Varian PrepStar 218 SD-1 Скачать руководство пользователя

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Varian, Inc.
2700 Mitchell Drive
Walnut Creek, CA 94598-1675/USA

©Varian, Inc. 2005

03-914947-20:Rev.

ProStar 210/215 and PrepStar

218/SD-1 Solvent Delivery

Module Control

Galaxie Driver Manual

Содержание PrepStar 218 SD-1

Страница 1: ...Varian Inc 2700 Mitchell Drive Walnut Creek CA 94598 1675 USA Varian Inc 2005 03 914947 20 Rev 5 ProStar 210 215 and PrepStar 218 SD 1 Solvent Delivery Module Control Galaxie Driver Manual...

Страница 2: ...the Synopsis 9 Building a Method 12 Creating a New Method 12 ProStar PrepStar Pump Control Method 14 Elution Control 16 Miscellaneous Control 18 Pressure Control 19 Injection Control 20 Starting and V...

Страница 3: ...er how to start and view a running acquisition and what actions are available during an analysis The ProStar 210 215 and PrepStar 218 Solvent Delivery Modules are identical in appearance and operation...

Страница 4: ...communicate with the ProStar 210 215 218 SD 1 module a RS232_Interface or a RS232_PC communication bus must be configured on the acquisition server The parameters of the bus to must be the following S...

Страница 5: ...eated Configuring the ProStar PrepStar Pump Click on the button corresponding to the ProStar PrepStar pump driver and the pump configuration screen appears The toolbar allows you to easily scroll thro...

Страница 6: ...ow Select from the list the name of the RS422 Bus where the system has been connected NOTE For more details about the RS422 Bus configuration refer to the section Configuring the Communication Server...

Страница 7: ...PrepStar modules to work as a binary pump three modules for a ternary one and four to work in quaternary mode With this type of pump a module can be used as an injector In this case a new Injection sc...

Страница 8: ...ect the ProStar 215 and PrepStar 218 have more powerful motors larger power supplies and can operate at higher pressures than the ProStar 210 NOTE The pump head size must be configured on the instrume...

Страница 9: ...erview part of the system configuration a synopsis can be defined for the system This synopsis depends on the configured devices 1 To save the configuration of these devices click on the OK button 2 R...

Страница 10: ...ection tube will appear between the two anchors Click on the button to delete a selected tube click on the button to delete all the tubes Click on to define a background color or on to make the backgr...

Страница 11: ...OTE Once the system has been created and correctly configured it must be associated with one or more projects in order to start acquisitions For more details about the creation and configuration of a...

Страница 12: ...t necessary to define all of the sub method sections however you must fill in the instrument control section prior to starting an acquisition 1 To create a new method select the FILE NEW METHOD option...

Страница 13: ...have been completed click on the OK button The new method is created and is opened with default parameters in the Galaxie Chromatography Data System The next step is the definition of each of the meth...

Страница 14: ...r 210 215 PrepStar 218 SD 1 SDM 14 03 914947 20 5 ProStar PrepStar Pump Control Method Once the new method is created select the control section in the lower part of the browser The following screen a...

Страница 15: ...the ProStar PrepStar pump control method section It contains up to four sub sections Elution Miscellaneous Pressure and Injection Click on the required sub section to define the corresponding paramet...

Страница 16: ...odule Here are listed all the available solvents Water Acetone Acetonitrile Benzene Carbon tetrafluoride Chloroform Cyclohexane Dichloroethane Diethyl Ether Dimethylformamide Dioxane Ethanol Ethyl Ace...

Страница 17: ...t lead to cavitations or bubble formation in the pump head causing a lower than expected flow rate If the refill time is too long excessive pulsations in the flow may be observed This parameter is pro...

Страница 18: ...he pump will start as soon as it is ready If inject trigger on pump X is chosen the pump will start when an inject marker is send to pump X End of Sequence In the scrolling list select either to stop...

Страница 19: ...ump head This limit is automatically adapted according to the connected pump head To know these limits refer to the Pressure Limits chapter in the appendix of this manual If a higher value of pressure...

Страница 20: ...Pump Injection Parameter Group Enter the time when the injection will start in the Injection time field Enter the flow rate of the injection in the Injection Rate field The end time of the injection i...

Страница 21: ...ProStar 210 215 PrepStar 218 SD 1 SDM 21 03 914947 20 5 NOTE During the injection period the current flow of each pump modules will be adjusted to take into account the injection flow as shown below...

Страница 22: ...ethod has been correctly programmed an analysis can be started The next section briefly describes how to start an acquisition Quick Start Single Acquisition 1 Press the button In the Quick Start windo...

Страница 23: ...ers for each acquisition channel can be entered in the Channel X tab Click on the Start button to start the acquisition if the system is a single injector system or click on the Next button if the sys...

Страница 24: ...or more details about how to start an acquisition refer to the Galaxie Chromatography Data System User s Guide Running Acquisition Status Viewing a Running Acquisition To view a running acquisition cl...

Страница 25: ...tatus window Elution Window In this window the elution parameters solvent composition pressure flow etc are shown with their current values depending on the control method program Most of these values...

Страница 26: ...ick on OK to validate Click on the button and the same screen as above will be displayed Click on or to start or stop the pump Click on the button when the pump is running to stop the progression of t...

Страница 27: ...status can be read in this screen The light becomes red indicating the nature of the error It is possible to define new pressure limits directly from this status screen by clicking on the button The s...

Страница 28: ...pStar modules are shown Overview Window Click on the button the Status Overview window is displayed and contains three tabs General displays the synopsis of the instrument where some current values ca...

Страница 29: ...914947 20 5 The same actions than in the Elution window can be performed by clicking on the appropriate buttons Not Ready contains the not ready information sent by the instrument Events contains the...

Страница 30: ...ProStar 215 PrepStar 218 Head Flow Rate Range mL min SS and Ti PEEK SS and Ti PEEK SS and Ti PEEK 5 0 01 5 599 NA 599 NA 599 NA 10 0 01 10 599 275 599 275 599 275 25 0 025 25 317 275 410 275 410 275 5...

Страница 31: ...ne 96 7 1046 Carbon tetrachloride 106 7 998 Chloroform 97 4 1227 Cyclohexane 114 800 Dichloroethane 111 9 1020 Diethyl Ether 188 700 Dimethylformamide 80 1500 Dioxane 60 1500 Ethanol 115 1100 Ethyl Ac...

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