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Water Analysis Instruments

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CIC0004053-01 0121

Содержание Orion 8010cX

Страница 1: ...User Manual CIC0004053 01 Revision C January 2021 Orion 8010cX Ammonia Analyzer ...

Страница 2: ...nual is for informational purposes only The contents and the product it describes are subject to change without notice Not all products are available in all countries Please consult your local dealer for details Thermo Fisher Scientific makes no representations or warranties with respect to this manual In no event shall Thermo Fisher Scientific be held liable for any damages direct or incidental a...

Страница 3: ...rview 5 Intended use 5 Specifications 5 Instrument Size 7 Principles of Operation 8 Installation 9 Unpacking Inspection 9 Requirements for Instrument Installation 9 Flow Cell Flow cell components are optional 12 Electrical Connection 15 Main Control Panel 16 Liquid Leakage Alarm 20 System Startup 21 Reagent Preparation 21 Tubing Connections 21 Instrument Startup 25 Priming 25 ...

Страница 4: ...unction 34 Instrument Diagnosis 35 Regular Maintenance 37 General Maintenance 37 Regular Maintenance 37 Cleaning 38 Liquid Leakage Maintenance 38 Long term Shutdown 39 Common Faults and Troubleshooting Measures 40 Customer Service 49 Compliance Precautions 49 Terms and Conditions 49 Warranty 50 Accessories Information 51 Consumables Parts and Accessories 51 Regulatory 52 ...

Страница 5: ... contract between Thermo Fisher Scientific Inc and a purchaser This document shall not govern or modify any Terms and Conditions of Sale which Terms and Conditions of Sale shall govern all conflicting information between the two documents Legal Information Note Specifications terms and pricing are subject to change Not all products are available in all countries Consult your local sales representa...

Страница 6: ...shall be sent to Thermo Fisher Scientific in MA or any of their authorized representatives All items must be returned at the customer s cost freight prepaid quoting a return authorization number that is available from the Service department All products or components repaired or replaced under warranty will be returned to the customer at Thermo Fisher Scientific s cost In all cases Thermo Fisher S...

Страница 7: ...s and all safety warnings marked on the instrument must be observed when using it otherwise personal injury or even threat to life may be caused In order to ensure that the protection provided by this instrument is not damaged do not install or operate this instrument in any way outside the scope listed in this manual Do not use the instrument in any environment not specified in this manual Before...

Страница 8: ...sed bottle are unblocked Ensure that you have obeyed applicable specifications for accident prevention Substances shall be disposed properly according to applicable local laws and regulations Grounding Warning When the product is marked with this symbol it indicates the location of connecting the grounding wire in case of the connection of wires Overheating When the product is marked with this sym...

Страница 9: ...Thermo Fisher Scientific Inc Specifications Table 2 Specifications of Orion 8010cX Ammonia Analyzer Measuring performance Range of measurement Range 1 0 02 2 mg L Range 2 0 1 15 mg L Range 3 0 5 30 mg L Range 4 2 100 mg L Range 5 30 500 mg L Five ranges in total Accuracy Range 1 0 02 2 mg L 3 0 04 mg L of the reading Range 2 0 1 15 mg L 3 0 1 mg L of the reading Range 3 0 5 30 mg L 3 0 2 mg L of t...

Страница 10: ...4 9 Chroma Platinum cobalt colorimetry 180 Instrument installation Housing protection class IP65 Case size W x H x D 450 mm x 737 mm x 322 mm 17 7 inches x 29 inches x 12 7 inches Transportation weight 40 kg 88 lbs Electrical parameters Requirements for power supply 100 240 V AC 100 W 50 60 Hz Data and control Current output two circuit 0 4 20 mA outputs maximum load of 900Ω Dry contact output 2 d...

Страница 11: ...of Ammonia Analyzer Note If a refrigerator is provided on site the reagent 2 must be stored in the refrigerator to prolong its service life 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 Flow cell optional 5 Instrument housing 2 Standard solution bottle Reagent bottle 6 USB port 3 Mounting panel base plate 7 Touch screen 4 Signal...

Страница 12: ...erfere with the measurement of ammonia When primary amine exists in water the test result will be on the higher side When water contains reducing substances the test result will be on the lower side Orion 8010cX Ammonia Analyzer includes the following systems 1 Electrical Control System 2 Water Sample Analysis System The Electrical Control System includes the power supply module measurement interf...

Страница 13: ...n of installation position Refer to the Specifications for the temperature and relative humidity requirements of the installation environment It is suggested to install the instrument in an instrument housing a protective case or an analysis room The temperature shall be controlled within 20 10 C and the maximum humidity without condensation is less than 95 Orion 8010cX Ammonia Analyzer has IP65 p...

Страница 14: ...ation of the instrument especially when installing external cables do not discard the rubber sealing covers on the side of the instrument External cables need to pass through these rubber sealing covers to maintain the integrity of the IP65 enclosure Schematic Diagram of on site instrument installation Figure 5 Schematic Diagram of On site Installation of Ammonia Analyzer Note This instrument need...

Страница 15: ...the wall hanging board in the assembly to the wall with expansion screws at least 4 expansion screws are needed and it is recommended to use more than 6 expansion screws Then take out two hangers from the assembly and fix them at the corresponding positions on the back of the ammonia nitrogen detector with M8 screws and gaskets Finally the instrument is secured on already fixed wall mounting brack...

Страница 16: ...per cover 1 3 Flow cell filter screen 1 Stainless steel mine sieve 200 microns 4 Upper cover connector 1 5 Flow cell plug 1 G1 2 external thread plastic 6 Pan head screw 2 M4 40 stainless steel 7 Quick connector 1 G1 2 external thread to gas tubes of 10 mm outer diameter stainless steel 8 Elbow fitting 2 G1 2 external thread to 19 5 mm elbow fitting plastic 9 T shape fitting 1 T shape equal diamet...

Страница 17: ...escription of flow cell installation steps 2 Water sample incoming and outgoing is controlled by the Ammonia Analyzer Description of flow cell installation steps The electric ball valve shall be purchased by the user a Use the 4 X 40 screw in the accessories to lock the Flow Cell to the side of the case b Connect the hose from the proportional sampler to the quick connector at the bottom of the Fl...

Страница 18: ...eter tee fitting at the other end of the steel wire reinforced hose and insert it as deep as possible g Insert the both ends of a section of steel wire reinforced hose into the elbow fitting on the side of the Flow Cell and the T type tee fitting on the bottom as shown below and insert it as deep as possible h Place the four hose clamps at the connection of the T fitting box steel wire reinforced ...

Страница 19: ... threads DN15 and 24 V and is installed at the water inlet of the flow cell For the installation of the electric ball valve refer to Figure 10 Figure 10 Diagram of Electric Ball Valve Installation 1 SW is closed and the valve is open After arriving in place the internal power is automatically turned off and kept in fully open straight through state 2 SW is open and the valve is closed After arrivi...

Страница 20: ...r supply previously connected to the relay Lead the live wire neutral wire and ground wire to the power supply terminal in the instrument electrical box and pay attention to the position of the fuse Insert the wire into the corresponding wiring terminal and tighten the screw All connections must conform to local safety standards Notices during Wiring Make sure that the instrument is not powered on...

Страница 21: ...ly Figure 13 Schematic Diagram of Power Cord Access Port Communication Connection 0 4 20 mA analog signal wiring The instrument provides two circuit 4 20 mA active analog signal outputs through the power control board which can drive a load of up to 900 Ω J23 and J24 are 4 20 mA analog signal wiring terminals see Figure 9 and Table 5 provides the description of corresponding functions Refer to Fig...

Страница 22: ...wer input or internal power of the instrument can be used If external power input is used the external power supply shall be 5 24 V DC If the internal power of the instrument is used pin 3 and pin 4 of J1 and J2 provide a 24 V DC power supply Refer to Figure 16 for specific digital power access Refer to Table 7 for digital signal input wiring Figure 16 Digital Power Access Table 5 J23 and J24 Wiri...

Страница 23: ...nterface typically has a maximum bus length of 1 200 m The actual maximum bus length depends on the signal rate cable characteristics and environmental conditions For example RS485 communication code requires the twisted pair connection If parallel lines are used the maximum bus length will be shortened accordingly Recommended RS485 cables include a 6453 Alpha wire b 3106A Belden Stress relief tre...

Страница 24: ...sing safety problems The liquid leakage sensor is connected to the control circuit of the entire instrument through a connector When the leakage liquid level exceeds the warning position the liquid leakage alarm sensor would give out an alarm signal And for the sake of safety the instrument would automatically stop measuring Only when the error is corrected and the liquid leakage sensor recovers t...

Страница 25: ...t A and Part B Bottles For safety purposes observe the following rules when handling reagents Wear protective clothing or experimental work clothes provided together with the instrument Wear safety goggles face mask or protective gloves Exhaust fans must be installed at the work site In this chapter only glass or high density polyethylene and other materials with good resistance to acids can be us...

Страница 26: ... Schematic Diagram of tubing Connections of Reagent Standard Solution and Deep Cleaning Solution 1 Reagent bottle 1 6 Standard Solution 2 Reagent bottle 3 7 Cleaning waste liquid tube 1 in total 3 Reagent bottle 2 8 Chemical waste liquid tube 1 in total 4 Deep cleaning solution bottle provided by customer 9 Deionized water tube 1 in total 5 Validation solution 10 Tubing of tested water sample 1 in...

Страница 27: ...No Reagent Name Remark Port 1 Deep cleaning solution To deep cleaning solution bottle Port 2 Standard and validation solution common port 3 port valve common port Port 3 Tested water sample port To on site tested water sample Port 4 Measuring cell outlet To measuring cell Port 5 Venthole To atmosphere Port 6 Reaction cell outlet To reaction cell Port 7 Chemical liquid waste port To reaction liquid...

Страница 28: ... the other is connected to the cleaning liquid waste tank It is also required that the liquid waste tube can be correctly connected to the lid of the liquid waste tank to prevent liquid waste from flowing out and causing safety problems Both the deionized water inlet and two liquid waste discharge ports are at the bottom of the instrument so both the deionized water tank and liquid waste tank need...

Страница 29: ...meters of the instrument enter the maintenance mode or conduct analysis and calibration If the automatic initialization option of the system has been set as ON the instrument will be initialized automatically after starting up Please wait patiently for the automatic completion of the initialization step It is recommended that the user shall set the automatic initialization option as ON Such settin...

Страница 30: ... structure of Ammonia Analyzer will be slightly different between different versions It is suggested that it shall be subject to the actual version Main Interface The analysis main interface includes the navigation bar equipment name time date bar equipment status identification icon user login port icon identification area measurement index and measurement result display area of external output i...

Страница 31: ...ication area is used to display the currently set reaction temperature absorbance measured last time and currently set measuring range Measurement Index and Measurement Result Display Area The area is used to mark the items and test results tested by this instrument In the measurement result display area the unit and current measurement mode of the measurement result can be displayed at the same t...

Страница 32: ...ach time After the analysis is completed the equipment enters the idle state Automatic In this mode the Analysis Cycle can be edited Press Start to start a periodic and continuous analysis The time interval between the start of two adjacent analyses is the set analysis cycle Automatic analysis cycle The analysis cycle can be set as a continuous analysis or any time between 45 minutes and 720 minut...

Страница 33: ...e tube length By this way it is necessary to ensure that the sample can fill the tube after sample pre loaded The pre loaded sample volume setting can be calculated according to the following formula sample tube length 50 1 0 2 mL For example when the sample tube length is 60 cm the pre loaded sample volume is 60 50 1 0 2 1 4 mL The default value of the pre loaded sample volume is 1 2 mL After the...

Страница 34: ...on the verification result exceeds the allowable deviation and the standard sample verification exception handling mechanism automatic calibration etc is automatically activated When the measured variance exceeds the allowable deviation the instrument will conduct an auto calibration and rerun the validation test to ensure the instrument is accurate enough for the measurement Remarks The concentra...

Страница 35: ...alarm records measurement records calibration records and operation records Click different record bars to enter different record query interfaces Alarm Records Alarm records are used to record various alarms and fault events occurring during the operation process of the instrument including the time date event current status of event and alarm code When querying alarm records you can query based ...

Страница 36: ...le specific month date and year can be set When setting a month date and year you can select by clicking the up and down arrows or sliding the corresponding panes of month date and year Click Save to save the settings After saving you can exit or enter other interfaces Time The time formats can be set including the 12 hour system and 24 hour system If you choose a different time format the selecte...

Страница 37: ...art button for verification During verification ensure that the instrument is in the idle state When the user is conducting instrument verification it is recommended that the standard sample shall be purchased from formal channels and used directly or diluted as required During calibration of the instrument the concentration of the standard sample with known concentration shall be within the measu...

Страница 38: ... 1 pre loading reagent 2 pre loading reagent 3 pre loading and deionized water pre loading etc When selecting the corresponding item set the pre loaded volume and then click Start to start tube pre loading Emptying of Reaction Cell and Measuring Cell It is used to emptying the reaction cell and measuring cell After entering the sub item click Start to start the sub process Sample Premixing It is u...

Страница 39: ...tatus position can be changed by switching After the setting is finished click Execute and the ten way valve and reagent switching three way valve will be switched according to the set positions Injection Pump It includes three way valve position injection pump target position injection speed and delay The Left and Right are used to determine whether the valve port at the upper end of the injectio...

Страница 40: ...d last reset time of the ten way valve can be seen When replacing the ten way valve the ten way valve needs to be reset Three way Valve Through the service life interface of three way valve the overall service life current service life and last reset time of the three way valve can be seen When replacing the three way valve the three way valve needs to be reset Heating Equipment It is used to cont...

Страница 41: ... check whether there are bubbles generating in the syringe pump when the push rod of syringe pump is moving downward Regularly check the circuit board and cables on the back of the flow path board for corrosion or damage Regular Maintenance Refer to Table 11 for the regular maintenance plan recommended by Orion 8010cX WARNING Only qualified Thermo Fisher Scientific certified service trained person...

Страница 42: ...ning solution is simply called as the deep cleaning in the instrument menu and this Manual It uses the special cleaning solution to thoroughly clean the sample injection tube buffer ring reaction cell and measuring cell thus eliminating bacteria and removing dirt in the tubeline system During a long term operation of the instrument it is recommended that the user shall conduct a deep cleaning of t...

Страница 43: ...tion of the cleaning Perform the above routine cleaning twice 2 Insert water sample tubeline standard solution tubeline reagent tubeline and deionized water tubeline into a deionized water bottle Click the icon Instrument maintenance Pre load tubeline in the main menu select All set the pre loaded volume to 1 2 ml then click Start and wait for the completion of the pre loading of all tubelines 3 T...

Страница 44: ...he after sales personnel to confirm the fault and repair it 2 Measurement results higher than the upper range limit measurement results lower than the lower range limit W17 W18 1 The measurement result exceeds the selected measurement range re select the measurement range according to the concentration of actual water sample If it is higher than the upper limit of measurement choose a higher range...

Страница 45: ...2 If the temperature of the reaction cell deviates too much from the set temperature the instrument may be failure contact the after sales personnel to confirm the fault and repair it 7 Expiration of service life of injection pump three way valve W4 1 The service life of the injection pump three way valve is designed to be 1 year Extended service will lead to instability of the system abnormal tes...

Страница 46: ...suggested to conduct LED calibration and calibration 12 Adherent objects in sample tube or liquid storage ring 1 Click the manual operation navigation icon to enter the manual operation interface 2 Click Manual Measurement to enter the manual measurement start up interface check the pre loaded sample volume value and check the sample tube length When the ratio of the sample tube length unit cm to ...

Страница 47: ...ic push rod of the syringe pump moves downward check whether there are bubbles generated or a large amount of gas entering inside If so tighten the syringe pump or replace the syringe pump and its black flat gasket 5 After all the above steps have been checked and the problem is solved rerun the analysis procedure to see if the fault has been eliminated If the fault still occurs contact the after ...

Страница 48: ...f the three way valve and whether the reagent back flow occurs at the COM port of the three way valve and at the port 10 of electronic rotary valve if yes the corresponding connection terminals need to be tightened 4 After all the above steps have been checked and the problem is solved rerun the analysis procedure to see if the fault has been eliminated If the fault still occurs contact the after ...

Страница 49: ...been checked and the problem is solved rerun the analysis procedure to see if the fault has been eliminated If the fault still occurs contact the after sales personnel to confirm the fault and repair it 21 Lack of cleaning solution E11 1 Check whether the cleaning solution in the cleaning solution bottle is used up or insufficient 2 Whether the cleaning solution tube has been inserted into the bot...

Страница 50: ...to power off replace relevant parts and try again 3 Cut off the power supply and manually push the big black sliding block under the syringe pump to see if it can move up and down smoothly If not remove the syringe pump and try again If it can move up and down smoothly the syringe pump needs to be replaced or cleaned note that the black flat gasket should not fall off and must be installed back ot...

Страница 51: ...e exceeds the time limit by one month the curve needs to be re calibrated 27 Failure of LED calibration The high value exceeds the limit value E29 1 Check whether the calibration setting concentration is consistent with the current calibration concentration if they are inconsistent conduct the modification and calibration 2 Shut down the instrument remove the LED and PD and observe whether there a...

Страница 52: ...s determine the leakage source and then carry out maintenance see Instrument Diagnosis for specific information 2 Possible causes of liquid leakage Loose tubeline connection terminals leads to leakage of liquid Improper connection of tubes results in leakage of liquid Broken reagent bottles result in leakage of liquid 3 Cracked reaction cell or measuring cell results in leakage of liquid 31 Lack o...

Страница 53: ...tion The requirement of international minimum order amount may vary For more details contact the international coordinator Hazardous Materials Some materials are corrosive oxidizing agents specified by DOT and IATA and may require special marks and treatment In addition the material is forbidden to combine with other products The freighter may incur additional freight charges for handling transpor...

Страница 54: ...failure during the warranty period the manufacturer or the authorized distributor selected by the manufacturer will repair or replace the unqualified product according to the above warranty terms or refund the purchase price of the product The warranty mentioned above is the only warranty certificate of Thermo Fisher Scientific for the product All other forms of warranties whether statutory expres...

Страница 55: ...8010RFG220 220 V Reagent 2 refrigerator mainly applicable to Chinese and European markets 8010RFG115 115 V Reagent 2 refrigerator mainly applicable to North American market 8010FSC Floor cabinet can be used to contain refrigerator waste liquid tank and deionized water tank etc 8010PCM Profibus communication module CIC0000126 Flow cell module 8010RE Reagents packet including Reagent 1 Reagent 2A Re...

Страница 56: ...ce to radio communications Operation of this equipment in a residential area is likely to cause harmful interference in which case the user will be required to correct the interference at his own expense Canadian ISED IC Notice This ISM digital apparatus complies with Canadian ICES 001 Cet appareil ISM est conforme á la norme NMB 001 du Canada WARNING Statement EMC Registration is done on this equ...

Страница 57: ... 22 4167 8800 wai asia thermofisher com Japan Tel 81 045 453 9175 wai asia thermofisher com North America Tel 1 978 232 6000 Info water thermofisher com Singapore Tel 65 6778 6876 wai asia thermofisher com Find out more at thermofisher com processwater 2021 Thermo Fisher Scientific Inc All rights reserved All trademarks are the property of Thermo Fisher Scientific and its subsidiaries unless other...

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