Analytik Jena SPECORD 200 Manual Download Page 9 | Manualshive

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SPECORD

®

Safety notes

General safety regulations

The SPECORD

®

was produced and tested in compliance with the following standards

and regulations:

•

DIN EN 61010-1 (IEC 1010-1)

•

73/23/EC

•

89/336/EC.

The SPECORD

®

meets the requirements as per Protection Type IP 20.

SPECORD

®

200/205/210/250 User's Manual – Edition 04/2005

Page 7

Analytik Jena AG

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Summary of Contents for SPECORD 200

Page 1: ...SPECORD PC 200 205 210 250 UV VIS Spectrophotometer...

Page 2: ...jena de Copyrights and Trademarks Microsoft Windows XP Windows NT Windows 2000 MS Excel are registered trademarks of Microsoft Corp Publication No 221 416 23 Edition April 2005 Technical documentatio...

Page 3: ...ectors and display elements 21 6 2 Removing the transport lock 23 6 3 Connecting the SPECORD 24 6 4 Start up 25 6 5 Switching the device off 26 6 5 1 Switching the deuterium lamp off 26 6 5 2 Switchin...

Page 4: ......

Page 5: ...al system without electromechanical modulator ensures true real time operation so that even variations in the absorbance of references can be compensated during the measurement The internal wavelength...

Page 6: ...you to a specific procedure or practice which if not followed correctly could cause personal injury Caution Caution messages refer you to procedures which if not observed could result in damage to th...

Page 7: ...rticular you should also observe the safety notes given on the labels and the information on the use storage and disposal of reagents reaction cells and the notes on the package inserts of test kits I...

Page 8: ...adiation emitted by the lamp to avoid the risk of getting conjunctivitis Therefore switch off the lamp for lamp replacement Lamp damage Do not grasp functioning halogen and deuterium lamps on their gl...

Page 9: ...roduced and tested in compliance with the following standards and regulations DIN EN 61010 1 IEC 1010 1 73 23 EC 89 336 EC The SPECORD meets the requirements as per Protection Type IP 20 SPECORD 200 2...

Page 10: ......

Page 11: ...range 3A 3A Wavelength accuracy with holmium oxide filter 0 5nm Wavelength reproducibility with holmium oxide filter 0 05nm Photometric accuracy VIS at 546nm with Hellma F4 neutral density filter 0 0...

Page 12: ...ometric accuracy VIS at 546nm with Hellma F4 neutral density filter 0 005 Photometric accuracy UV with potassium dichromate as per Ph Eur 0 01 Stray light at 200nm KCl Merck 1 08164 0001 0 2 T Stray l...

Page 13: ...T 3 15 AH 250V Type 19181 Wickmann 115 V T 3 15 AH 250V Type 19181 Wickmann Radio noise suppression as per EN 55011 Class A Noise immunity as per DIN EN 50082 1 Protection Type IP 20 Data interfaces...

Page 14: ......

Page 15: ...t Fig 4 1 Mechanical design of SPECORD The major subassemblies of the SPECORD are Light sources Halogen lamp and deuterium lamp generate the light that is monochromatized in the spectrometer system Th...

Page 16: ...diodes are used as radiation detectors which are Peltier temperature controlled on SPECORD 200 210 250 Power supply module The power supply modules supply the electrical voltage to the electronic syst...

Page 17: ...f either deuterium or halogen lamp is sent onto the entrance slit of the monochromator You can choose the wavelength at which the lamp is changed over a wide range using the WinASPECT control and anal...

Page 18: ...eration of measured data The entrance and exit slits of the spectrometer system are mounted to the slit carrier Depending on the device model the slits allow the following spectral slit widths SPECORD...

Page 19: ...wall The two pairs of carrier rods serve to accommodate the universal holder and other accessories which easily clamp to the rods The receptacles for the cells 7 9 with turbid samples are located dire...

Page 20: ...scription and operating principle SPECORD Design of subassemblies 400 193 94 70 70 70 96 Fig 4 6 Dimensions of sample compartment Page 18 SPECORD 200 205 210 250 User s Manual Edition 04 2005 Analytik...

Page 21: ...acid or caustic vapors away from the vicinity of the device The installation site of the SPECORD must meet the following requirements The place should be free of draft dust corrosive vapors as well as...

Page 22: ......

Page 23: ...ystem optional accessory 3 Status indicators for line voltage halogen and deuterium lamps 4 Lid of lamp housing Fig 6 1 SPECORD overall view The LEDs indicating Power ON and lamp standby are located o...

Page 24: ...32 port PC 2 USB port PC 3 Connector for xyz autosampler APG 4 Connector for control of Peltier temperature controlled cell holder ACC 5 6 Hose conduits for coolant and waste hoses Fig 6 4 Connectors...

Page 25: ...device Transport lock Fig 6 6 Transport lock on SPECORD Note The transport lock screw is not removed from the device but is left in its holder in the SPECORD If the device must be transported again or...

Page 26: ...able Spare fuses 5 x 20 T 3 15 A L User s Manuals for the SPECORD the accessories and the WinASPECT control and analysis software Connecting SPECORD and PC 1 Remove the device from its transport packa...

Page 27: ...on on the Windows desktop or by clicking the Start button on the taskbar Start Programs WinASPECT WinASPECT Fig 6 7 Program symbol of WinASPECT 2 Using the power switch on the left panel of the device...

Page 28: ...longer this day you can switch it off by software control following this procedure 1 In WinASPECT activate the device driver with menu command Measurement Set Parameters 2 Activate the Device tab 3 In...

Page 29: ...ing a pathlength of up to 50 mm and a width of 12 5 mm 1 Cell support 2 Guide Fig 7 1 Standard cell holder Push the cell holder with its guide 2 from top onto the cell holder mount The beam transmits...

Page 30: ...he detector capture the total scattered radiation For this purpose the sample and the reference substance must be arranged as close to the detector as possible Therefore the receptacles for the cells...

Page 31: ...for round cells Holder for solid samples 11 60 variable Angle Reflectance Accessory Absolute Reflectance Accessory Universal sipper system with flow cell and peristaltic pump XYZ autosampler Fiber co...

Page 32: ......

Page 33: ...ou can order consumables and wear parts by phone from our Service Department Hotline No 49 3641 77 7407 In the case of malfunction of the device please contact our Service Department For the address r...

Page 34: ...ng coil has burnt out its energy is insufficient or the operating hours counter indicates 2000 h 8 3 2 Opening the flap of the lamp compartment The flap of the lamp compartment front left corner of de...

Page 35: ...e enclosed by a protective cover SPECORD 250 1 Protective cover of halogen lamp two parts 2 Knurled screw for protective cover of halogen lamp 3 Protective cover of deuterium lamp 4 Top part of protec...

Page 36: ...Desiccator 6 Illuminating mirror 7 Screw for adjusting the illuminating mirror Fig 8 3 Lamp compartment of SPECORD 200 205 210 opened Closing the flap of the lamp compartment 1 Put the flap of the la...

Page 37: ...you touched the glass bulb with your fingers wipe the fingerprints off with a clean lintfree cloth and pure alcohol The performance of the lamp will deteriorate by contamination After you have remove...

Page 38: ...ensure that maximum intensity of the lamp is incident on the entrance slit of the monochromator For this purpose you can slightly move the illuminating mirror by means of setscrew Fig 8 3 7 Caution D...

Page 39: ...ment flap The protective cover of the halogen lamp is visible 1 Loosen the knurled screw of the protective cover of the halogen lamp Fig 8 2 2 and remove the front part of the protective cover Note Th...

Page 40: ...will bring up the SPECORD xxx Service Check dialog box 3 Click on the Zeroth Order button and choose the halogen lamp HL Lamp 4 View the image of the sample beam in the sample compartment by holding...

Page 41: ...tool such as an appropriate coin unscrew the desiccator from its holder 3 Remove the new desiccator from the packaging and screw it into the holder 4 Finally close the flap of the lamp compartment Use...

Page 42: ......

Page 43: ...levant legal and local regulations When the service life of the device is over dispose of the device with its electronic components as electronic scrap observing the relevant regulations You can also...

Page 44: ......

Page 45: ...ig 6 4 Connectors on right hand side panel 22 Fig 6 5 Rear view of device 23 Fig 6 6 23 Transport lock on SPECORD Fig 6 7 Program symbol of WinASPECT 25 Fig 6 8 Dialog box of SPECORD 250 device driver...

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