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pH 315i

Lists

41

Glossary

Adjusting

To manipulate a measuring system so that the relevant value (e. g. the 
displayed value) differs as little as possible from the correct value or 
a value that is regarded as correct, or that the difference remains with-
in the tolerance.

Asymmetry

Designation for the offset potential of a pH electrode. It is the measur-
able potential of a symmetrical electrode, the membrane of which is 
immersed in a solution with the pH of the nominal electrode zero point 
(WTW electrodes: pH = 7).

AutoRange

Name of the automatic selection of the measuring range.

AutoRead

WTW name for a function to check the stability of the measured value.

Calibration

Comparing the value from a measuring system (e. g. the displayed 
value) to the correct value or a value that is regarded as correct.  Of-
ten, this expression is also used when the measuring system is adjust-
ed at the same time (see adjusting).

Diaphragm

The junction is a porous body in the housing wall of reference elec-
trodes or electrolyte bridges. It forms the electrical contact between 
two solutions and makes electrolyte exchange more difficult. The ex-
pression, junction, is also used for ground or junction-less transitions.

Electrode voltage

The electromotive force U of the electrode is the measurable electro-
motive force of an electrode in a solution. It equals the sum of all the 
galvanic voltages of the electrode. Its dependency on the pH results 
in the electrode function which is characterized by the parameters, 
slope and zero point.

Electrode zero point

The zero point of a pH electrode is the pH value at which the electro-
motive force of the pH electrode at a specified temperature is zero. 
Normally, this is at 25 °C.

Measured parameter

The measured parameter is the physical dimension determined by 
measuring, e. g. pH, conductivity or D. O. concentration.

Measured value

The measured value is the special value of a measured parameter to 
be determined. It is given as a combination of the numerical value and 
unit (e. g.  3 m; 0.5 s; 5.2 A; 373.15 K).

Measuring system

The measuring system comprises all the devices used for measuring, 
e. g. measuring instrument and probe.  In addition, there is the cable 
and possibly an amplifier, terminal strip and armature.

Molality

Molality is the quantity (in Mol) of a dissolved substance in 1000 g sol-
vent.

MultiCal

®

WTW name stating that a measuring instrument provides several cal-
ibration procedures.

Содержание pH 315i

Страница 1: ...ba52308e02 03 2004 Handheld meter pH 315i ba52308e Operating manual PH 6 4 2 9 9 6 C TP AR CAL M O pH measuring instrument...

Страница 2: ...se The instrument warranty covers manufacturing faults that are discov ered within the warranty period The warranty does not cover compo nents that are replaced during maintenance work e g batteries T...

Страница 3: ...missioning 11 4 Operation 13 4 1 Switching on the measuring instrument 13 4 2 Measuring 14 4 2 1 Measuring the pH value 15 4 2 2 Measuring the ORP voltage 16 4 3 Calibrating 17 4 3 1 AutoCal TEC 19 4...

Страница 4: ...List of contents pH 315i 4...

Страница 5: ...l applications The proven MultiCal calibration procedure and the special AutoRead function support you in your work with the pHhandheld meter Note If you need further information or application notes...

Страница 6: ...of equipment You will find additional information on this and other accessories in the WTW catalog or via the Internet Set sample configuration 1 Measuring instrument pH 315i 2 Stand 3 KCI solution fo...

Страница 7: ...AR CAL M Select the measuring mode M pH value ORP voltage Switch measuring instrument on off ON OFF Calibrate select the calibration proce dure CAL Activate deactivate the AutoRead function AR Confir...

Страница 8: ...imiting Almost all electrodes in particular WTW electrodes fulfill these con ditions 1 pH electrode 2 Reference electrode 3 Temperature probe F S ConCal Auto Store Time Baud Day Month No Ident Year RC...

Страница 9: ...tors will know the necessary safety precautions to take when handling chemicals Symbols used Warning indicates instructions that must be followed to prevent damage to your instrument Note indicates no...

Страница 10: ...e formation of condensate can lead to the faulty func tioning of the instrument In this event wait until the temperature of the instrument reaches room temperature before putting the instrument back i...

Страница 11: ...ing Scope of delivery l Handheld meter pH 315i l Operating manual and short operating manual l 4 batteries 1 5 V Mignon type AA in the instrument For details of scope of delivery of SETs see chapter 1...

Страница 12: ...Commissioning pH 315i 12...

Страница 13: ...are used appear for approx one second one after the other In addition the calibration proce dure of the last calibration is shown AutoCal TEC or AutoCal DIN or no display in the delivery state or aft...

Страница 14: ...on the display by TP If you nevertheless use an electrode without a temperature probe the instrument operates with a reference temperature of 25 C Thus the sample and calibration solution must have th...

Страница 15: ...ing the current value by pressing RUN ENTER 1 Perform the preparatory activities according to section 4 2 2 Immerse the pH electrode into the test sample 3 Press the M key until pH appears on the stat...

Страница 16: ...s using a test solution 1 Perform the preparatory activities according to section 4 2 2 Immerse the ORP electrode in the test sample 3 Press the M key until U appears on the status display The ORP vol...

Страница 17: ...ted after the first buffer solu tion This corresponds to a single point calibration To do this the instrument uses the standard slope 59 2 mV pH at 25 C and deter mines the asymmetry of the electrode...

Страница 18: ...58 20 20 58 57 25 25 61 60 5 or 57 56 Clean the electrode according to the electrode operating manual 30 30 62 61 or 56 50 E3 Eliminate the error according to chapter 6 WHAT TO DO IF 30 or 30 62 or 5...

Страница 19: ...ection 4 4 CONFIGURATION the instrument displays the relevant buffer nomi nal value or the current electrode voltage in mV 1 Press the CAL key repeatedly until the Ct1 display indicator and the functi...

Страница 20: ...tore TempError RCL LoBat CalError ARng ConCal Time Baud Day Month No Ident Year 1 F S mg L ppm ISE 8 4 2 C TP mV pH mol L 8 Auto Store TempError RCL LoBat CalError ARng ConCal Time Baud Day Month No I...

Страница 21: ...y mV appears on the display 10 Change to the measuring mode with M or proceed to the three point calibration with RUN ENTER 0 L s TP C ConCal AR AutoCal DIN mol L 8 Auto Store RCL LoBat CalError ARng...

Страница 22: ...pH appears on the display The probe symbol shows the evaluation of the current calibration three point cal ibration CalError ARng AR AutoCal DIN LoBat 8 mV pH 8 1 U F S ConCal Auto Store Time Baud Da...

Страница 23: ...bration is complete 0 L s TP C ConCal AR AutoCal DIN mol L 8 Auto Store RCL LoBat CalError ARng Time Baud Day Month No Ident Year 1 U F S TempError mg L ppm ISE pH 1 59 AutoCal TEC mV pH y s a RCL AR...

Страница 24: ...sensor symbol in the delivery state or after the measurement parameter has been reset 2 Immerse the pH electrode in the first buffer solution 3 Press the RUN ENTER key The AR display indicator flashe...

Страница 25: ...le 8 When the measured value is stable AR disappears The value of the slope mV pH appears on the display The probe symbol shows the evaluation of the current calibration two point cali bration AutoCal...

Страница 26: ...t calibration with RUN ENTER AutoCal TEC 0 L s TP C ConCal AR mol L 8 Auto Store RCL LoBat CalError ARng Time Baud Day Month No Ident Year 1 U F S TempError mg L ppm ISE pH 0 59 mV pH AutoCal DIN Auto...

Страница 27: ...pH appears on the display The probe symbol shows the evaluation of the current calibration three point cal ibration CalError ARng AR AutoCal DIN LoBat 8 mV pH 8 1 U F S ConCal Auto Store Time Baud Da...

Страница 28: ...bration is complete AutoCal TEC 0 L s TP C ConCal AR mol L 8 Auto Store RCL LoBat CalError ARng Time Baud Day Month No Ident Year 1 U F S TempError mg L ppm ISE pH 4 59 mV pH AutoCal DIN AutoCal TEC...

Страница 29: ...ly on the display Afterwards the measuring instrument switches automatically to the setting of the display during the pH calibration 4 Select the required display during the pH calibration with CAL mV...

Страница 30: ...Resolution of pH display 0 01 low resolution 1 Press the RUN ENTER key and hold it down 2 Press the CAL key 3 Confirm with RUN ENTER The settings are reset The pH meter switches to the pH measuring m...

Страница 31: ...e sure that the poles of the batteries are the right way round The signs on the batteries must correspond to the signs in the bat tery compartment Only use leakproof alkaline manganese batteries 1 Ope...

Страница 32: ...port packing We recommend Keep the packing material The original packing pro tects the instrument against damage during transport Batteries This note refers to the battery regulation that applies in t...

Страница 33: ...el electrolyte dried out Replace electrode Cause Remedy Electrode Diaphragm contaminated Clean diaphragm Membrane contaminated Clean membrane Moisture in the plug Dry plug Electrolyte out of date Repl...

Страница 34: ...dy pH electrode Diaphragm contaminated Clean diaphragm Membrane contaminated Clean membrane Test sample pH value not stable Measure with air excluded if necessary Temperature not stable Adjust tempera...

Страница 35: ...itable electrode Temperature difference between buffer and test sample too high Adjust temperature of buffers or sample Measurement procedure not suitable Follow special procedure Cause Remedy Operati...

Страница 36: ...What to do if pH 315i 36...

Страница 37: ...ble relative hu midity Yearly mean 75 30 days year 95 Other days 85 Measuring range Resolution pH 2 000 16 000 2 00 16 00 0 001 0 01 U mV 999 9 999 9 1999 1999 0 1 1 T C 5 0 105 0 0 1 pH 2 pH units fr...

Страница 38: ...ment Note This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protectio...

Страница 39: ...lains the indicators and the abbreviations that appear on the display and in the manual Specialist terms The glossary briefly explains the meaning of the specialist terms How ever terms that should al...

Страница 40: ...Display indicator during calibration for pH mea surements Indicates the selection of the buffer data record for buffer solutions prepared according to DIN 19 266 Ct Display indicator during calibratio...

Страница 41: ...e difficult The ex pression junction is also used for ground or junction less transitions Electrode voltage The electromotive force U of the electrode is the measurable electro motive force of an elec...

Страница 42: ...activity divided by the unit of the molality The practical pH value is the value of a pH measurement Reference temperature Fixed temperature value to compare temperature dependent mea sured values For...

Страница 43: ...8 Displaying calibration data 17 Drift control 15 E Error messages 33 I Initialization 30 J Jack field 8 K Keys 7 L LoBat 34 O Operating safety 10 ORP electrode 16 ORP voltage 16 R Replacing the batte...

Страница 44: ...Index pH 315i 44...

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