameters screen see above Press ...

Page 42: ...the keys to scroll the list of BOD initial data records The seed records will have the symbol displayed after the bottle ID Press More to view detailed information for the selected record Select the Bottle ID that is currently being measured by the probe and press EvalBOD The BOD will be calibrated Press RCL while in the BOD application BOD recall ...

Page 43: ...ct the desired seed BOD and then press Correct to compute the corrected BOD value The meter will display the corrected BOD value If the information about the BOD of a certain seed doesn t exist at the moment of the BOD evaluation for a seeded sample the sample s BOD can be corrected at a later time from the BOD recall menu view logged BOD data In order to perform a seed correction from the BOD rec...

Page 44: ...44 BOD MEASUREMENT Note Various error message will pop up if limits are exceeded Also if the final DO value is greater than the initial DO value an error message will be displayed ...

Page 45: ... test in seconds total volume sample volume Dilution factor of sample Before starting an OUR test remember to set the OUR configuration from the Setup menu This a an example of possible setting Follow your normal SOP Make sure the DO probe has been calibrated before using Clean off probe between samples Press MODE to select the OUR measurement mode Place the calibrated probe into the airtight cont...

Page 46: ...of this analysis To analyze another sample clean and dry off probe Place probe into the next prepared sample Press Start OURErrormessageswillbedisplayedanytimeameasurementexceedsthelimitsthatwereconfigured These will have to be reconfigured and the analysis restarted If the DO value is less than the minimum start DO value the meter will display an error message and the test cannot be started ...

Page 47: ...ure Correction The SOUR value is corrected to 20 C 68 F according to the Farrel and Bhide equation SOUR20 SOURTxΘ 20 T Where T is the measured temperature in C and Θ is a temperature dependent variable Θ 1 05 for T above 20 C Θ 1 07 for T below 20 C This calculation is valid only for temperature values in the range 10 to 30 C Temperature correction is performed only if the option SOUR 20 C is enab...

Page 48: ...DO value set during SOUR configuration a warning icon will be displayed and a beep will be heard every two seconds Press Stop to stop the test and the beeper In case that the SOUR value is corrected to 20 C 68 F and the measured temperature isn t in the range 10 to 30 C the temperature value will blink to alert that the temperature correction isn t valid Press LOG to save a complete set of data re...

Page 49: ...UREMENT Press Start to begin a new SOUR test or ESC to return to the SOUR measure screen SOUR recall Note In case that the SOUR value was corrected to 20 C the message 20 C will be displayed before the SOUR value ...

Page 50: ... 4 Insert four new 1 5V AA batteries in the battery compartment while paying attention to the correct polarity 5 Close the battery compartment using the four screws If the battery capacity is less than 10 the backlight feature is not available Note The meter is provided with the BEPS Battery Error Prevention System feature which automatically turns the meter off when the batteries level is too low...

Page 51: ... black protective layer on the Smart Cap will affect the calibration and measurement Replace the Smart Cap if the sensing surface has been compromised Cleaning the Smart Cap Use a mild detergent and a soft bristled toothbrush to clean the Smart Cap Rinse the cap with water after cleaning and dry with a laboratory tissue Yearly Replacement of the Smart Cap Easy to use smart caps contain pre loaded ...

Page 52: ...empty contents into the syringe Using the syringe sparingly lubricate the o ring with a thin film of the supplied grease Avoid getting any kind of grease or fingerprints onto the optical window Do not substitute other grease lubricants as it may cause the o ring to swell 7 Clean the lens with an unused portion of the supplied lens cleaner wipe 8 Remove the new optical cap from the box Align the no...

Page 53: ...frequent use and short term storage it is recommended to remove the stainless steel guard and replace with the storage vessel that has a small amount of deionized water The probe can also be stored with the stainless steel guard on in a beaker containing deionized water For longer term storage remove the stainless steel guard and replace with the storage vessel ...

Page 54: ...n connect the batteries Display shows No Cap Detected Cap not on correctly Check Cap Reseat Cap Display shows No Cap Info Detected with Cap Cannot read Cap Info Check Cap and Retry Replace Cap if it continues Display shows Cap Damaged Sensor Damaged Try reseating cap If this doesn t resolve issue replace Cap Display shows Cap Expired Cap reached lifetime use expiration Continue OR Replace Cap Cont...

Page 55: ... AA batteries 12 pcs HI764113 Optical DO probe with built in temperature sensor shield and 4 m 13 4 cable HI764113 1 Smart Cap with o ring HI764113 2 Calibration storage vessel HI764113 3 Stainless steel protective shield HI764113 10 HI764113 with 10 m cable HI764113 20 HI764113 with 20 m cable HI920016 USB Type A to C cable ...

Page 56: ...n contact your city your local household waste disposal service the place of purchase or go to www hannainst com RECOMMENDATIONS FOR USERS Before using this product make sure it is entirely suitable for your specific application and for the environment in which it is used Any variation introduced by the user to the supplied equipment may degrade the instrument s performance For your and the instru...

Page 57: ...nect the equipment into an outlet on a circuit different from that to which the receiver is connected Consult the dealer or an experienced radio TV technician for help WARRANTY HI98198 is warranted for two years against defects in workmanship and materials when used for its intended purpose and maintained according to instructions Electrodes and probes are warranted for a period of six months This...

Page 58: ...58 58 MAN98198 10 20 ...

Page 59: ...Hanna Instruments reserves the right to modify the design construction or appearance of its products without advance notice ...

Page 60: ...World Headquarters Hanna Instruments Inc Highland Industrial Park 584 Park East Drive Woonsocket RI 02895 USA www hannainst com MAN98198 Printed in ROMANIA ...

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