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CryoFIT

CryoProbe Flow Conversion System

Installation Manual

Version 003

Innovation with Integrity

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NMR

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Summary of Contents for NMR CryoFIT

Page 1: ...CryoFIT CryoProbe Flow Conversion System Installation Manual Version 003 Innovation with Integrity NMR ...

Page 2: ... trademarks or registered trademarks of their re spective holders This manual was written by T Marquardsen J Ganz August 14 2015 Bruker Corporation P N H12214 For further technical assistance for this product please do not hesitate to contact your nearest BRUKER dealer or contact us directly at Bruker Corporation Am Silberstreifen 76287 Rheinstetten Germany Phone 49 721 5161 6155 E mail nmr suppor...

Page 3: ...ction at Delivery 10 3 3 Packaging 11 3 4 Storage 11 4 Flow Hardware 13 4 1 CryoFIT Accessory PZ H13485 14 5 Installation 15 5 1 Installation with a Warm CryoProbe 15 5 2 Installation with a Cold CryoProbe 16 5 3 Assembling the CryoFIT Accessory 16 6 Inserting the Flow Cell 19 7 Removing the Flow Cell 29 8 Dismantling and Disposal 33 8 1 Dismantling 33 8 2 Disposal 33 9 Contact 35 List of Figures ...

Page 4: ...Contents 4 H12214_1_003 ...

Page 5: ... It is the policy of Bruker to improve products as new techniques and components become available Bruker reserves the right to change specifications at any time Every effort has been made to avoid errors in text and figure presentation in this publication In order to produce useful and appropriate documentation we welcome your comments on this publication Support engineers are advised to regularly...

Page 6: ...ce of not following the warning 1 This is the safety condition u This is the safety instruction NOTICE NOTICE indicates a property damage message This is the consequence of not following the notice 1 This is a safety condition u This is a safety instruction SAFETY INSTRUCTIONS SAFETY INSTRUCTIONS are used for control flow and shutdowns in the event of an error or emergency This is the consequence ...

Page 7: ...of Material Damage Due to Improper Usage Failure to observe the following safety warnings may result in material damage u Never try to spin the flow cell u Never use the sample lift if the flow cell is installed u Do not try to insert NMR sample tubes u Do not use the sample changer u Do not use the device with a BCU05 freezing u Make sure the sample changer is not used during the flow application...

Page 8: ...Introduction 8 H12214_1_003 ...

Page 9: ...amaged Fragile Marks packages with fragile or sensitive contents Handle the package with care do not allow the package to fall and do not allow it to be impacted Protect Against Moisture Protect packages against moisture and keep dry Attach Here Lifting gear lifting chain lifting strap must only be attached to points bearing this symbol Center of Gravity Marks the center of gravity of packages Not...

Page 10: ...irect sunlight Protect from Heat and Radioactive Sources Protect packages against heat direct sunlight and radioactive sources Table 3 1 Symbols on the Packaging 3 2 Inspection at Delivery Upon receipt immediately inspect the delivery for completeness and transport damage Proceed as follows in the event of externally apparent transport damage Do not accept the delivery or only accept it subject to...

Page 11: ...the unit has to be returned to the factory When the packaging material is no longer needed dispose of in accordance with the relevant applicable legal requirements and local regulations 3 4 Storage Storage of the Packages Store the packages under the following conditions Do not store outdoors Store in dry and dust free conditions Do not expose to aggressive media Protect against direct sunlight Av...

Page 12: ...Transport Packaging and Storage 12 H12214_1_003 ...

Page 13: ...the CryoFIT may result in misalignment of the flow cell u Do not remove the screws from the spinner adapter at the end of the CryoFIT NOTICE Material damage to the CryoFIT flow cell The flow cell is very fragile and may be damaged when sliding the lift down when the CryoFIT is not installed u Slide the lift down very slowy and carefully NOTICE Material damage to the flow cell during storage and ha...

Page 14: ...395 CRP CRYOFIT LOCATING SPINNER CPL Z74385 CRP CRYOFIT AIR CONNECTOR T PIECE CPL 85988 FITTING LONG PEEK NUTS 10 32 WITHOUT FERRUL 85936 TUBING SLEEVES 785 825U 88385 TOOL HEX SCR KEY T HANDLE 3MM 84510 HOSE PTFE ID 0 8 AD 1 6 84584 PACKING CORRUGATED CARDBOARD CARTON 2 3 HZ14633 PH CRYOFIT ANTI ROTATION PROTECTION UNIT HZ13395 LOGO AVANCE ONE TWO BAY BRUKER EMBLE 88650 WZ DOUBLE OPEN ENDED WRENC...

Page 15: ...with a Warm CryoProbe 15 Installation with a Cold CryoProbe 16 Assembling the CryoFIT Accessory 16 is the same for either case 5 1 Installation with a Warm CryoProbe Insert the CryoProbe into the magnet Plug in the T piece for the VT gas and capillary and connect the CABLE BVT CRP P N Z14278 Figure 5 1 Bottom of CryoProbe left and T Piece right Mount the ATM unit or the mechanical Tuning Matching ...

Page 16: ...T gas tube from the CryoProbe Plug in the T piece for the VT gas and capillary on the CryoProbe Mount the ATM unit or the mechanical Tuning Matching adapter The CryoProbe is now ready again for use with NMR sample tubes To use the flow cell follow the instructions in the following chapters of this manual 5 3 Assembling the CryoFIT Accessory Before using the CryoFIT Accessory the valve bracket and ...

Page 17: ...ET on the shim upper part as shown Figure 5 3 Bracket Mounting on the Shim Upper Part Assemble of the CryoFIT Holder Unit as shown Figure 5 4 The CryoFIT Holder Unit Mount of the CryoFIT Holder Unit to Holder Bracket on the upper part of the shim system ...

Page 18: ...18 H12214_1_003 Figure 5 5 Mounting the CryoFIT Holder on the Upper Part of the Shim System Adjust the length of the bracing holder on the magnet until the plate is horizontal Figure 5 6 Height of the Bracing Holder ...

Page 19: ...5 to prevent freezing Close the valve to disable the spinning flow Move the slider to the closed position Figure 6 1 Valve Parts Activate the sample lift CAUTION Make sure the sample changer is not used during the flow application Figure 6 2 Activating the Sample List Note The insert guide is needed to insert the capillary properly into the probe The insert guide looks similar to a classical sampl...

Page 20: ...low Insert the insert guide into the magnet Figure 6 3 Inserting the Guide into the Shim Upper Part Figure 6 4 Switching Off the Sample Lift Unscrew the plug on the T piece of the VT gas at the bottom of the probe Do not leave it open for more than 10 minutes Do not disconnect the VT gas hose Some VT gas will escape from the opened T piece ...

Page 21: ...ill be needed when the Flow Cell is removed see Removing the Flow Cell 29 To prepare the CryoFIT take the CryoFIT out of the box and bend the rod at the frame joint Figure 6 6 Bending the Frame Joint NOTICE Before installation be sure that the inlet capillary is clean and free of dirt particles on the surface ...

Page 22: ...ce of the VT gas adapter If you feel some slight resistance when the capillary hits the T piece at the probe bottom cautiously increase the force slightly to push the capillary through Put the CryoFIT into the CryoFIT Mounting Unit If the capillary gets stuck Make sure the insert guide is in the shim system Ask someone else to move the T piece back and forth while you insert the capillary Figure 6...

Page 23: ...sample lift so that the insert guide is lifted Figure 6 8 Activating the Sample Lift Take the insert guide and rotate the two pieces against each other until the two slots are in line Carefully weave out the capillary Figure 6 9 Removing the Insert Guide ...

Page 24: ...he sample lift Figure 6 10 Switching Off the Sample Lift Lift the CryoFIT and let the CryoFIT glide all the way down into the magnet Hold the CryoFIT to control the lowering motion At the frame joint bend the CryoFIT straight and glide it until to a stop ...

Page 25: ...re 6 11 Inserting the CryoFIT Hold the CryoFIT with one hand and with the other hand take the lift and pull it up Turn the lift and then move it down carefully Now the flow cell is inserted into the probe and the outlet capillary can be connected ...

Page 26: ...ll At the bottom of the probe take the nut with the green sleeve and put it over the inlet capillary just below the T piece of the VT gas Screw the nut tight on the T piece of the VT gas The VT gas will no longer escape from the T Piece Figure 6 13 Nut Screwed on the T Piece ...

Page 27: ...w equipment Connecting the CryoFIT to the LC NMR or BEST When you connect the Inlet capillary with a 1 16 capillary to the LC NMR interface Prospekt2 BPSU 36 BPSU 12 BSFU make sure that the capillary does NOT extrude out of the end of the sleeve Ensure that the capillary ends at the end of the sleeve ...

Page 28: ...Inserting the Flow Cell 28 H12214_1_003 ...

Page 29: ... do a Wash and Dry Probe Otherwise use a syringe to blow air through the CryoFIT to remove any liquid Unscrew the nut with the green sleeve at the bottom of the probe and the outlet capillary at the top of the magnet Figure 7 1 T piece and Disconnected Outlet Capillary NOTICE Be sure the capillary is clean and free of dirt particles on the surface Carefully pull out the lift of the CryoFIT Lock th...

Page 30: ...ure 7 2 Removing the Flow Cell Carefully pull out the CryoFIT to the frame joint At the frame joint push the ring and bend the CryoFIT Pull out the CryoFIT and inlet capillary Put the CryoFIT back in its package with straight bended frame joint ...

Page 31: ...Removing the Flow Cell H12214_1_003 31 Figure 7 3 Removing the CryoFIT ...

Page 32: ... onto the T piece of the VT gas Figure 7 4 Plugging in the T Piece Open the valve to enable the spinning flow Move the slider to the OPEN position Figure 7 5 Valve Parts The CryoProbe is now ready again for using NMR sample tubes with or without a sample changer ...

Page 33: ...and parts properly and dismantle in compliance with applicable local occupational safety and environmental protection regulations 8 2 Disposal After the lifespan of the product Bruker takes responsibility for disassembly and disposal in accordance with the European Directive WEEE 2012 19 EC Bruker BioSpin will take back the components free of charge upon request by the customer If the customer wan...

Page 34: ... the environment from incorrect handling of pollutants Incorrect handling of pollutants particularly incorrect waste disposal may cause serious damage to the environment u Always observe local environmental regulations regarding handling and disposal of pollutants u Take the appropriate actions immediately if pollutants escape accidentally into the environment If in doubt inform the responsible mu...

Page 35: ...ervice centers Bruker BioSpin NMR provide dedicated hotlines and service centers so that our specialists can respond as quickly as possible to all your service requests applications questions software or technical needs Please select the NMR service center or hotline you wish to contact from our list available at http www bruker com service information communication helpdesk magnetic resonance htm...

Page 36: ...Contact 36 H12214_1_003 ...

Page 37: ...vating the Sample List 19 Figure 6 3 Inserting the Guide into the Shim Upper Part 20 Figure 6 4 Switching Off the Sample Lift 20 Figure 6 5 Unplugging the T Piece 21 Figure 6 6 Bending the Frame Joint 21 Figure 6 7 Inserting the Capillary 22 Figure 6 8 Activating the Sample Lift 23 Figure 6 9 Removing the Insert Guide 23 Figure 6 10 Switching Off the Sample Lift 24 Figure 6 11 Inserting the CryoFI...

Page 38: ...List of Figures 38 H12214_1_003 ...

Page 39: ...H12214_1_003 39 ...

Page 40: ...Bruker Corporation info bruker com www bruker com Order No H12214 ...

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