background image

35

34

Press 

LOG

 to memorize the current reading. A message indicating the free log space will be

displayed for a few seconds.

In order to take pH measurements follow the next steps:
• Submerge the pH bulb 2 cm (0,8’’) and the temperature probe into the sample to be tested

and stir gently. Allow time for the electrode to stabilize. When the reading becomes stable the

 (unstable measurement) symbol will disappear.

• If the pH reading is less then -2.00 pH or greater then 16.00 pH the closest full-scale value

(-2.00 pH or 16.00 pH) will be displayed blinking.

If measurements are taken successively in different samples, it is recommended to rinse the

electrodes thoroughly with deionized water or distilled water and then with some of the next
sample to prevent cross-contamination.
The pH measurement is affected by temperature. In order to have accurate pH measurements, the
temperature effect must be compensated for. To use the Automatic Temperature Compensation
(

ATC

) feature, connect and submerge the 

HI 7662-M

 temperature probe into the sample in the

dedicated tubeguide and wait for a few seconds. The 

“ATC”

 message will be shown on the

display. Automatic Temperature Compensation will provide pH corrected values at the temperature
of measurements. If Manual Temperature Compensation (

MTC

) is desired, the temperature probe

must be disconnected from the instrument. The default temperature of 25 °C (77 °F) or the last
temperature reading will be displayed preceded by the symbol   and the 

“MTC”

 message.

The manually set temperature can now be adjusted with the 

ARROW 

keys (from -20.0 to 120.0 °C).

pH MEASUREMENT

The 

HI 84430

 may be used as a pH meter for direct measurements.

Verify that the instrument has been calibrated before taking pH measurements. Set the instrument
to 

pH meter

. At power up the instrument enters 

pH meter

 mode. From titrator mode press ESC

until pH units are displayed.
If an electrode calibration hasn’t been performed, or the number of days exceedes calibration time
out value set, the message 

“CAL DUE”

 will blink on the left side of the display (see 

Calibration

timeout

 option in 

Setup 

for details).

If 

CAL DUE

 is displayed perform an electrode calibration.

Place calibrated pH electrode into electrode holder. Open the fill hole.
Rinse the pH tip with distilled or deionized water. Immerse the pH electrode (bottom 2 cm / 0.8”)

in the sample and stir gently for a few seconds.
For a faster response and to avoid cross-contamination of the samples, rinse the electrode tip

with a few drops of the solution to be tested, before taking measurements. Press LOG to record

sample pH in instrument pH log.
Press 

MENU

 to access the instrument’s menu.

Press 

HELP

 to view the contextual help, every time you need supplementary information. The help

is customized for every situation that can appear during instrument usage.
Press 

STIR

 to start/stop the stirrer.

Press 

Titrator

 to enter titrator mode.

Press 

CAL

 to access the calibration menu.

The pump 

GLP

 displays the Time and Date of the last pump calibration.

If a calibration hasn’t been performed the message 

“Not Calibrated”

 will be displayed.

Summary of Contents for HI 84430

Page 1: ...1 Instruction Manual HI 84430 TOTAL ACIDITY MINITITRATOR pH METER for Water Analysis www hannainst com...

Page 2: ...mail us at tech hannainst com This instrument is in compliance with directives TABLE OF CONTENTS PRELIMINARY EXAMINATION 4 GENERAL DESCRIPTION 4 SPECIFICATIONS 6 PRINCIPLE OF OPERATION 8 FUNCTIONAL AN...

Page 3: ...precipitates solids suspensions oils samples containing polyvalent cations aluminum iron manganese chromium may react slowly with the titrant causing a drifting end point To eliminate or diminish the...

Page 4: ...le acidity high range mg L 400 4000 mg L as CaCO3 meq L 8 80 meq L as CaCO3 Resolution Titratable acidity low range 0 1 mg L 0 1 meq L Titratable acidity high range 1mg L 1meq L Accuracy 5 of reading...

Page 5: ...than 3 7 only total acidity can be determined The HI 84430 utilizes two different titrant solutions to cover the entire measurement range The titrantsusedhavedifferentconcentrations appropriateforeach...

Page 6: ...titrator top Purge the titrant Calibrate the pump Prepare the sample Run a titration and log sample results 5 Functional key area 6 Indicates that the displayed value can be changed using ARROW keys 7...

Page 7: ...ut saving the new value pH resolution Options 0 1 0 01 Press the displayed function key in order to change the pH resolution Options C F Press the function key in order to change the temperature unit...

Page 8: ...es on the screen Press the function key to select this option Tutorial Option AM PM or 24 hours Press the functional key to select the new value Time format Press to highlight the value to be modified...

Page 9: ...ial link between the instrument and a PC Both must use the same setting Baud rate Option 0 to 9999 This option is used to set the instrument s ID The instrument ID is used while exchanging data with a...

Page 10: ...olution to be used for the first calibration point Put the first beaker with calibration buffer in the beaker holder Place the electrode holder on the top of the beaker and secure it by turning clockw...

Page 11: ...heck if the correct buffer has been used or regenerate the pH electrodes by following the Cleaning Procedure see the pH Cleaning Procedure section If necessary change the buffer or the electrode When...

Page 12: ...temperature reading is out of the defined temperature range of the buffer 0 to 45 C the Wrong Buffer Temperature error message will be displayed and the symbol C will blink on the display Calibration...

Page 13: ...key from the titrator main screen The purging stops automatically after 5 minutes To access the Purge key follow the next steps From the instrument main screen pH meter screen press Titrator function...

Page 14: ...he electrode holder on the top of the beaker and secure it by turning clockwise Immerse the pH electrode approximatively 2 cm 0 8 into the standard paying attention not to touch the stir bar Insert th...

Page 15: ...the beaker and secure it by turning clockwise Insert the temperature probe into the dedicated guide tube Immerse the pH electrode approximatively 2 cm 0 8 into the sample to be tested paying attention...

Page 16: ...t of range the symbol is displayed in front of the reading From the titrator main screen press Titration To enter titrator main screen from pH meter mode press Titrator and then Titration If the tutor...

Page 17: ...a calibration hasn t been performed the message Not Calibrated will be displayed If GLP pump is pressed one of the next screens is displayed Press Delete to enter record deleting mode Press Delete Al...

Page 18: ...ayed preceded by the symbol and the MTC message The manually set temperature can now be adjusted with the ARROW keys from 20 0 to 120 0 C pH MEASUREMENT The HI 84430 may be used as a pH meter for dire...

Page 19: ...to return to the previous screen without deleting If the pH log is empty the message No Records will be displayed VIEW DELETE RECORDED pH DATA To view or delete previously logged pH records press MEN...

Page 20: ...eference thermometer The unstable measurement symbol will be shown on the display until the reading becomes stable When the reading is stable and close to the selected calibration point the unstable m...

Page 21: ...he HI 92000 Windows compatible software optional HI 92000 also offers graphing and on line help features Data can be exported to the most popular spreadsheet programs for further analysis To connect y...

Page 22: ...arameters setting The answer string contains Instrument ID 4 chars Calibration alarm time out 2 chars Concentration unit 1 char 0 mg L 1 meq L Acidity type 1 char 0 Total LR 1 Total HR 2 Strong LR 3 S...

Page 23: ...o s p u s e t a u t c u l f g n i d a e R e s i o n n w o d d n a n o i t c n u j y t r i d d e g g o l C l e v e l e t y l o r t c e l e w o L s e d o r t c e l e H p e l b a l l i f e r y l n o n o...

Page 24: ...ake all necessary steps to correct interferences Any variation introduced by the user to the supplied equipment may degrade the instrument EMC performance To avoid damages or burns do not put the inst...

Page 25: ...l 210 823 5192 Fax 210 884 0210 Indonesia Tel 210 4584 2941 Fax 210 4584 2942 Japan Tel 03 3258 9565 Fax 03 3258 9567 Korea Tel 02 2278 5147 Fax 02 2264 1729 Malaysia Tel 603 5638 9940 Fax 603 5638 98...

Reviews: