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Hanna Instruments HI 3221, Instruction Manual

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PREPARATION PROCEDURE

Remove the electrode protective cap.
DO NOT BE ALARMED IF ANY SALT DEPOSITS ARE PRESENT. This is normal
with electrodes and they will disappear when rinsed with water.
During transport tiny bubbles of air may have formed inside the glass bulb.
The electrode cannot function properly under these conditions. These bubbles
can be removed by "shaking down" the electrode as you would do with a glass
thermometer.
If the bulb and/or junction are dry, soak the electrode in

HI 70300

Storage

Solution for at least one hour. Open the fill hole if refillable.

Not present in gel electrodes.

ELECTRODE CONDITIONING

ELECTRODE CONDITIONING

ELECTRODE CONDITIONING

ELECTRODE CONDITIONING

ELECTRODE CONDITIONING

& MAINTENANCE

& MAINTENANCE

& MAINTENANCE

& MAINTENANCE

& MAINTENANCE

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Summary of Contents for HI 3221

Page 1: ...1 Calibration Check pH mV ISE Temperature Bench Meters HI 3220 HI 3221 HI 3222 Instruction Manual www hannainst com...

Page 2: ...prescribed maintenance isnotcovered If service is required contact the dealer from whom you purchased the instrument If under warranty report the model number date of purchase serial number and the na...

Page 3: ...Calibration Time Out to remind when a new calibra tionisnecessary Hanna Instruments reserves the right to modify the design construction and appearance of its products without advance notice Remove th...

Page 4: ...type and unit selection capability for HI 3222 the ion change selection capability for HI 3221 and the ISE calibration in up to five calibration standard solutions make this instrument very useful for...

Page 5: ...tch between pH and mV range HI 3220 pH mV and ISE range HI 3221 7 HELP key to enter exit contextual help 8 CAL key to enter calibration mode 9 ESC to escape the current mode exit calibration setup hel...

Page 6: ...ttom of the display 6 RANGE key to switch between pH and mV range Ch1 ISE and mV range Ch2 7 HELP key to enter exit contextual help 8 CAL key to enter calibration mode 9 ESC to escape the current mode...

Page 7: ...ector 13 BNC electrode connector for channel two HI 3222 only 14 Temperature socket for channel two HI 3222 only 15 Reference electrode connector for channel two HI 3222 only 16 BNC electrode connecto...

Page 8: ...p m e T m o r f c i t a m o t u A r o l a u n a M F 0 8 4 2 o t 0 4 C 0 0 2 1 o t 0 0 2 e d o r t c e l E H p B 1 3 1 1 I H d e d u l c n i e b o r p e r u t a r e p m e T T 2 6 6 7 I H d e d u l c n...

Page 9: ...6 8 6 1 0 4 8 6 1 s r e f f u b m o t s u c 5 d n a n o i t a r b i l a C e p o l S 0 1 1 o t 0 8 m o r F n o i t a r b i l a C E S I s t n i o p o w t o t p U s n o i t u l o s d r a d n a t s 6 m p...

Page 10: ...i o p n o i t a r b i l a c t n i o p e v i f o t p U e l b a l i a v a s n o i t u l o s d r a d n a t s 6 m p p 0 0 0 0 1 0 0 0 1 0 0 1 0 1 1 1 0 n o i t a s n e p m o c e r u t a r e p m e T m o r...

Page 11: ...ecorrespondingreference input socket For temperature measurements and automatic temperature compensation connect the temperature probe to the appropriate socket HI 3222 two channels instrument use a p...

Page 12: ...H measurements temperature must be taken into consideration If the sample temperature is different from the temperature at which the pH electrode was kept allow a few minutes to reach thermal equilibr...

Page 13: ...time see Accessories section page61 RELATIVE mV MEASUREMENTS To enter Relative mV mode press Rel mV function key while in mV measure mentmode TherelativemVreadingwillbedisplayedalongwiththeAbsolute mV...

Page 14: ...E CALIBRATION for details page 25 Notes Whenthereadingisoutofrange thedisplaywillflashtheclosest full scalevalue The instrument will display on the primary LCD if it is not calibrated Perform at least...

Page 15: ...uetothe actual pH value at the temperature of measurement Use ARROW keys to change the value within a 1 00 pH window and then press Accept Press ESC to leave custom buffers value unchanged Press Confi...

Page 16: ...Confirm function key is displayed Press Confirm to confirm first point The calibrated value and the second expected buffer value is then dis played on the LCD Afterthefirstcalibrationpointisconfirmed...

Page 17: ...temperature probe approximately 3 cm 1 into a third buffer solution and stir gently The temperature probe should be close to the pH electrode If necessary press the ARROW keys to select a different bu...

Page 18: ...t will be added to the existing data and the slope is calculated The slopes between current buffer and nearest lower and higher buffers will be reevaluated Ifthe Offset optionisselected anelectrodeoff...

Page 19: ...alibration cannot be confirmed The pH reading is not close to the selected buffer Select another buffer using the ARROW keys or change the buffer Electrode Dirty Broken alternatively with Buffer Conta...

Page 20: ...ation Iftheexistingstoredcalibrationisfull fivecalibrationpoints afterconfirming the calibration point the instrument will ask which buffer will be replaced by current buffer On the Buffer line will b...

Page 21: ...it or to use custom buffers With these buffers it is possible to closely bracket the measurement range of interest and insure an accurate measurement The resolution of the meter must be set to 0 001...

Page 22: ...fter calibration The cond remains active until the end of the calibration day Note The electrode condition is evaluated only if current calibration includes at least two standard buffers CLEANELECTROD...

Page 23: ...7 2 9 2 1 0 1 0 8 2 1 0 2 8 6 8 6 1 0 0 4 8 8 6 3 0 7 2 2 9 6 0 0 1 2 6 2 1 5 2 7 7 8 6 1 1 0 4 6 8 6 1 0 7 8 1 9 1 0 0 1 5 4 2 1 0 3 6 8 8 6 1 2 0 4 5 8 6 0 0 7 4 1 9 6 9 9 9 2 2 1 5 3 5 9 9 6 1 3 0...

Page 24: ...the reading is stable in mV range and the Relative mV offset is inside the offset window 2000 mV the Confirm function key is displayed Press Confirm to confirm relative mV calibration The instrument w...

Page 25: ...been previously calibrated at least one point the will be displayed Poursmallquantitiesofthebuffersolutionsintocleanbeakers Ifpossible use plastic beakers to minimize any EMC interferences Foraccurat...

Page 26: ...ing is stable and close to the selected standard the Confirm function key is displayed Press Confirm to confirm calibration The calibrated value and the second expected standard value will be displaye...

Page 27: ...ferent standard value The tag will blink on the LCD until the reading is stable Whenthereadingisstableandclosetotheselected standard theConfirm function key is displayed Press Confirm to confirm calib...

Page 28: ...nconsistency between present and previous old calibration is detected Clear old calibration parameters and proceed calibration from the current point Theinstrumentwillkeepallconfirmedvaluesduringcurre...

Page 29: ...ctly 4 days after the last calibration However if at any moment the expiration value is changed e g to 5 days then the alarm will be immediately recalculated and appear 5 days after the last calibrati...

Page 30: ...automatically after a successful calibration To view the ISE calibration data press GLPfunction key while in ISE measure ment mode If GLP function key is not displayed press MENU key The instrument wi...

Page 31: ...nt 00 00to23 59 date time Time Format AM PMor24hours 24hours DateFormat DD MM YYYY YYYY MM DD MM DD YYYY YYYY MM DD YYYY MM DD MonDD YYYY DD Mon YYYY YYYY Mon DD Language Messagedisplay Uptofour Engli...

Page 32: ...Max 5buffers No pH setting pHResolution SetpHresolution 0 1 0 01 0 01 display 0 001 Viewcalibr Displaycalibration Enableordisabled Enable points pH points Displayoutofcalibr Enableordisable Enable ra...

Page 33: ...t item PressModify Use keys to change the intensity then press Accept to confirm Press ESC to leave without changing Contrast Focus on the Contrast item PressModify Use keys to change contrast then pr...

Page 34: ...sed values Press Accept to confirm new setting or ESC to leave without changing Time Format Focus on the Time Format item Press function key to change the option Date Format Focus on the Date Format i...

Page 35: ...ssages are displayed in English and Help is not available Temperature unit Focus on the Temperature unit item Press the displayed function key in order to change the temperature unit Beep On Focus on...

Page 36: ...memorized only when is stable If a specific interval is selected the reading is memorized at the start of the specificinterval AutoEnd stability Focus on AutoEnd item Pressoneofthedisplayedfunctionkey...

Page 37: ...the instrument ID Press Accept to confirm or ESC to exit without saving Baud Rate Focus on the Baud Rate item PressModify Use ARROW keys to select the desired communication baud Press Accept to confi...

Page 38: ...ed CAL DUE warning will be displayed the set number of days after calibration is over passed The meter informations are displayed firmwareversion language version mV and temperature factory calibratio...

Page 39: ...ers item PressModify Press Delete to delete focused buffer Press Add to add a new buffer to the list max 5 Press Modify to set custom buffer value Use ARROW keys to change the value Press Accept to co...

Page 40: ...t of Cal Range Warning Focus on the Out of Cal Range Warning item Press the displayed function key in order to change option If enabled the Out Cal Range message will be displayed if the pH reading is...

Page 41: ...the desired combination If None 59 16 is selected the slope of the probe can be changed by pressing Modifykey PressModify Use ARROW keys to change the slope Press Accept to confirm or ESC to exit Foc...

Page 42: ...ISE unit Focus on the ISE unit item PressModify Use ARROW key to select unit Press Accept to confirm selection or ESC to exit Note If the unit is changed or User is selected a warning message will be...

Page 43: ...readingintomemory pressLOGwhileinmeasurementmode Theinstrument willdisplayfor few seconds the record number and the amount of the free log space If the LOG space is full the Log space is full message...

Page 44: ...f the Recall function key is not displayedpressMENU key TheRecallselectionscreenisdisplayed Press the corresponding function key to view the records If Man Log is pressed the list of records is displa...

Page 45: ...onfirm to confirm or ESC to exit without deleting If AutoLog is pressed The lot information of the specific range are displayed Use the ARROW keys to scroll the lots Press the Delete All function key...

Page 46: ...he nearest Hanna Customer Service Center or follow the instructions below ENTER CALIBRATION MODE With the instrument off press and hold down the then power on the instrument Press either Ch 1 or Ch 2...

Page 47: ...he second expected calibrated point is displayed Immersethetemperatureprobeintothesecondvesselascloseaspossibleto the reference thermometer Allow a few seconds for the probe to stabilize Use the ARROW...

Page 48: ...esecondcalibrationpointof1800mVwillbe displayed Set 1800 0 mV on the simulator When the reading is stable and close to the selected calibration point the Confirm function key is displayed Press Confir...

Page 49: ...strument with any terminal program Use an USB cabletoconnecttheinstrumenttoaPC starttheterminalprogram and set the communication options as follows 8 N 1 no flow control COMMAND TYPES To send a comman...

Page 50: ...6 ASCII code character recognized command NAK is 21 ASCII code character unrecognized command CAN is 24 ASCII code character corrupted command COMMANDS REQUIRING AN ANSWER The instrument will answer f...

Page 51: ...esponding to the selected range 11 ASCII chars including sign and decimal point and exponent Secondary reading only when primary reading is not mV 7 ASCII chars including sign and decimal point Temper...

Page 52: ...tion data if available when x 1 HI 3221 or when x 2 HI 3222 which contains the number of calibrated standards 1 char the ion charge with sign 2 chars HI 3221 thecalibrationslope withsignanddecimalpoin...

Page 53: ...nt 9 ASCII characters whenx 1 HI3221 or when x 2 HI 3222 The electrode slope 6 ASCII chars The ion charge 2 chars The ISE unit 2 chars The short name of the selected language 3 chars NSLxy Requests th...

Page 54: ...uests all mV Rel mV Log on demand LODxIALLRequests all ISE Log on demand when x 1 HI 3221 or when x 2 HI 3222 The answer string for each record contains The logged mode 2 chars xx 10 pH range 0 001 re...

Page 55: ...ffset with sign and decimal point 7 chars not available for ISE Temperature probe presence 1 char Notes Err8 is sent if the instrument is not in measurement mode Err6 is sent if the requested range is...

Page 56: ...e electrode life is drastically reduced TEMPERATURE CORRELATION TEMPERATURE CORRELATION TEMPERATURE CORRELATION TEMPERATURE CORRELATION TEMPERATURE CORRELATION FOR FOR FOR FOR FOR p p p p pH SENSITIVE...

Page 57: ...cannot function properly under these conditions These bubbles canberemovedby shakingdown theelectrodeasyouwoulddowithaglass thermometer If the bulb and or junction are dry soak the electrode in HI 703...

Page 58: ...submersed STORAGEPROCEDURE To minimize clogging and assure a quick response time the glass bulb and the junction of pH electrode should be kept moist and not allowed to dry out Replace the solution i...

Page 59: ...c Soak in Hanna HI 7074 Inorganic Cleaning Solution for15minutes Oil grease Rinse with Hanna HI 7077 or HI 8077 Oil and Fat Cleaning Solution IMPORTANT After performing any of the cleaning procedures...

Page 60: ...a e l t a s w o h s y a l p s i D f o t n o r f n i l o b m y s g n i d a e r e r u t a r e p m e t r o r e d r o f o t u O e r u t a r e p m e t g n i s s i m e b o r p e b o r p e r u t a r e p m e...

Page 61: ...8 Buffer Solution in FDA approved bottle 500 mL HI 8010L pH 10 01 Buffer Solution in FDA approved bottle 500 mL ELECTRODE STORAGE SOLUTION HI 70300L Storage Solution 500 mL bottle HI 80300L Storage So...

Page 62: ...zing Pretreatment Solution 500 mL bottle ORP SOLUTIONS HI 7020L Test Solution 200 275 mV 500 mL bottle HI 7021L Test Solution 240 mV 500 mL bottle HI 7022L Test Solution 470 mV 500 mL bottle pH ELECTR...

Page 63: ...body singlejunction refillable combinationpHelectrode Use general purpose HI 1330B Glass body semimicro singlejunction refillable combinationpHelectrode Use laboratory vials HI 1331B Glass body semim...

Page 64: ...general purpose FC 100B Plastic body PVDF doublejunction refillable combinationpHelectrode Use general purpose for food industry FC 200B Plastic body PVDF openjunction conic Viscolene non refillable...

Page 65: ...very high humidity HI 1413B Glass body single junction flat tip Viscolene non refillable combination pH electrode Use surfacemeasurement ORP ELECTRODES HI 3131B Glass body refillable combination plat...

Page 66: ...Plastic electrode refilling pipet 20 pcs HI76404N Electrodeholder HI7662 T Stainless steel Temperature probe with 1 m 3 3 screened cable HI8427 pH and ORP electrode simulator with 1 m 3 3 coaxial cabl...

Page 67: ...static discharges Avoid touching this glass bulb at all times During operation ESD wrist straps should be worn to avoid possible damage to the electrode by electrostatic discharges Any variation intro...

Page 68: ...3258 9565 Fax 03 3258 9567 Korea Tel 02 2278 5147 Fax 02 2264 1729 Malaysia Tel 603 5638 9940 Fax 603 5638 9829 Singapore Tel 6296 7118 Fax 6291 6906 SouthAfrica Tel 011 615 6076 Fax 011 615 8582 Tai...

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