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6

Care and maintenance

N.B.  Before commencing any maintenance, cleaning or fault

finding the equipment should be isolated from the
mains electricity supply. These operations should only
be carried out by suitably qualified personnel.

Only spare parts supplied or approved by Bibby Scientific Ltd or its
agent should be used. Fitting of non-approved parts may affect the
performance or safety of the equipment.

Cleaning

Over a period of operation scale will build up inside the boiler. To
obtain optimum performance this scale should be removed on a
regular basis.

Please note that scale can build up both in the neck and main
body of the boiling chamber.

The time span between cleaning depends greatly on the hardness of
the water and the amount of use. Frequently used stills in hard
water areas may need descaling once a week whereas in a soft
water area several weeks may elapse before descaling is necessary.

N.B.  Heavy scaling will reduce distilled water quality and can

shorten the life of the heating element.

It is possible to descale the Distinction Water Still without
dismantling the glassware by following these instructions in
conjunction with Control of Substances Hazardous to Health
regulations (COSHH) 1988:

1.  Switch off the electricity supply to the still and allow it to cool

completely.

2.  Turn off the cooling water supply.

3.  Open the stopcock on the constant level control and allow the

boiler to drain completely. Close stopcock.

4.  Turn on the cooling water supply and allow the boiler to fill to

approximately half way to its normal operating level. Turn off
the water supply.

5.  Into the open funnel of the constant level control carefully add

about 100ml of concentrated hydrochloric acid.

WARNING!
ALWAYS HANDLE STRONG ACIDS WITH GREAT CARE.
PROTECTIVE CLOTHING, GLOVES AND FACE-MASKS
SHOULD BE WORN DURING THE DESCALING OPERATION.
REMOVE ANY ACID SPILLS IMMEDIATELY.

Turn on the water supply and fill the boiler  to the normal
operating level. The water will flush the acid into the boiler. The
water supply should be turned off when the level in the boiler
is slightly below the overflow.

6.  Leave the acid in the boiler to dissolve the scale. This may take

some time depending on the severity of the build-up.

7.  Open the stopcock and allow the boiler to drain.

Note: If the acid in the boiler has not been completely
neutralised the liquid flowing to drain may be highly
acidic. All necessary safety precautions should be
observed around the drain and any effluent control
procedures followed.

8.  Close the stopcock, turn on the water and allow the boiler to

fill with cold water. Turn off the water, re-open the stopcock
and allow the boiler to drain.

Repeat this procedure three times.

9.  The Distinction Water Still may now be restarted by referring to

the instructions given under “Operation” in this manual.

Note:

The stand and outer surfaces of the glassware should be

cleaned using a damp cloth and a mild detergent solution.

Heater replacement*

1.  Isolate the Still from the electricity supply.

2.  Clean the heater and boiler if they are heavily scaled by

following the cleaning instructions given in this manual.

3.  It will be found easier to replace the heater by working with

the boiler “on the bench”.

Therefore:

Drain the boiler via the stopcock.

Remove the end panel.

Disconnect the heater cable.

Disconnect all water hoses.

Remove the condenser.

Remove the boiler, complete with heater, from the stand.

Unscrew the 3 bolts securing the heater and 
withdraw the heater from the boiler.

Remove the aluminium plate and silicone rubber 
ring from the heater.

4.  Now fit a new heater as described in assembly instruction

number 4.

N.B. Examine the silicone ring and replace if not in good
condition.

5.  Re-assemble the Still by following the assembly instructions.

*Note: 

Heater is

not 

covered by the 3 year warranty. 

It is only guaranteed for up to 1000 hours in use.

Summary of Contents for Distinction D4000

Page 1: ...Distinction Assembly and operating instructions Instructions de montage et de fonctionnement D4000 D4000 EURO Water Still Distinction...

Page 2: ...ith or be affected by other equipment with similar qualifications We cannot be sure that other equipment used in its vicinity will meet these standards and we cannot guarantee that interference will n...

Page 3: ...n Water Still can be wall or bench mounted Select a convenient location which has access to the following services Electricity Supply Before connection please ensure that the line supply is suitable T...

Page 4: ...struct access to the thermostat reset buttons see figure 1 5 Take the two metal straps and attach the springs to the rear of the cradles on the stand Place the assembled boiler and element onto the cr...

Page 5: ...d use 1 5mm M4 eyelet crimps with a performance conforming to BS 4G178 part 1 1984 and part 2 1986 A suitable crimp tool should be used Operation 1 Turn on the cold water supply and adjust the flow to...

Page 6: ...SCALING OPERATION REMOVE ANY ACID SPILLS IMMEDIATELY Turn on the water supply and fill the boiler to the normal operating level The water will flush the acid into the boiler The water supply should be...

Page 7: ...Failed electricity supply Restore supply c Thermostat operated Identify and rectify the cause and reset thermostat Water level in boiler a Supply of cooling water is Adjust the supply to is too low h...

Page 8: ...de fr quences radio Il ne doit donc pas interf rer avec d autres appareils r pondant aux m mes directives Ne pouvant tre s r que d autres appareils en fonctionment autour du distillateur soint confor...

Page 9: ...2 i Ins rer les boulons au travers du collier m tallique et le placer autour du tube vas du bouilleur ii Enrouler le collier en fibre et l ins rer entre le tube vas et le collier m tallique Le pliage...

Page 10: ...collier plastique fourni 10 Placer l extr mit libre du tuyau vers l vacuation en s assurant qu il ne pr sente aucun coude pouvant perturber l coulement de l eau 11 V rifier que le robinet du c ntroleu...

Page 11: ...pince sertir est n cessaire Mise en route 1 Ouvrir le robinet d alimentation en eau froide et r gler le d bit 1 l mn environ L eau doit circuler travers le r frig rant Attendre que le niveau d eau dan...

Page 12: ...TECTION DES GANTS ET DES MASQUES FACIAUX DEVRONT ETRE UTILISES LORS DES OPERATIONS DE NETTOYAGE NETTOYER IMMEDIATEMENT TOUTE ECLABOUSSURE D ACIDE Ouvrir l alimentation d eau pour remplir le bouilleur...

Page 13: ...tion du distillat vers V rifier que le tuyau de sortie du vers l vacuation le r servoir se fait mal distillat ne pr sente aucun coude b Event obstru par la sonde du D gager l vent thermostat r frig ra...

Page 14: ......

Page 15: ...Notes...

Page 16: ...f bibby scientific fr www bibby scientific com Bibby Scientific Italia Srl Via Alcide de Gasperi 56 20077 Riozzo di Cerro al Lambro Milano Italia Tel 39 0 2 98230679 Fax 39 0 2 98230211 e mail marketi...

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