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Buchi HydrolEx H-506, Operation Manual

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5 | Installation

BÜCHI Labortechnik AG

18/30

Operation Manual HydrolEx H-506

Precondition:

R

The suction tube is assembled. See Chap-
ter 5.5 "Assembling the suction tube", page 16

u

Moisten the rubber coupling with water.

u

Slip over the rubber coupling on the suction
tube.

u

Make sure that the rubber coupling is in the
correct position.

ð

The rubber coupling is assembled.

u

Assemble all rubber couplings in the same
way.

Summary of Contents for HydrolEx H-506

Page 1: ...HydrolEx H 506 Operation Manual 11593968 B en...

Page 2: ...ht to make changes to the manual as deemed necessary in the light of experi ence especially with respect to structure illustrations and technical details This manual is copyrighted Information from it...

Page 3: ...1 Principle of hydrolysis 10 3 2 Configuration 11 3 2 1 Front view 11 3 2 2 Rear view 12 3 3 Type plate 12 3 4 Scope of delivery 12 3 5 Technical data 12 3 5 1 HydrolEx H 506 12 3 5 2 Ambient conditio...

Page 4: ...Regular maintenance work 23 8 Help with faults 25 8 1 Troubleshooting 25 9 Taking out of service and disposal 27 9 1 Disposal 27 9 2 Taking out of service 27 9 3 Returning the instrument 27 10 Appendi...

Page 5: ...ere are four danger levels each identifiable by the signal word used Signal word Meaning DANGER Indicates a danger with a high level of risk which could result in death or serious injury if not preven...

Page 6: ...this Dialog Dialogs are marked up like this Button Buttons are marked up like this Field names Field names are marked up like this Menu Menu item Menus or menu items are marked up like this Status Sta...

Page 7: ...ied laboratory staff These operating instructions are aimed at the following target groups Users Users are persons that meet the following criteria They have been instructed in the use of the device T...

Page 8: ...ual serve to alert the user to these residual dangers 2 5 1 Hot surfaces The surfaces of the device can become very hot If touched they can cause skin burns u Do not touch hot surfaces or else wear su...

Page 9: ...ending on the application hazards due to heat and or corrosive chemicals may arise u Always wear appropriate personal protective equipment such as safety goggles protective clothing and gloves u Make...

Page 10: ...xes in yeast eggs etc For fat determination including acid hydrolysis such as the method according to Weibull Stoldt in food and animal feed the product is to be hydrolyzed to make the fat accessible...

Page 11: ...nfiguration 3 2 1 Front view 9 8 7 5 6 10 11 12 4 3 2 1 Fig 2 Front view 1 Sample aspiration tube 2 Lift device 3 Rinsing funnel 4 Rack 5 Hydrolysis vessel 6 Upper insulation plate 7 Lever 8 Power reg...

Page 12: ...in strument 3 4 Scope of delivery NOTE The scope of delivery depends of the configuration of the purchase order Accessories are delivered as per the purchase order order confirmation and deliv ery no...

Page 13: ...1200 W Number of hydrolysis posi tions 6 6 Approvals CE CSA CE CSA 3 5 2 Ambient conditions For indoor use only Max altitude above sea level 2000 m Ambient temperature 5 40 C Maximum relative humidit...

Page 14: ...glass components for damage u Damage that has occurred in transit should be reported to the carrier u Keep packaging for future transportation 4 2 Storage u Make sure that the ambient conditions are...

Page 15: ...p only when using a water jet pump NOTE Make sure that the power supply can be disconnected at any time in an emergency 5 3 Establishing electrical connections NOTE Observe the regulatory provisions w...

Page 16: ...sure that they match the specifica tions on the type plate u Make sure that all connected devices are grounded u Make sure that the power plug is freely accessible at all times u Insert the power cab...

Page 17: ...ies page 29 Waterjet pumpt see Chapter 10 1 2 Accessories page 29 Precondition R The suction tube is assembled See Chap ter 5 5 Assembling the suction tube page 16 u Moisten the vacuum tube with water...

Page 18: ...e is assembled See Chap ter 5 5 Assembling the suction tube page 16 u Moisten the rubber coupling with water u Slip over the rubber coupling on the suction tube u Make sure that the rubber coupling is...

Page 19: ...ip over the top rubber coupling on the sam ple aspiration tube u Make sure that the upper rubber coupling is in the correct position The sample aspiration tube is assembled u Assemble all upper rubber...

Page 20: ...ls of the hydrolysis vessel with 50 mL 4 M HCl NOTE Use quartz sand with a grain size of 0 3 0 9 mm 4 In case the grain size is too small it will clog the frit of the glass sample tube 4 In case the g...

Page 21: ...ondition R All installations are done See Chapter 5 Installation page 15 R The samples are prepared R The sample aspiration tube is assembled See Chapter 6 1 Assembling the sam ple aspiration tube pag...

Page 22: ...vessel is completely transferred u Repeat the rinsing step of the hydrolysis vessel three times u Remove the sample aspiration tube u Remove the glass sample tube from the rubber coupling u Perform a...

Page 23: ...the glass parts with commer cially available cleaning agents u If heavily soiled use ethanol or a mild detergent u WARNING Do not clean the glass sample tube with frit in an ultra sonic bath u Dry th...

Page 24: ...servicing B CHI Labortechnik AG 24 30 Operation Manual HydrolEx H 506 Component Action Frequency Control panel u Wipe down the display with a damp cloth Monthly Rubber couplings u Replace the rubber c...

Page 25: ...re connected properly u Make sure that the glass parts are not cracked or broken u Make sure that the hose is not por ous u Make sure that the water jet pump or vacuum pump is switched on u Close the...

Page 26: ...em Action Breakage hydrolysis vessel Precondition R WARNING Wear gloves during carrying out the following instruc tions u Let the temperature of the instrument decrease until it is the same as the amb...

Page 27: ...lations and statutory require ments regarding waste disposal u When disposing observe the disposal regulations of the materials used Materials used see Chapter 3 5 Technical data page 12 9 2 Taking ou...

Page 28: ...with the prior written permission of BUCHI 10 1 1 Spare parts Order no Image Insulation plate 11065169 Suction tube cpl 11064546 Set of hydrolysis vessels 2 pcs 11064547 Set of aspiration tubes 2 pcs...

Page 29: ...ass sample tubes PTFE 11067220 Holder for glass sample tubes stainless steel 11067219 Weighing support for hydrolysis vessels 11067040 Hydrolysis vessel carrier 11067492 Adapter clips for B 411 sample...

Page 30: ...n zh India BUCHI India Private Ltd IN Mumbai 400 055 T 91 22 667 75400 F 91 22 667 18986 india buchi com www buchi com in en Indonesia PT BUCHI Indonesia ID Tangerang 15321 T 62 21 537 62 16 F 62 21 5...

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