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Section 6



Calibration

of the Instrument for Measurement Analysis

42



Thermo Scientific Orion

2230XP Silica Analyzer

Mode of Measurement

The Orion 2230XP Silica Analyzer is designed to provide on-line process measurements, and
has two modes of operation. The mode is always displayed at the bottom right, i.e., below the
Info field and above the status field of the display.

The two modes of the instrument are AUTO restart mode (the instrument resumes auto
analysis mode after 0.5 Hr of inactivity) and MANUAL restart mode. The instrument awaits the
user to initiate the RUN or AUTO ANALYSIS mode by pressing the RUN key.

To change the instrument mode, from MAIN MENU follow the sequence:

MENU

➔

SETUP

➔

(+) ANALYSIS PARAMETERS

➔

MODE

The instrument has two special keys to start and stop the measurement. Pressing the RUN key
starts the auto analysis immediately and analysis repeats at the rate of the time set in
measurement frequency, which is selectable. During this mode, the instrument displays RUN
MODE indicating that the instrument is running continuously.

To edit the measurement frequency, from the MAIN MENU follow the sequence:

MENU

➔

SETUP

➔

(+) ANALYSIS PARAMETERS

➔

SAMPLE

FREQUENCY

The STOP key aborts the measurement at any stage irrespective of the mode of the instrument.

NOTE:

RUN is not the mode of the instrument. It indicates that the instrument is
performing measurement continuously, at the rate of measurement
frequency.

Auto Restart Mode

The default mode of the instrument is auto restart. In this mode, if the instrument keypad is
untouched (i.e. stays idle) for the period of auto restart idle time (default value of 30 minutes),
then it automatically starts the measurement, the mode is displayed as RUN MODE and
repeats the measurement as per the measurement frequency set in analysis parameters.

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Содержание Orion 2230XP

Страница 1: ...Thermo Scientific Orion 2230XP Silica Analyzer 271539 001 Revision A March 2016 User Manual ...

Страница 2: ......

Страница 3: ...ntal Considerations 17 Mounting the Instrument 17 Plumbing Connections 19 Installing Peristaltic Pump Head Tubing 20 Installing the Reagents 22 Connecting Power to the Analyzer 22 Analog Outputs Connections 24 Alarm Connections 24 Inputs Signal Connections 27 Communication Signal Connections 27 Section 4 28 Startup and Operation 28 Executing a manual calibration 29 In Auto Calibration mode 29 Plac...

Страница 4: ...1 Mode of Measurement 42 Auto Restart Mode 42 Manual Restart Mode 43 Measurement Cycle 44 Cell Wash 44 Sample Capture 44 Optics Testing 44 Checking Reaction Temperature 45 Blank Measurement 46 Add Reagents 46 Collect Data 47 Post Wash 47 Measurement Data 48 Printing Results 48 Section 7 49 Menu Overview 49 Setup Menu 50 Measurement Menu 51 View Data and Alarms Menu 52 Service Menu 53 System Admini...

Страница 5: ...and By Mode and Extended Shutdown 71 SECTION 10 76 Standby and On Demand Modes 76 Overview 76 Factory Setup Recommendations When Operating In ON DEMAND Mode 78 SECTION 11 79 Customer Services 79 Notice of Compliance 79 Declaration of Conformity 80 Warranty Information 81 Warranty Shipments Returns Adjustments 82 Consumables 82 Assistance 82 ...

Страница 6: ...nt These warnings identify areas of potential hazard which could result in personal injury or loss of life To ensure that the protection provided by this equipment is not impaired do not use or install this equipment in any manner other than that which is specified in this manual Do not use this product for any purpose other than described in this manual Disconnect power before servicing and prior...

Страница 7: ...ot and should not be touched without care EARTH Ground This symbol when noted on the product identifies the location of the connection for Protective Earth ground NOTE Indicates important information that requires special attention Specifications General Display Graphic LCD 120 mm x 92 mm 4 7 in x 3 6 in Enclosure Fluidics IP 65 NEMA 4X Electronics IP 52 NEMA 12 rated for indoor installation Dimen...

Страница 8: ...ays with 250 VAC 2A resistive contact ratings Outputs Each relay may be configured separately to a list of programmable alarm functions Inputs Two isolated analog outputs 0 4 20mA max load 900 ohms Environmental Storage Temperature Range 5 45 C 41 113 F Operating Temperature Range 5 45 C 41 113 F Relative Humidity 90 at 40 C 104 F non condensing Altitude Up to 2000 m Sample Requirements Inlet Pres...

Страница 9: ...own reacted standard The colored compound absorbs energy at a specific wavelength in accordance with the Beer Lambert Law The instrument uses Light Emitting Diodes LEDs that emit light at a narrow bandwidth selected for the specific application The Silica analysis method uses the near infrared LED NIR at 810 nm Unpacking the Instrument Remove the analyzer from its shipping carton and inspect it fo...

Страница 10: ...strument Startup Procedure 1 Power on instrument 2 To allow longer lifetime of unit the pinch valve and pump head tubing are not fully engaged when the unit is shipped Refer to Plumbing Connections Section a Reset tubes in pumps heads Note This step must be repeated for all three pump heads i Remove tape ii Slide tube retainer into place along keyway iii Install tubing cover by squeezing both side...

Страница 11: ...fer to Section 4 Additional detail can be found in the following sections Section 4 Instrument Operation Section 5 Analyzer Hardware Configuration and Calibration Section 6 Calibration of the Instrument for Measurement Analysis Section 7 Menu Overview Section 8 Terms Definition Section 9 Maintenance Schedule General Product Description This User Manual provides the information necessary to obtain ...

Страница 12: ...d process analyzing It is designed for long life under continuous rigorous use The Orion 2200 series analyzers are designed for accommodating several applications Each application requires a specific configuration in hardware and software that is set at the factory The product as supplied will have a configuration sheet detailing the setup and the detailed tests and validation that were conducted ...

Страница 13: ...s information instructions to navigate 7 USER field shows current user name 8 MODE field shows whether the instrument is working in Auto Manual or Run mode 9 STATUS field shows current working status of the instrument 10 FUNCTIONAL KEYS ASSIGNMENT FIELD shows the functions allotted to the functional keys 11 FUNCTION KEYS select functions 12 OPERATIONAL KEYS are meant for operation of the instrumen...

Страница 14: ...In measurement mode the instrument displays current and previous readings units date and time The measurement results can be displayed as large size fonts or normal size fonts F1 key will toggle between large and normal fonts NOTE In AUTO mode the user can navigate between different menus even though the instrument is performing a measurement or a calibration Figure 1 Orion 2230XP Silica Analyzer ...

Страница 15: ...which is the reacted mixture of the sample with the reagents absorbs energy at a specific wavelength in accordance to Beer Lambert Law Fluids Storage Store all reagents and standards in a dark place at room temperature Calibration Standard Standard part 223020 the calibration standard required for this application is a 200 ppb solution Each calibration cycle consumes approximately 50 mL Each bottl...

Страница 16: ...U option and then PRIME FLUIDICS AUTO PRIME ENTER The instrument will go through a priming sequence of all the available solution to the analyzer Follow the startup procedure described in Section 4 You may repeat the AUTO PRIME sequence as necessary to purge out any trapped bubbles in the lines Reagent Consumption The Silica analysis requires three reagents The reagent usage depends on the frequen...

Страница 17: ...ument grade with over voltage protection and a provision for disconnecting power Mounting the Instrument The instrument case is designed for wall or panel mounting Use four 10 screws or equivalent for proper support Refer to Figure 2 and Figure 3 for dimensions in mm and inches Make sure that the wall that you choose can support the weight of the instrument approximately 20 kg or 44 lbs See Figure...

Страница 18: ...SER TO INSTALL A 40 to 60 MICRON FILTER SIZE IS BASED ON SAMPLE CONDITION SET FLOW RATE BETWEEN 50 TO 500 ML MIN AC POWER SAMPLE CHAMBER SAMPLE BACK N C STANDARD FRONT N O RGT1 RGT3 STD RGT2 RGT3 DRAIN SAMPLE INLET RGT1 Figure 2 Mounting dimensions SAMPLE CHAMBER SAMPLE IN 1 4 SAMPLE RETURN 1 4 DRAIN 3 8 VENT LINES AIR PURGE AIR PURGE AIR VENT I O SIGNALS POWER IN ALLOW 20 INCHES 510 mm CLEARANCE ...

Страница 19: ...he bottom of analyzer require in OD 6 mm OD flexible tubing The drain fitting at the bottom of the analyzer requires in OD 9 6 mm OD flexible tubing The air purge inlets require in OD tubing The air purge supply must be filtered externally and free of oil and any other particulates Figure 3 Typical external plumbing connections SAMPLE IN SAMPLE RETURN FLOW DIRECTION FILTERED AND OIL FREE AIR PURGE...

Страница 20: ...ristaltic Pump Head Tubing Press the STOP key Disengage the U shape pressure plate of the pump head assembly by pressing with two fingers and gently move upside as shown in Figure 6 Slide the tube fitting retainers at each side as shown in Figure 5 Replace the old tube by sliding off the barbed fitting If necessary clean the pump rollers Lubricate the tubing with a pea sized quantity of silicone o...

Страница 21: ...ntific Orion 21 Repeat above steps for all pumps You can test the pump under Diagnostics menu for proper operation MENU SERVICES DIAGNOSTICS PUMPS VALVES STIRRER Figure 5 Installing peristaltic pump head tubing Dual channel Figure 6 Installing peristaltic pump head tubing Single channel ...

Страница 22: ... touching any electronic components such as printed circuit cards and the components on them you should discharge static electricity from your body This can be accomplished by touching an earth grounded metal surface such as the chassis of an instrument metal conduit or pipe The analyzer is equipped with a three terminal power connector strip located in the electronics enclosure as shown in Figure...

Страница 23: ...cation of the fuse Insert the wire into the terminal connector and make sure to tighten the screw Route signal connections to the back hub and power connections separately to the front hub All connections must conform to local safety standards Analyzer Terminal Destination North America Wire Color European Wire Color HOT or L Line black brown Protective Earth Ground PG green green with yellow trac...

Страница 24: ...d according to application needs The outputs have a common isolation from the main system and can drive up to a 900 Ohms load Please refer to Figure 9 page 26 and Table 2 page 27 for signal terminal connection detail Alarm Connections The analyzer has five level sensor inputs that accept a dry contact closure signal to indicate the state of the level sensors Input 5 is typically assigned for sampl...

Страница 25: ...Analyzer Thermo Scientific Orion 25 RELAY contacts are rated at 250V 2A AC 500W non inductive load All inputs except IN 6 7 must be connected to POTENTIAL FREE contacts Figure 9 Terminal strips for analog and relay outputs Figure 10 Communication ports Ethernet RS 232 ...

Страница 26: ...Digital input 6 return External 1 control return 13 in7 Digital input 7 live External 2 control 14 rTn Digital input 7 return External 2 control return 15 24V 24V DC live limited to 20 mA source 16 GnD 24V DC ground 17 Earth Ground System earth ground 18 GnD Analog output 1 ground 19 OUT1 Analog output 1 900 Ohms Max 20 Earth Ground System earth ground 21 GnD Analog output 2 ground 22 OUT2 Analog ...

Страница 27: ...igital input 6 live 12 Digital input 6 return 13 Digital input 7 live 14 Digital input 7 return 15 24V DC live 16 24V DC ground Input 6 is assigned by default to RUN STOP function with Close Open of a dry contact Input 7 is left unassigned by default Dry contact voltage free contact The functionality along with the state of the enabling signal is programmable by the user Communication Signal Conne...

Страница 28: ... a calibration is a number that the analyzer uses to determine the sample concentration The particular value of this number is not important but it should be within 5 of the corresponding value in the Quality Control Report If so you can be confident that all subsystems of your analyzer are working properly Before proceeding please make sure of the following The reagent bottles 1 2 and 3 are full ...

Страница 29: ...e is within 5 of your system QC report then the system is operating properly and ready for running sample analysis If the data is different repeat the calibration cycle before proceeding further Executing a manual calibration If the result is outside the user specified tolerance default 5 the Analyzer will warn the user to avoid storing the wrong calibration data The user may then ACCEPT or REJECT...

Страница 30: ...nalyzer s calibration accuracy at any time using the validation function Validation consists of running a single measurement cycle and reporting the result in concentration This reported result can then be compared to the expected value which is the known concentration of the validation solution to determine the accuracy of system calibration The advantage of using this function over the Run Analy...

Страница 31: ... tubing lines to the reaction measuring cell Sample Analysis and Validation The SAMPLE ANALYSIS mode is similar to the calibration mode with the exception that during calibration the instrument calculates the relevant parameters correlating to the standard concentrations used for calibration During sample analysis the system relies on the CURRENT calibration parameters to calculate the sample conc...

Страница 32: ...on A cleaning cycle can be performed by pressing STOP MENU MEASUREMENT CLEAN This cycle helps maintain clean reaction cell NOTE To avoid damage and contamination to the reaction cell use only cleaning solutions recommended by the factory Post Wash Automatic post wash cycles are typically part of every measurement cycle At the end of the analysis the post wash cycle evacuates the reacted sample fro...

Страница 33: ... Orion 33 The Prime Volume may be specified as a number this allows the user to pump back the reagents inside the tubing back into the reagents containers allowing for safer service when replacement of the tubing is needed User may select to pull back all or any one of the reagents or standard ...

Страница 34: ... Analyzer optics consists of a NIR LED light path and a photo detector The analyzer is capable of driving three LED and the intensity of each of the LED can be individually varied The light path is preset in the reaction cell sample chamber The photo detector receiving the light energy is connected to an amplifier with programmable gain The output of the photo detector amplifier is digitized and m...

Страница 35: ...from the LED present in the system along with tuning the front end detection to maximize the signal levels with de ionized water in the cell The system stores all the parameters for the application The calibration results are available for editing From the MAIN MENU follow the sequence MENU SERVICES HARDWARE SETUP EDIT CALIBRATED VALUES The stray light measurement is listed as OPTICS DARK the opti...

Страница 36: ...er uses peristaltic pumps to move fluids through the reaction cell The pump tubing will require replacement periodically Please refer to Chapter 9 for details The maximum rate of flow of the fluid is dependent on both the inner diameter of the tubing conveying the fluid and the rpm of the pump The pumps are used to move the following fluids sample standard and reagents WHEN REPLACING WITH SAME TYP...

Страница 37: ...ATE ANALOG OUTPUTS The user is asked to connect a 900 ohms resistor to each two analog outputs The calibration requires the use of a current meter 0 100 mA range placed in series with the output under test The user may select one output at a time for calibration The calibration starts by adjusting the full scale to 20mA The buttons are used to adjust the output to 20mA The instrument waits for the...

Страница 38: ...esult with the absorbance of light through a standard solution of known concentration The Method of Analysis defines the detection wavelength for Silica It is set at 810 nm Theory of Calibration Using two known standards one of low concentration and the other of high concentration the absorbance for each concentration is measured and the slope and intercept are calculated from the calibration curv...

Страница 39: ...LINE For Calibration from the MAIN MENU follow the sequence MAIN MENU MEASUREMENT CALIBRATE CALIBRATE STANDARD Single Point Calibration For single point calibration typically the intercept value is zero Therefore Concentration Slope x Absorbance The technician may modify the intercept value The analyzer uses a 200 ppb concentration standard solution for calibration The absorbance of the standard s...

Страница 40: ...is calibration is only allowed in manual mode with user prompts and confirmation required at the end of the cycle Extended range calibration MENU SETUP CALIBRATION PARAMETERS Set the STANDARD CONC 3000 ppb for a 0 to 5000 ppb range And execute a manual calibration MAIN MENU MEASUREMENT CALIBRATE CALIBRATE STANDARD When the system detects a high absorbance level of the reacted solution above the se...

Страница 41: ...wavelength of light through the sample and comparing the result with the absorbance of the same wavelength of light through a standard solution of known concentration If the two absorbencies match then the sample concentration is equal to the standard solution To facilitate the comparison the analyzer is first calibrated with standards to determine the slope and intercept of the range of concentra...

Страница 42: ...sing the RUN key starts the auto analysis immediately and analysis repeats at the rate of the time set in measurement frequency which is selectable During this mode the instrument displays RUN MODE indicating that the instrument is running continuously To edit the measurement frequency from the MAIN MENU follow the sequence MENU SETUP ANALYSIS PARAMETERS SAMPLE FREQUENCY The STOP key aborts the me...

Страница 43: ... key during measurement gets back to the MANUAL RESTART mode In this mode if the instrument is untouched for a period of the standby mode idle time 60 minutes default it switches to standby mode During standby operation all fluidics devices are shut down and the analyzer goes into a standby housekeeping mode in which the pumps and the valves are activated on an hourly basis to prevent tube pinchin...

Страница 44: ...sequence MENU SETUP METHOD CELL WASH VOLUME In cell wash volume the positive volume is to pump the sample into the reaction cell and the negative volume is to pull back an amount below the drain after the cell wash is completed During the cell wash the stirrer is on and the info field if enabled shows the sample pumping progress with a progress bar along with the volume pumped Sample Capture In th...

Страница 45: ...re When reaction cell temperature control is enabled at this stage in the cycle the reaction cell temperature is tested against the set point To enable or disable the REACTION TEMPERATURE CONTROL from the MAIN MENU follow the sequence MENU SETUP METHOD REACTION TEMPERATURE CONTROL If reaction temperature control is enabled then the temperature set point is editable To edit the temperature set poin...

Страница 46: ...Y CRITERIA During this stage the info field if enabled shows the blank measurement progress bar with the BLANK ABSORBANCE reading in AU This is a relative value and NOT an absolute value For the silica measurement the event of blank measurement and its sequence in the measurement cycle is done before adding the third color developing reagent NOTE When unstable and not meeting the stability criteri...

Страница 47: ...he choice of editing the stability criteria To do this from the MAIN MENU follow the sequence MENU SETUP ANALYSIS PARAMETERS STABILITY CRITERIA Now the concentration is calculated as follows and the current concentration is updated Concentration Slope x Absorbance Intercept Where slope and intercept are from the CURRENT calibrated values of the instrument for measurement NOTE If unstable and doesn...

Страница 48: ...ercept temperature wavelength and status The stored results are displayed with respect to the selectable period of time such as Last 12 Hours Last 1 Day Last 2 Days Last 3 Days Last 1 week Last 2 weeks Last 3 weeks Last 4 weeks All which is selected as DATA RANGE To display the measurement results from the main menu follow the sequence MENU VIEW DATA AND ALARMS REVIEW ANALYSIS RESULTS DISPLAY NOTE...

Страница 49: ...nalysis calibration validation and cleaning cycles View Data and Alarms For reviewing the collected data of up to the last 31 days in text and graphics mode and for reviewing and resetting the various Alarms and Faults triggered during the latest cycle performed Services For system administration hardware setup prime fluidics and diagnostics and control of the various devices including LED pumps v...

Страница 50: ...ations repeats The new calibration results are tested against the reference calibration parameters listed under the REFERENCE column The CURRENT column shows the current operating parameters that are being used by the instrument when calculating the analysis measurement result Calibrations are similar to analysis cycles and are on the method set in METHOD PARAMETERS menu Validation Parameters Menu...

Страница 51: ... Power Failure Menu Allows configuration of the instrument after power failure recovery Ethernet Parameters Menu Allows configuration of Ethernet Parameters RS 232 Parameters Menu Allows selection of the BAUD RATE for the RS 232 port Default setting of 115200 Baud Language Menu Allows configuration of the instrument s language Current release is ENGLISH language Consult factory for other languages...

Страница 52: ...s Allows the user to review and print the calibration results from the stored calibration database using a selectable time scale The database holds data from the last 31 days Review Analysis Results Allows the user to review and print the analysis results from the stored analysis database using a selectable time scale The selected results can be displayed in text or graph modes The database holds ...

Страница 53: ... components of the analyzer Calibration results are editable by the technician Prime Fluidics Menu Allows user to prime the fluidics lines of the analyzer Diagnostics Menu Diagnostics provide a direct mechanism to individually test devices such as pumps valves relays optics and stirrer Turn various pumps and valves ON and OFF for testing or during adjustment Maximum of two devices can be turned on...

Страница 54: ...hnician to enable disable online printing See Appendix A for the default analyzer parameters listing printouts Hardware Setup Menu Calibrate Thermistor Allows technician to calibrate the thermistor Only required if the factory installed thermistor has been serviced or replaced To calibrate the thermistor user is required to enter the reaction block temperature using an external reference thermomet...

Страница 55: ...ts and its value may vary between 0 to 10 Default value is 1 0 PLEASE NOTE THE SIGN Diagnostics Menu Pumps Valves and Stirrer Allows technician to selectively check the functionality of the pumps valves and stirrer Inputs Status Allows technician to check the status of the external inputs Once a function has been assigned to a digital input it disappears from the next menu of available functions f...

Страница 56: ...etector Control Allows the technician to check the functionality of the optics system and its individual components Also allows adjusting the detector preamp gain for the selected LED Any new setting of the gain or of the intensity of the LED will override any previous optics calibration setting CONSULT FACTORY before overriding any setting This diagnostics menu allows direct reading of the mV lev...

Страница 57: ...tup Relays Mapping Validate Review Analysis Results Prime Fluidics Analog Outputs Clean Delete All Calibration Results Diagnostics Inputs Delete All Analysis Results Display Parameters Temperature Units Page 2 Analysis Parameters Validation Parameters Cleaner Parameters Calibration Parameters Method Page 3 Date Time Daylight Saving Recovery After Power Failure Ethernet Parameters RS232 Parameters ...

Страница 58: ...Serial Number Clean Review Analysis Results Unit Label Change Press Enter Display Printing Options Print System Configuration View Graph Print Analysis Parameters Print Print Method Parameters Data Range Selection Print Cleaner Parameters Delete All Calibration Results Online Print Enable Disable Delete All Analysis Results Hardware Setup Calibrate Thermistor Calibrate Pumps Pump 1 2 3 4 Calibrate...

Страница 59: ...Address Level Sensors Sensor 1 5 Stability Criteria Dilution Parameters Server IP External Inputs Input 1 2 Validation Parameters RS232 Parameters Display Parameters Validation Source Baud Rate Contrast No of Repeats Language Back Light On time Cleaner Parameters Display Help Cleaner Source Display Info Volume to Add Result Decimal Point Clean Flow Rate Large Font Screen Stir Time Temperature Unit...

Страница 60: ...X Value depends on precision selected in Setup Display parameters result Decimal Point RELAY Up to FOUR spare relays available MODE Allows fault ON or OFF operation Normal or Fail Safe ANALOG OUTPUT Type Normal or reverse acting 0 to 20 4 20 20 0 or 20 4 Low Low concentration value High High concentration value EXTERNAL INPUT Label User programmable label Event Dry contact event Close Open or Open...

Страница 61: ... The CURRENT Slope value represents the coefficient that is multiplied by the absorbance to calculate the concentration of the sample Intercept value Intercept Reference and current numbers based on the base line calibration cycle Default value of 1 Calibration Tolerance Repeat tolerance tested during auto calibration cycles to accept or reject automatic calibrations Default value of 5 VALIDATION ...

Страница 62: ...cleaning the cell Sample Reagent Cleaner Standard Not Assigned Volume to add The amount pumped for cleaning 0 to 255 mL Clean Flow Rate The rate at which the cleaner source is pumped to clean the cell Depends on the inner diameter of the pump tubing It is derived from the calibration of pumps Stir Time The amount of time the fluid is stirred for cleaning the cell 0 to 999 seconds Frequency The tim...

Страница 63: ...5200 default LANGUAGE Language Language in the instrument English other languages consult factory REVIEW RESET ALARMS Reset All Alarms Resets all the raised alarms which are shown below this option Reset All Alarms Reset All Faults Resets all the faults which are shown below this option None REVIEW CALIBRATION RESULTS Display Displays the calibration results for the selected data range None Print ...

Страница 64: ...Add a new user to the users list User name is 6 characters long and only 6 users are allowed Password Password of the new user entered 6 characters long A Z 0 9 and space are allowed Measure Permission Measurement permission for the new user Enabled Disabled Calibrate Permission Calibration permission for the new user Enabled Disabled Validate Permission Validation permission for the new user Enab...

Страница 65: ...0 mV PRIME FLUIDICS Priming Volume The volume of the fluid selected for priming 0 to 99 9 mL PUMPS VALVES STIRRER Pump1 Pump2 Pump3 To check the functionality of pumps ON OFF Valve1 Valve2 Valve3 To check the functionality of valves ON OFF Stirrer To check the functionality of stirrer ON OFF RELAYS Relay1 Relay2 Relay3 Relay4 To check the functionality of relays ON OFF ANALOG OUTPUTS Channel1 Chan...

Страница 66: ...s CAUTION Wear gloves or protective equipment your site may require when changing reagents Press the STOP key Press the MENU key Remove the cap from each bottle and change them over one by one Do NOT re use or re fill old or existing bottles Dispose of the used bottles and contents safely and according to local regulations Tighten bottle caps and route the tubing properly making sure that it does ...

Страница 67: ...described below Press MENU and scroll down to SERVICES and then select PRIME FLUIDICS and then set the PRIMING VOLUME to 5 mL This step allows the user to pump back the reagents contents of the connecting tubing including the peristaltic pump tubing Scroll up to each of the reagents and press ENTER to pump back the selected reagent fluid into its container Repeat for each reagent 1 2 3 Disconnect ...

Страница 68: ...FLUIDICS menu the sign for the priming volume will be reset to upon next menu entry SAMPLE STANDARD Reagents 1 2 and 3 Pumps PUMP larger tubing OD smaller tubing OD all the same Always use 2 drops of Silicone Oil on the platen before replacing on pump Figure 14 Maintenance kit assembly detail ...

Страница 69: ...ipe A1 and A2 to fill the cell with cleaning solution and let it soak for about hour For a more thorough cleaning swing the reaction cell down as shown in photos below and use a non fiber swab with a bent tip reach inside the reaction cell and wipe the side optical windows of the cell and the inner surfaces to dislodge and remove any deposits Cleaning of the reaction cell should be performed month...

Страница 70: ...o a 1 liter measuring cylinder and make to the mark with more high purity water Mix well and store in a tightly sealed plastic bottle Recipe A2 Extra Strength Cleaning Solution for troubleshooting and more intense Cleaning To prepare 1 liter of extra strength cleaning solution 1 Dissolve 50 g of analytical grade sodium hydroxide pellets NaOH in approximately 600 ml of high purity water in a plasti...

Страница 71: ...of the float level sensor The sample chamber is located on the right lower corner of the fluidics enclosure The chamber can be removed for service and clean up Stand By Mode and Extended Shutdown To put the System in Stand by mode make sure to press the STOP key and check the DISPLAY field next to F4 to show MANUAL RESTART If AUTO RESTART is selected you need to set the mode to Manual MENU SETUP A...

Страница 72: ...progress Trying to perform measurement when it is already under way Wait for measurement to complete User programmable measuring frequency Editing option of analysis frequency is selected Edit the analysis frequency User programmable calibration frequency If same type of solution is assigned to two or more inputs Edit the calibration frequency Two or more inputs are of same type If same type of so...

Страница 73: ...nt3 empty Performing Analysis Calibration Validation with two or three Reagents and Reagent3 is exhausted Fill the empty reagent3 bottle with Reagent3 Reagent1 Reagent2 are empty Performing Analysis Calibration Validation with two or three Reagents and Reagent1 2 are exhausted Fill the empty Reagent1 2 bottles with Reagent1 2 Standard empty Performing single point or baseline calibration and the S...

Страница 74: ...able to reach the set point and is above the set point Re calibrate the Thermistor Try a different set point temperature Call a service agent Taking blank measurement unstable signal Unstable temperature Cell may be coated or may be due to Optics failure Perform Clean Cycle and Calibrate Optics and thermistor Collecting data unstable signal Unstable temperature or cell may be coated or may be due ...

Страница 75: ...log Number Description Maintenance and Service Items 2230XPMK Maintenance Kit for 2230XP 2230PA Pump Head Tubing Covers 3 each 2230PS Power Supply Assy 2230FS Power Fuses 2230PI Air Purge Fittings 2230XPTK Main Tubing Kit for 2230XP 2230BC Empty Auto Cal Btl Validation Sample Bottle 2230SF Fittings Sample In Sample Out and Drain 2230RC Reagent Bottle Cap includes fittings 2230SC Standard Bottle Ca...

Страница 76: ...equipped with two modes of operations 1 AUTO RESTART mode default 2 MANUAL mode The mode of operation may be selected by the user by pressing the MENU key SET UP pg2 ANALYSIS PARAMETERS MODE AUTO RESTART allows automatic restart of the sample measurement mode same as pressing the RUN key after 30 minutes wait idle time The unit will resume running analyses per the selected frequency default 15 min...

Страница 77: ...stem will run four clean cycles per day and will not consume any standard Note that in stand by mode the standard is used only to flush the cell Distilled water may be substituted instead of silica standard or a time to refill the standard bottle if unit is kept in stand by CAUTION Make sure reagents and standard bottles have enough fluids to maintain wet lines when the analyzer is kept in stand b...

Страница 78: ...mode the analyzer will switch to stand by after one hour of inactivity after receiving the STOP command MENU SETUP pg 2 ANALYSIS PARAMETERS MODE Select MANUAL mode 2 Program external control input 6 MENU SETUP INPUTS EXTERNAL INPUTS INPUT 6 Press the down key to select ACTION RUN STOP Refer to Manual Inputs Signal Connections Section for additional wiring details By using the ON OFF external remot...

Страница 79: ...f FCC Rules which are designed to provide reasonable protection against such interference in a commercial environment Operation of the analyzer in a residential area may cause interference in which case the user at his own expense will be required to take whatever measures may be required to correct the interference This Class A digital apparatus complies with Canadian ICES 003 Cet appareil numéri...

Страница 80: ... EC Low Voltage Directive EN IEC 61010 1 2010 EMC 2004 108 EC Electromagnetic Compatibility Emissions and Immunity EN 61326 1 2006 This Thermo Scientific Orion product has been manufactured in compliance with the provisions of the relevant manufacturing and test documents and processes These documents and processes are recognized as complying with ISO 9001 2008 by QMI SAI Global listed as File 001...

Страница 81: ...ice to maintain the warranty Parts not in contact with sample for a period of one 1 year from the date of shipment Peristaltic pump tubing for a period of thirty 30 days under normal operation The following user serviceable parts are not warranted Probes O rings THE WARRANTIES DESCRIBED ABOVE ARE EXCLUSIVE AND IN LIEU OF ALL OTHER WARRANTIES WHETHER STATUTORY EXPRESSED OR IMPLIED ALL OTHER WARRANT...

Страница 82: ...S United Parcel Service or an equivalent service In all cases Thermo Fisher Scientific or your Thermo Fisher Scientific authorized distributor has sole responsibility for determining the cause and nature of failure and Thermo Fisher Scientific s or the distributor s determination with regard thereto shall be final All parts that are replaced under warranty will become the property of Thermo Fisher...

Страница 83: ...5 1480 Tel 1 978 232 6000 Info water thermo com Netherlands Tel 31 020 4936270 info water uk thermo com China Tel 86 21 68654588 wai asia thermofisher com India Tel 91 22 4157 8800 wai asia thermofisher com Singapore Tel 65 6778 6876 wai asia thermofisher com Japan Tel 81 045 453 9175 wai asia thermofisher com Australia Tel 613 9757 4300 in Australia 1300 735 295 InfoWaterAU thermofisher com Water...

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