©
2012 - 2017
EL-CELL GmbH
Electrochemical Test Cell
ECC-Press-Air (-DL)
User Manual
Release: 1.5
2017-06-12
Page 1: ...2012 2017 EL CELL GmbH Electrochemical Test Cell ECC Press Air DL User Manual Release 1 5 2017 06 12...
Page 2: ...se or application of this product Content 1 Product Description 3 2 Features and Specification 3 3 Safety Precautions 7 4 Unpacking 7 5 Cell Assembly 8 6 Operation Modes Gas Supply 11 7 Electrical Con...
Page 3: ...draw gas samples from the cell s headspace The cell hardware is based on the ECC Std and ECC Ref test cells and can be used with or without a reference electrode The ECC Press Air comes with a control...
Page 4: ...um port for drawing gas samples by means of a syringe Attached pressure sensor for monitoring of inside gas pressure Default pressure range of 0 to 2 5 bar absolute Conditioning electronics with analo...
Page 5: ...eliable electrolyte filling upon assembly Fast assembly and dismantling and easy cleaning of cell components Electrodes are easily accessible for post mortem analysis Reusable cell components except f...
Page 6: ...ssure and temperature Resolution of pressure analog output 0 05 of measurement range Error of pressure analog output 0 5 of measurement range comprising non linearity including hysteresis and non repr...
Page 7: ...or damaged NOTE Damaged shipments must remain with the original packaging for freight company inspection List of Components 1 ECC Press Air test cell with pressure sensor assembled for use in a 2 elec...
Page 8: ...ed to the cell lid For this purpose plug the siphon into the cell lid with the siphon side bore pointing to the gas outlet port in the lid Then attach the tube transfer line to the gas outlet port so...
Page 9: ...disc 18 mm diameter approx 0 2 mm thick on top of the cell stack ix Push the cell base over the assembly hold the components tightly together and turn the assembly back into the upright position x Re...
Page 10: ...6 2017 Lid with 2mm banana jacks Wing Nut Siphon Connection line to pressure sensor Gas inlet or gas sample port valve Locking ring Piston PE seal REF sleeve Cell base with 2mm banana jacks Spring Cel...
Page 11: ...n this configuration the gas outlet at the sensor adapter is plugged and the test cell is pressurized at the beginning of the experiment through the attached sample valve port After equilibration of t...
Page 12: ...e signals are available at the Analog Out connector of the controller box These signals can either be routed to the analog inputs of the controlling potentiostat if available or to some other recordin...
Page 13: ...d on the PTFE ferrule and is thus preventing any bleeding from inside the cell through the septum In order to draw a gas sample i pierce the septum with the sample syringe ii open the valve by turning...
Page 14: ...and close down all active programs c On the installation CD run X setup This will install the EC Link data logger software Follow any instructions that may appear on your screen d Once installation i...
Page 15: ...Biologic potentiostat MPG 2 SP VSP and VMP series is described as an example The Biologic potentiostats feature two analog inputs that are used here to record both pressure and temperature 1 Connect...
Page 16: ...other appropriate solvents Ultrasonic cleaning is recommended Persistent dirt on the cell base and plunger may be removed by treatment with aqueous nitric acid 20 2 hours at room temperature All part...
Page 17: ...Page 17 of 23 Manual_ECC_PRESS_AIR_Release 1 5 docx 13 06 2017 12 Accessories and Spare Parts ECC Press Air DL complete...
Page 18: ...Page 18 of 23 Manual_ECC_PRESS_AIR_Release 1 5 docx 13 06 2017 Test Cell assembled as 3 electrode cell...
Page 19: ...Page 19 of 23 Manual_ECC_PRESS_AIR_Release 1 5 docx 13 06 2017 Gas sample port assy ECC1 00 0155 A...
Page 20: ...Page 20 of 23 Manual_ECC_PRESS_AIR_Release 1 5 docx 13 06 2017 Reference pin assy ECC1 00 0010 D...
Page 21: ...D M9 connector to auxiliary input connector of the Biologic potentiostat The cable shield is tied to both connector housings Part No ECE1 00 0040 B Pin Signal Cable Color Comments 1 V1 Red Red plug 2...
Page 22: ...GmbH for repair 1 Send an e mail to info el cell com to obtain a return authorization number and a decontamination report form 2 Sign the decontamination report asserting that the instrument has been...
Page 23: ...able care modification or the attachment of improper devices to the goods This Limited Warranty does not cover expendable items This warranty is void when repairs are performed by a non authorized per...
