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取扱説明書

取扱説明書

N-1300 Series

R03

Instruction Manual

取扱説明書

Instruction Manual

Rotary 
Vacuum

Evaporator

This instruction manual is designed to use the product safely while keeping its best 

performance.

Please keep this manual in a place easily accessible to every user.

IMPORTANT

Be sure to read “Safety precautions” before use.

Tokyo Rikakikai Co., Ltd.

Summary of Contents for N-1300 Series

Page 1: ...ual Rotary Vacuum Evaporator This instruction manual is designed to use the product safely while keeping its best performance Please keep this manual in a place easily accessible to every user IMPORTANT Be sure to read Safety precautions before use Tokyo Rikakikai Co Ltd ...

Page 2: ...e set gray 12 Screw plug 13 Cooler clamp 14 Cooler support bar 15 Support bar clamp 8 Rotary joint ring Rotary joint ring Ball joint clamp Eyela clip Screw plug For V type 5 Vacuum seal 1 1 2 AC adopter 1 Vacuum seal Sub seal Main seal 9 Adaptor S type 1 1 set 1 1 1 1 1 2 sets 1 V type 1 1 set 1 1 1 1 1 2 sets 1 1 1 1 1 E type 1 1 set 1 1 1 1 1 1 1 1 1 1 1 1 1 16 Set screw 3 3 Set screw 1 3 Power ...

Page 3: ...own slowly and gently while watching how deep it is soaked and fix at the correct position Caution Rotating part Be cautions high liquid temperatures bring the risk of burns Do not touch the specimen flask or the bath when you use the product at a high liquid temperature Also take care for the rotation speed of the flask for possible splashing and burning depending on the rotation speed Do not put...

Page 4: ...dimensions Highest position mm 672W 342D 504 684 H 479W 342D 823 1003 H 514W 342D 645 825 H Mass 8 2kg 8 9kg 8 8kg Power input 1 1A 110VA Rated power supply AC100V 240V 50 60Hz 2 2 2 Specifications This product is a rotary evaporator that is used for condensation purification and fractional distillation of solutions under reduced pressure Take care for conditions and handling of glass parts Broken...

Page 5: ...er Power cord 3 Power jack for vacuum controller Dedicated for model NVC 3000 Base adjuster 2 3 Names of parts Capillary feed tube Continuous specimen supply port Cooler Ball joint clamp Eyela clip Receiver flask Stand base Drive unit Angle adjusting knob bolt Specimen flask Vacuum nozzle white Coolant nozzle gray ...

Page 6: ...all joint clamp Eyela clip Receiver flask Stand base Drive unit Angle adjusting knob bolt Specimen flask Screw plug Cooler clamp Cooler support bar AC adaptor Power unit holder Signal connector for vacuum controller Power cord Power jack for vacuum controller Dedicated for model NVC 3000 Base adjuster Vacuum nozzle white Coolant nozzle gray ...

Page 7: ...all joint clamp Eyela clip Receiver flask Stand base Drive unit Angle adjusting knob bolt Specimen flask Screw plug Cooler clamp Cooler support bar AC adaptor Power unit holder Signal connector for vacuum controller Power cord Power jack for vacuum controller Dedicated for model NVC 3000 Base adjuster Vacuum nozzle white Coolant nozzle gray ...

Page 8: ...ame Display Causes Operation Abnormal rotation alarm 1 Measured number of rotation has not reached or is considerable below the setting The motor or the control assembly is malfunctioning A19 flashes Control stops Power outage recovery alarm When the power outage recovery function is OFF Displayed alternately The power was shut off during rotation due to power outage and then turned on again You c...

Page 9: ...ina 220 240V Power code B type 267695 Approx 2 0m Approx 5 6mm 0 75mm2 AWG18 U K India 220 240V Power code C type 267697 Approx 2 0m Approx 5 6mm 0 75mm2 AWG18 Europe Never use a branching socket or a table tap for connecting to the power supply 4 1 Installation environment Select a place that meets the conditions below for installing this product Never install the product in a potentially hazardo...

Page 10: ...y the brake to engage the lock 2 Raise the jack turn the jack handle clockwise to engage the lock 2 Adjusting the base adjuster Control case assembly Base adjuster LOCK FREE Down Up When using the unit in the reverse side specification the specimen flask is at the left follow the procedures in 6 Changing to the reverse side specification on P 13 Reverse side specification Because the upward force ...

Page 11: ...ck Sleeve ring spring inside Rotary joint ring Flask removal screw 4 Installing the vacuum seal Wrong orders or direction in installation of the main seal or the sub seal will degrade vacuum level or accelerate wear of the seal Main seal Spring side Rotary joint Sub seal Teflon seal optional Spring side 1 Insert the main seal with its side with the spring visible at the body side through the rotar...

Page 12: ...d tube Coolant nozzle gray Vacuum nozzle white Set screw Housing Rotary joint Eyela clip Specimen flask Receiver flask Ball joint clamp 1 Allow the cooler to tightly contact against the vacuum seal in the housing and then tighten with the cap screw When you have tighten to some extent re tighten both the cap screw and the cooler at the same time and position the receiver flask so that its fixing o...

Page 13: ...the jack is raised during setting work a personal injury may result Caution Take care for conditions and handling of glass parts Broken or flowed glass parts may result in accidents Inspect for damages or flows on glass parts and take care when handling them 5 Fix the receiver flask to the cooler with the ball joint clamp 6 Fix the specimen flask to the rotary joint with the Eyela clip 7 Gently in...

Page 14: ... the hole of the support bar clamp with the set screw Adjust the position after setting a glass part 2 Allow the adopter to tightly contact against the vacuum seal in the housing and then tighten with the cap screw When you have tighten to some extent re tighten both the cap screw and the adopter at the same time and position the receiver flask so that its fixing opening faces downward 3 Install t...

Page 15: ...ing assembly and the jack 3 Install the support bar clamp into the motor cover fixing screw hole with the set screw 4 Securely tighten the angle adjusting knob bolt For the reverse direction specification change the driving assembly in the reversed direction before installation Raise the jack before setting the support bar clamp First raise the jack before setting the support bar clamp If the jack...

Page 16: ...ecting hose through the hose holder Allow the coolant to circulated from the outside of the corrugated tube 8 Adjusting the angle of the drive body Adjust the angle of the drive body while holding the cooler with hand When you loosen the angle adjusting knob bolt the drive may suddenly incline from the weight of the cooler or specimen and fall down and you might be injured with broken glass Cautio...

Page 17: ... OSB 2200 or a power outlet AC adapter Plug Power jack Connector Power cord Power plug Power unit holder You can connect disconnect the hose using the optional fingertip connecter 9 2 Connecting the fingertip cooling hose optional Coolant nozzle Fingertip connector Fingertip connector optional Relief sleeve Fingertip cooling hose optional Fingertip hose nozzle I D 10mm optional The connecting hose...

Page 18: ...men on the unit If any specimen is spilt on the body or on the bath immediately wipe it out Some types of specimen may be ignited with heat of the body or the bath Warning Take care for conditions and handling of glass parts Broken or flowed glass parts may result in accidents Inspect for damages or flows on glass parts and take care when handling them Continuous specimen supply port Capillary fee...

Page 19: ...s rot and setting of the rotation mode is enabled 3 Turn the dial key to select one of Positive Negative Time reversal lamps Press the dial key once to switch to the display of the measured number of rotations normal stop status Both the TIME lamp and the rotation direction lamp come on when setting the timer reversal mode 4 To set the power outage recovery mode press the dial key for 5 seconds or...

Page 20: ...p and the positive rotation lamp come on Follow the procedures in Setting the rotation mode and the power outage recovery mode on P 17 to set to the timer reversal mode 2 Press the dial key once The display indicates flashing 20 or the number of rotations in the previous session and you can enter a number of rotations The number of rotations is 20rpm at the factory shipping 3 Turn the dial key to ...

Page 21: ...nd then set it Activate the decompressing unit to start decompression in the evaporator Slowly lower the jack to put the specimen flask in the bath Press the Run Stop key The specimen flask will rotate Follow the procedures in 2 Inputting a number of rotation and 3 Inputting the timer reversal mode on P 18 1 Press Run Stop key to stop rotation gently raise the jack and then take out the specimen f...

Page 22: ...ly stop operation and contact your dealer or the nearest service center The motor is malfunctioning The pulley and the belt are worn Strange noise is heard during rotation The vacuum seal is worn Replace the vacuum seal The lock sleeve light blue that tightens and fixes the rotary joint has loosened Turn the lock sleeve light blue clockwise while holding the lock housing black to tighten securely ...

Page 23: ...enter Power outage recovery alarm at OFF PoF 0 is displayed alternately and rotation will stop Power shut off during rotation and then recovered You can clear the indication by pressing the dial key The alarm display can also be cleared by resuming rotation by pressing the RUN STOP key Power outage recovery alarm at ON Pon Number of measured rotations is displayed alternately during rotation Power...

Page 24: ...eve ring spring 6 While securely inserting the rotary joint turn the lock sleeve light blue clockwise to securely tighten The internal sleeve ring spring will tighten and the rotary joint is secured Sleeve ring spring Name Standard Code No Rotary joint 272mm TS29 38 142500 Rotary joint 178mm TS29 38 142520 Vacuum seal For N NE 142610 Nozzle packing 12 For N NE 142691 Sleeve ring spring For N 1300 ...

Page 25: ...g 514 W 342 D 645 H Components Major materials Main unit stand base Aluminum Main unit jack assembly Aluminum iron stainless steel PBT GF POM PA6 Glass part Glass stainless steel PP PA6 8 Disposal of Products Disposal of product or part must be done according to the specified disposal method Principal components parts and disposal method We ask you to discard packing materials after classifying th...

Page 26: ...k first by referring to the page on troubleshooting to see if this is actually a trouble 2 If the product remains unsatisfactory even after checking contact the shop from which the user has purchased the product or the service center described in the manual and request repair 4 After expiration of the guarantee period the charged repair will be made at the customer s request ...

Page 27: ...8 264 0 91 8 46 6 88 2 204 0 94 2 159 2 77 3 162 6 134 4 540 0 120 4 80 3 98 6 68 7 141 3 96 8 97 8 50 0 116 0 77 6 120 6 81 9 82 9 100 8 770 678 598 571 532 412 332 306 279 266 159 199 159 129 80 126 57 111 27 21 32 53 41 45 33 9 19 8 24 4 16 4 12 9 10 Atomo p 931 705 678 452 519 399 359 346 332 199 239 173 159 102 159 77 146 36 29 43 70 55 59 40 13 27 12 31 7 19 5 15 12 13 Atomo p Atomo p Atomo ...

Page 28: ... 2 3 4 31 30 29 17 18 19 20 36 38 12 43 1 35 7 8 9 1 1 1 1 2 2 2 2 24 TS29 TS24 2 3 4 31 30 7 8 9 29 28 27 28 25 26 16 17 14 13 21 18 19 20 36 37 23 2 38 43 10 11 19 20 36 15 22 16 17 37 23 2 38 10 11 43 6 6 39 40 39 40 18 39 40 32 33 32 33 34 34 List of Consumable and Replacement parts Optional parts 11 1 2 2 ...

Page 29: ...Mauin Flask removal screw Lock sleeve light blue Sleeve ring spring 2 267620 For N 1300 1 3 267630 For N 1300 1 15 1 268870 Standard 15 2 268880 Chemical coating゙ 10 116340 S35 20 1 11 202790 S35 1 18 142690 For N NE 3 sets Rotary joint for V E types Code No Std total length Transparent edging type Coe No Std total length Thick type Code No Std total length Standard Rotary joint for S type Code No...

Page 30: ... North America 31 267699 For N 1300 1 Cooler support bar 19 178900 For N NE 2 sets Airtight stopper for E cooler 22 255830 GL25 1 AC power adaptor 30 267680 For N 1300 1 35 36 37 38 Teflon seal optional 35 244980 N 1200 1 33 267695 For N 1300 1 AC power cord 230V B type U K India 34 267697 For N 1300 1 AC power cord 230V C type Europe AC power cord 220V O type China 32 267698 For N 1300 1 Coolant ...

Page 31: ... No Std Q ty No Code No Std Q ty Condensation prevention cover 43 1 270730 For S 1 44 269480 For N 1300 1 43 44 45 46 45 269490 For N 1300 1 46 269450 For N 1300 1 No Code No Std Q ty No Code No Std Q ty No Code No Std Q ty No Code No Std Q ty 47 269390 For N 1300 1 46 47 44 45 Fixing plate for PBX NVC 3000 Fixing plate for NVC 3000 Communication cable COM 0 5m Connecting cable NVC PBX NP0 5m Vacu...

Page 32: ...S35 20 JIS std Chemical coating 1L 116380 228450 500mL 116370 228440 500mL 116850 116860 156610 156630 156640 300mL 116800 116810 156650 116820 116830 156660 116840 200mL 116750 116760 156680 116770 116780 156690 116790 100mL 116700 116710 156700 116720 116730 156710 116740 Std Code No TS29 38 TS24 40 29 38 24 40 19 33 15 30 24 40 19 33 15 30 500mL 228890 228900 228910 228920 228930 300mL 228820 2...

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