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35

Troubleshooting

Incorrect measurement 
values

Dampness inside the measuring probe/faulty 
sensor electronics 
Check the sensor electronics by using the test 
cartridge (

section 7.2 on page 37

). 

1

Select 
SENSOR-SETUP>DIAG/TEST>SERVICE>
TEST CARTRIDGE>Test cartridge
Ready? Press ENTER

2

Compare the displayed values with the guide 
values. The displayed values should be in the 
same range as the guide values below. Wait 
for stabilization before pressing ENTER:

NITRATE:
SIGNAL –237.0<(–226.2 mV)<–217.0
MESS 2263.6<(2274,4 mV)<2283.6
REF 2450.6<(2500.6 mV)<2550.6
ENTER 

CHLORIDE:
SIGNAL –10.0<(–2.9 mV)<10.0
MESS 2490.6<(2497.7 mV)<2510.6
REF 2450.6<(2500.6 mV)<2550.6
ENTER 

TEMPERATURE VALUES: 
TEMP 24.5<(24.8 ºC)<25.5/
76.1<(76.6ºF)<77.9
ENTER

3

If the test cartridge data are within range, the 
sensor electronics are functional:   
Test cartridge 
OK
ENTER

If the test cartridge data are not within this 
range or if the test cartridge check is not 
successful, contact our service or technical 
support department.

Unstable measurement 
values

Air bubbles, depth of immersion

Check the installation
Check the configuration of the cleaning unit

Dampness at the contacts of the sensor cartridge

Dry the contacts with a cloth or some paper.
Check the opaque gasket for damage and 
the correct position of the gasket.
Screw the locking ring on. 

Note: 

Use the cap of the storage container as 

a tool/screwing aid for the locking ring.

Sensor membrane damaged

Check installation/replace sensor cartridge

Reference element damaged

Check installation/replace sensor cartridge

Airbubbles underneath the membrane

Hold sensor cartridge in hand with 
membranes facing straight down and shake 
gently in a downward motion two times to 
remove air bubbles that may form 
underneath the membrane.

6.3.1 Troubleshooting during operation (continued)

Symptom

Possible cause

Corrective actions

Summary of Contents for NO3D sc

Page 1: ...DOC023 53 90140 NO3D sc Nitrate Sensor USER MANUAL 12 2008 Edition 1A HACH Company 2008 All rights reserved Printed in Germany...

Page 2: ...2...

Page 3: ...tup menu 20 4 6 Calibration 22 4 6 1 Sensor code calibration 22 4 6 2 Matrix correction overview 23 4 6 3 Matrix correction 24 4 6 3 1 MATX1 correction one point matrix correction 24 4 6 3 2 MATX1 CL...

Page 4: ...4 Table of Contents Section 10 Certification 43 Appendix A Modbus Register 45 Index 47...

Page 5: ...temperature Sensor 20 to 60 C 4 to 140 F Sensor cartridge 5 to 40 C 41 to 104 F Operating temperature Air 20 to 45 C 4 to 113 F Sample temperature 2 to 40 C 35 to 104 F Max flow velocity 4 m s Max sen...

Page 6: ...6 Specifications 1 1 Dimensions Figure 1 Stainless steel sensor dimensions...

Page 7: ...supplements points in the main text 2 1 2 Precautionary labels Read all labels and tags attached to the instrument Personal injury or damage to the instrument could occur if not observed A symbol if n...

Page 8: ...ncludes the ion selective electrodes for nitrate and chloride compensation electrode a pHD electrode used as a reference system and a temperature sensor for temperature compensation An optional cleani...

Page 9: ...ve direct contact with the process and therefore it is particularly stable against drift Ion selective electrodes have a special membrane to which only a specific type of ion can adhere As a result an...

Page 10: ...10 General Information...

Page 11: ...e cartridge into operation for maximum life of the sensor cartridge 2 Remove the cap of the storage container see Figure 6 on page 13 3 Take the sensor cartridge out of the storage container and remov...

Page 12: ...The sensor cartridge only fits correctly in the sensor adapter in one position Pay attention to the markings on the sensor cartridge and on the sensor adapter see Figure 8 on page 14 Figure 5 Storage...

Page 13: ...Note Without the opaque gasket damage of the sensor will occur 3 Align the markings on the sensor cartridge with the sensor adapter see Figure 8 on page 14 and connect the sensor cartridge into the s...

Page 14: ...or cartridge 1 Make sure that this end remains wet 2 Make sure that the contacts on this end stay dry Figure 8 Sensor assembly 1 Locking ring 4 Sensor adapter 2 Sensor cartridge 5 Sensor housing 3 Ali...

Page 15: ...lation Install the sensor where the sample that comes into contact with the sensor is representative of the entire process Position the sensor at least 200 mm 7 87 in from the tank wall When using a c...

Page 16: ...16 Installation Figure 10 Example of sensor installation with Rail Mount Kit...

Page 17: ...the connector opening in case the sensor must be removed Optional extension cables may be purchased to extend the sensor cable length 1 Unscrew the protective cap from the socket on the controller 2 I...

Page 18: ...18 Installation...

Page 19: ...confirm 4 Select CONFIGURE and confirm 5 Select EDIT NAME and edit the name Confirm or cancel to return to the Sensor Setup menu 4 3 Sensor data logging The sc controller provides a data log and an e...

Page 20: ...T NO3 N CONC Entry and display of the NO3 N reference value lab value or CAL CONFIG MATX2 2 point matrix correction see section 4 6 3 3 on page 25 CONC MEAS 1 Saving the currently measured measurement...

Page 21: ...IOUS CAL Selection of one of the last four matrix and value corrections performed or CAL CONFIG FACTORY CAL Selection of the preset sensor code DATE Date of last calibration SENSOR CODE Enter the sens...

Page 22: ...t to the process 4 6 1 Sensor code calibration When activating a new sensor cartridge or during initial calibration the sensor code must be entered The default sensor code is IIIIIIIIIIIIIIII all 16 I...

Page 23: ...c sensor Correction Option Application MATX1 The most commonly used Matrix correction It performs a 1 point matrix correction offset adjustment for nitrate 4 6 3 1 on page 24 MATX1 CL With the MATX1 C...

Page 24: ...the measured value is stable 4 Wait until the measured value is stable and confirm by pressing ENTER Drift should be 0 03 mg L The values for nitrate and chloride are saved 5 Immediately after saving...

Page 25: ...aboratory reference value for chloride and press ENTER to confirm Confirmation of the entered laboratory value activates the matrix correction 4 6 3 3 MATX2 correction 2nd point matrix correction Proc...

Page 26: ...EAS 1 and wait until the NO3 N and Cl values are stable drift should be 0 03 mg L 4 Press ENTER to confirm The value for nitrate and chloride are saved 5 Immediately after measuring take a water sampl...

Page 27: ...trations as far apart as possible 4 Select CAL CONFIG CALIBRATE VALUE CORR from the menu and press ENTER to confirm Enter the 3 noted values 5 1 NO3 N NO3D sc Enter the displayed NO3 N value for the 1...

Page 28: ...28 Operation...

Page 29: ...r and then carefully and evenly polish the coating away Important Note Only the LZY671 polishing paper supplied may be used 5 1 Maintenance schedule Maintenance task 30 days1 6 months Clean sensor2 x...

Page 30: ...of the old sensor cartridge and opaque gasket per applicable regulations 4 Ensure that the new opaque gasket is installed during every sensor cartridge replacement 5 Insert the new sensor cartridge i...

Page 31: ...31 Maintenance Figure 13 Replace the sensor cartridge 1 Locking ring 4 Sensor adapter 2 Sensor cartridge 5 Sensor housing 3 Markings 6 Opaque gasket...

Page 32: ...ill the container with drinking water or use the shipping boot solution NO DISTILLED WATER and ensure that the sensor cartridge remains wet Check the membranes and ensure they are still moist every 2...

Page 33: ...de mV value is out of measuring range pHD RANGE pHD reference value out of measuring range TEMP RANGE Temperature value out of measuring range NO CARTRIDGE No sensor cartridge connected Connect sensor...

Page 34: ...cleaning interval Sensor membrane damaged Check sensor installation replace sensor cartridge Reference element damaged Check sensor installation replace sensor cartridge NO3 mV RANGE Nitrate mV value...

Page 35: ...OK ENTER If the test cartridge data are not within this range or if the test cartridge check is not successful contact our service or technical support department Unstable measurement values Air bubb...

Page 36: ...se the previous calibration Clean or replace the sensor cartridge SLOPE Error in the last nitrate calibration sensor cartridge too old contaminated faulty Repeat the calibration Use the previous calib...

Page 37: ...it LZX914 99 12400 Stainless Steel Basin Edge Mounting LZX414 00 80000 High Output Air Blast compressor 115 V 50 Hz 6860003 High Output Air Blast compressor 230 V 50 Hz 6860103 Test cartridge 6188300...

Page 38: ...38 Spare Parts and Accessories...

Page 39: ...DK 2700 Br nsh j Tel 45 36 77 29 11 Fax 45 36 77 49 11 info hach lange dk www hach lange dk HACH LANGE AB Vinthundsv gen 159A SE 128 62 Sk ndal Tel 46 0 8 7 98 05 00 Fax 46 0 8 7 98 05 30 info hach l...

Page 40: ...tact information HACH LANGE MAROC SARLAU Villa 14 Rue 2 Casa Plaisance Quartier Racine Extension MA Casablanca 20000 T l 212 0 522 97 95 75 Fax 212 0 522 36 89 34 info maroc hach lange com www hach la...

Page 41: ...ural disaster labor unrest acts of war declared or undeclared terrorism civil strife or acts of any governmental jurisdiction Damage caused by misuse neglect accident or improper application or instal...

Page 42: ...s of repair replacement or refund of purchase price as stated above are the exclusive remedies for the breach of this warranty On the basis of strict liability or under any other legal theory in no ev...

Page 43: ...andard criterion B IEC 1000 4 5 EN 61000 4 5 Electromagnetic compatibility EMC Testing and measurement techniques Surge immunity test criterion B IEC 1000 4 6 EN 61000 4 6 Electromagnetic compatibilit...

Page 44: ...44 Certification...

Page 45: ...W P19 42 UNIT SELECT 40018 Unsigned Integer 1 R W U0 2 TEMP OFFSET C 40019 Float 2 R W 1 5 1 5 TEMP OFFSET F 40021 Float 2 R W 2 7 2 7 SENSOR NAME 40024 String 8 R W CAL CONFIG 40032 Unsigned Integer...

Page 46: ...t 2 R 500 500 TEMP CONC 2 40109 Float 2 R 0 45 OFFSET BY NITRATE 40111 Float 2 R 70 50 SLOPE NITRATE 40113 Float 2 R 20 150 OFFSET BY CHLORIDE 40115 Float 2 R 150 50 SLOPE CHLORIDE 40117 Float 2 R 20...

Page 47: ...22 Modbus 45 P Power supply 5 R Replacement of the sensor cartridge 29 Replacement parts 37 S Sensor Cleaning 29 Diagnostics menu 19 Installation 15 Settings menu 20 Setup 19 Unpacking 11 Sensor cart...

Page 48: ...48...

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