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Operating Manual SIGMA 1-6P 

 

 

page 62 of 67 

05/2007 

Resistant at +20 °C

 

 

 

 

 

 

 

 

 

 

 

  

  

   

  

  

  

  

  

  

  

  

  

-  no data 
1 resistant 
2 practically resistant 
3 partially resistant 
4 not resistant 
 

  

Co

n

cen

tratio

n

 

High De

ns

ity

 

Poly

e

thy

le

ne

 

Po

lyamid

e 

Polycarbonate 

Po

lyo

xymeth

y

len

e

 

Poly

propy

le

n

e

 

Po

lysu

lfo

n

e

 

Polyvinyl chlo

ride, hard 

Po

lyvin

y

l ch

lorid

, weak 

Poly

te

tra

fluore

thy

le

ne

 

Aluminum 

Medium 

Formula 

 [%] HDPE PA  PC POM PP PSU PVC PVC PTFE AL

Dipropylene glycol (mono)methyl ether  C

4

H

10

O 

100

3 

1

4 

1 

4 

4 

4 

4 

1 1

Ethyl acetate 

C

4

H

8

O

2

100

1 

1

4 

1 

1 

4 

4 

4 

1 1

Ethylene chloride 

C

2

H

4

Cl

2

100

3 

3

4 

1 

3 

4 

4 

4 

1 1

Ferrous chloride 

FeCl

2

saturated

1 

3

1 

3 

1 

1 

1 

1 

1 4

Formaldehyde solution 

CH

2

O 

30

1 

3

1 

1 

1 

- 

- 

- 

1 1

Formic acid 

CH

2

O

2

100

1 

4

3 

4 

1 

3 

3 

1 

1 1

Furfural 

C

5

H

4

O

2

100

1 

3

3 

2 

4 

- 

- 

- 

1 1

Gasoline 

C

5

H

12

 - C

12

H

26

100

2 

1

3 

1 

3 

3 

2 

- 

1 1

Glycerol 

C

3

H

8

O

3

100

1 

1

3 

1 

1 

1 

1 

2 

1 1

Heptane, normal 

C

7

H

16

100

2 

1

1 

1 

2 

1 

2 

4 

1 1

Hexane, n- 

C

6

H

14

100

2 

1

2 

1 

2 

1 

2 

4 

1 1

Hydrogen chloride 

HCl 

5

1 

4

1 

4 

1 

1 

1 

- 

1 4

Hydrogen chloride 

HCl 

concentrated

1 

4

4 

4 

1 

1 

2 

3 

1 4

Hydrogen peroxide 

H

2

O

2

3

1 

3

1 

1 

1 

1 

1 

- 

1 3

Hydrogen peroxide 

H

2

O

2

30

1 

4

1 

4 

1 

1 

1 

- 

1 3

Hydrogen sulfide 

H

2

S 

10

1 

1

1 

1 

1 

1 

1 

3 

1 1

Iodine, tincture of 

I

2

 

1 

4

3 

1 

1 

- 

4 

4 

1 1

Isopropyl alcohol 

C

3

H

8

O 

100

1 

1

1 

1 

1 

1 

1 

4 

1 2

Lactic acid 

C

3

H

6

O

3

3

1 

3

1 

2 

1 

1 

2 

- 

1 1

Magnesium chloride 

MgCl

2

10

1 

1

1 

1 

1 

1 

1 

1 

1 1

Mercuric chloride 

HgCl

2

10

1 

4

1 

3 

1 

1 

1 

1 

1 4

Mercury 

Hg 

100

1 

1

1 

1 

1 

1 

1 

3 

1 3

Methyl acetate 

C

3

H

6

O

2

100

1 

1

4 

2 

1 

- 

4 

4 

1 1

Methyl alcohol 

CH

4

O 

100

1 

2

4 

1 

1 

3 

1 

3 

1 1

Methyl benzene 

C

7

H

8

100

3 

1

4 

1 

3 

4 

4 

4 

1 1

Methyl ethyl ketone (MEK) 

C

4

H

8

O 

100

1 

1

4 

1 

1 

4 

4 

4 

1 1

Methylene chloride 

CH

2

Cl

2

100

4 

3

4 

3 

3 

4 

4 

4 

1 1

Mineral oil 

— 

100

1 

1

1 

1 

1 

1 

1 

- 

1 1

Nitric acid 

HNO

3

10

1 

4

1 

4 

1 

1 

1 

- 

1 3

Nitric acid 

HNO

3

100

4 

4

4 

4 

4 

- 

4 

- 

1 1

Nitrobenzene 

C

6

H

5

NO

2

100

3 

4

4 

3 

2 

4 

4 

4 

1 1

Oleic acid 

C

18

H

34

O

2

100

1 

1

1 

2 

1 

- 

1 

- 

1 1

Oxalic acid 

C

2

H

2

O

4

 x 2H

2

O 

100

1 

3

1 

4 

1 

1 

1 

1 

1 1

Ozone 

O

3

100

3 

4

1 

4 

3 

1 

1 

- 

1 2

Petroleum 

— 

100

1 

1

3 

1 

1 

1 

1 

3 

1 1

Phenol 

C

6

H

6

O 

10

1 

4

4 

4 

1 

4 

1 

3 

1 1

Phenol 

C

6

H

6

O 

100

2 

4

4 

4 

1 

3 

4 

3 

1 1

Phosphoric acid 

H

3

PO

4

20

1 

4

2 

4 

1 

- 

- 

- 

1 4

Phosphorus pentachloride 

PCl

5

100

- 

4

4 

4 

1 

- 

4 

4 

1 1

Potassium hydrogen carbonate 

CHKO

3

saturated

1 

1

2 

1 

1 

- 

- 

- 

1 4

Potassium hydroxide 

KOH 

30

1 

1

4 

3 

1 

1 

1 

1 

1 4

Содержание 1-6P

Страница 1: ...Laboratory Centrifuge 1 6P Operating Manual From Serial No 119956 Please retain for later use...

Страница 2: ......

Страница 3: ...ngs are executed via the control panel with a coated surface that protects the device against moisture and dust In addition the interior of the centrifuge is also rather easy to clean We offer you a d...

Страница 4: ......

Страница 5: ...d sign e ci dessous est produit et examin conforme aux directives 2006 42 EG 2006 95 EG und 2004 108 EG Bezeichnung der Maschine Laborzentrifuge Machine Laboratory Centrifuge D signation de la machin...

Страница 6: ......

Страница 7: ...ion 18 2 4 1 Special Instructions 18 2 4 2 Resistance of Plastics 19 2 5 Prohibited Centrifuging Operations and Hazard Warnings 19 2 5 1 Special Hazards 20 2 6 Checks by the Operator 21 2 7 Instructio...

Страница 8: ...Centrifuge ON 29 5 2 2 Opening and Closing the Lid 29 5 2 3 Installation of Rotors 30 5 2 4 Installation of Accessories 31 5 2 4 1 Tubes 32 5 2 5 Service Life of Rotors and Accessories 32 5 2 6 Start...

Страница 9: ...eration 41 6 2 4 Lid cannot be opened 42 6 2 5 Emergency Lid Release 42 6 2 6 Error Codes 43 6 2 7 Service Contact 43 7 Care and Maintenance 44 7 1 Cleaning and Care 44 7 1 1 Centrifuge 44 7 1 2 Acces...

Страница 10: ...53 11 1 1 Relative Centrifugal Force RCF 53 11 1 2 Density 53 11 1 3 Speed Gravitational Field Diagram 53 11 2 Declaration of Decontamination Return Declaration 55 11 3 Resistance Data 61 12 Index 65...

Страница 11: ...regulations for the prevention of accidents must be complied with 1 2 Intended Use Centrifuges are power driven machines that separate liquids from solid matter liquid mixtures or solid mixtures by c...

Страница 12: ......

Страница 13: ...age locations 10 sec 11 h 59 min short run continuous run 10 Physical data Depth mm Width mm Height mm Weight kg EMC as per EN 61326 Noise level dBA 320 240 245 13 Class B 58 Notes by the user please...

Страница 14: ......

Страница 15: ...V Part no 70102 for 100 120 V Documentation Operating manual incl EU Declaration of Conformity page 5 Equipment Decontamination Certificate page 59 Accessories according to your order our order confi...

Страница 16: ...bindung Off Power Arr t mise hors tension Schutzleiteranschluss Protective earth ground Liaison la terre Erde Earth ground Terre Netzstecker ziehen Unplug mains plug Tirer la fiche de prise Vorsicht Q...

Страница 17: ...otes on Safety The operating manual is an integral part of the product Please retain the operating manual throughout the service life of the centrifuge Please hand the operating manual over to any sub...

Страница 18: ...e installation of accessories see 5 2 4 Installation of Accessories page 31 2 4 1 Special Instructions If liquids with a density 1 2 g cm3 are used reduce the speed see 11 1 2 Density page 53 Protecti...

Страница 19: ...d the operating manual in whole are authorized to operate the centrifuge see 2 3 Informal Notes on Safety page 17 Keep informed about local fire prevention regulations and measures to contain harmful...

Страница 20: ...e Contact page 43 2 5 1 Special Hazards Do not open the lid when the rotor is in motion Do not reach into the rotor chamber when the rotor is in motion Do not use the centrifuge if the rotor is overlo...

Страница 21: ...s actuate the emergency switch at the exit if installed or in the room next door see 4 2 3 Fuses Emergency Circuit Breaker on Site page 24 Or Disconnect the main power plug Fire fighting measures or m...

Страница 22: ...Transport the centrifuge within suitable packaging and if at all possible in its original packaging 3 3 Notes on Storage The centrifuge can be stored for up to a year without any problems Store the ce...

Страница 23: ...wards When lifting or carrying the centrifuge always reach under the centrifuge from the side Attention The centrifuge weighs approx 13 kg Please retain the packaging for any possible future transport...

Страница 24: ...ance with DIN VDE 0700 and have a three wire power cord 2 5 m and a shockproof right angle plug On the back next to the mains power input there is an additional ground wire connector see Fig 5 2 page...

Страница 25: ...e centrifuge 1 7 8 1 Mains power switch 2 Stop key 3 Lid key 4 Lid 5 Display 6 Start key 7 Left rotary knob 8 Right rotary knob 6 3 2 9 Name plate 10 Equipotential bonding screw 11 Mains power input 9...

Страница 26: ...Display for rotor deceleration curve and programs 7 Rotary knobs Fig 5 3 Operating Panel 5 1 1 2 Name Plate 2 9 10 11 3 12 13 1 Manufacturer and registered office 2 Type name 4 5 6 7 8 1 Fig 5 4 Name...

Страница 27: ...ealed LCD display It is operated by way of two rotary knobs and indicates the operating statuses 5 1 5 Electronic System The microprocessor controlled electronic system ensures a wide range of adaptat...

Страница 28: ...Release page 42 5 1 6 2 Standstill Monitoring Opening of the centrifuge lid is only possible if the rotor is at a standstill This standstill is checked by the microprocessor 5 1 6 3 System Check An i...

Страница 29: ...losing the Lid The lid can be opened if the centrifuge is at a standstill and if the lid key is illuminated Press the lid key in order to open the lid see 5 3 7 Activating Deactivating the Automatic L...

Страница 30: ...old the rotor at its outer rim After frequent use the rotor tie down screw must be loosened by some turns and fastened again This must be done once a day or after 20 cycles This ensures a proper conne...

Страница 31: ...50 f Always load the opposite compartments of the rotors with the same accessories and filling to avoid imbalance Centrifugation with low capacity The tubes must be installed symmetrically so that the...

Страница 32: ...nstructions on safety and hazards in chapter 2 page 16 ff 5 2 5 Service Life of Rotors and Accessories The rotors and accessories have a limited service life Please perform regular checks at least onc...

Страница 33: ...whereas the softstop function is used to extend the deceleration time The current combination is shown on the display The stop key can be used to cyclically select various combinations Press the key o...

Страница 34: ...tion by pressing or turning the right rotary knob The set cursor will now flash Turn the right rotary knob until the desired duration is displayed Press the right rotary knob in order to confirm the i...

Страница 35: ...9 and the duration of the short run is also displayed When the start key is released the centrifuge decelerates at maximum power to a standstill 5 3 1 3 Continuous Run During the continuous run the r...

Страница 36: ...ht rotary knob The set cursor will now flash Turn the right rotary knob until the desired value is displayed Press the right rotary knob to confirm the selected value If this is not done the value wil...

Страница 37: ...to confirm the selected value If this is not done the value will be automatically reset to the last setting It is also possible to change the RCF value during a centrifugation run Fig 5 12 Setting the...

Страница 38: ...ty storage location numbers flash Press the right rotary knob to confirm the input The settings are now saved under this program number program number 8 in the example Fig 5 14 Saving programs here pr...

Страница 39: ...the help of the start key when the lid is open Press the start key three times and on the third time hold it down for approx two seconds After the activation of the function the padlock symbol Fig 5...

Страница 40: ...ing is displayed in the form of a message running over the display Auto Lid Open on or off 5 3 8 Activating Deactivating the Sound Signal If this function is active a sound signal can be heard at the...

Страница 41: ...ectly Fuse OK Replace fuse see fig 5 4 name plate page 26 Mains power switch on Switch on power Lid closed Close lid see 6 2 4 Lid cannot be opened page 42 6 2 2 Centrifuge cannot be started Start key...

Страница 42: ...to manually open the centrifuge lid using a stopper that is secured with a screw It is located on the front of the bottom panel Switch off the mains power switch and disconnect the power cord from th...

Страница 43: ...foreign matter from the opening of the lid lock device With error 50 and 51 the centrifuge will stop 60 69 Process error allow to slow down power off on With error 60 message power failure during run...

Страница 44: ...t generators 7 1 1 Centrifuge Disconnect the power cord from the socket before cleaning Carefully remove all liquids including water and particularly all the solvents acids and alkaline solutions from...

Страница 45: ...ke suitable precautions for your own safety if there is a risk of toxic radioactive or pathogenic contamination Dry the accessories with a soft cloth or in a drying chamber at approx 50 C 7 1 2 1 Plas...

Страница 46: ...rly at least once a month for cracks visible damage of the surface pressure marks signs of corrosion other changes Check the bores of the rotors Replace any damaged components immediately for your own...

Страница 47: ...approx 2 000 rpm The glass and metal particles will now collect at the greased part and can easily be removed with a cloth together with the grease Remove the grease with glass and metal particles wi...

Страница 48: ...30 40 20 Polypropylene tubes 115 118 30 40 30 Teflon tubes 134 138 3 5 100 Aluminum rotors 134 138 3 5 Polycarbonate Polyallomer lids for angle rotors 115 118 30 40 20 Polysulfone lids for angle roto...

Страница 49: ...her applicable local rules and regulations 8 2 Disposal of the Packaging Use the packaging to return the centrifuge for disposal Or Dispose of the packaging after having separated the individual mater...

Страница 50: ...round bottom tube approx 5 ml max 12 8 x 75 90 mm e g 15060 RIA or hemolyse tubes polypropylene 13072 Adapter for 1 round bottom tube 4 5 6 ml max 12 3 x 90 105 mm e g 15007 15027 polypropylene 15060...

Страница 51: ...accessories available upon request Maximum speed for tubes Some tubes such as centrifuge glass tubes microtubes culture tubes fluoropolymer tubes and especially high volume tubes can be used in our ro...

Страница 52: ...sentation of the rotors shows the maximum and minimum radii of the accessories used If necessary the values must be manually calculated see 11 1 1 RCF page 53 Fig 10 1 Minimum and maximum radius of an...

Страница 53: ...the resulting RCF will be recalculated If the RCF is altered the speed will be adapted accordingly under the consideration of the radius r radius in cm n speed in min 1 RCF without dimension 11 1 2 De...

Страница 54: ...Operating Manual SIGMA 1 6P page 54 of 67 05 2007 Abb 11 1 Drehzahl Schwerefeld Diagramm...

Страница 55: ...rve for maintaining the safety and health of our employees Fill out the forms and attach them when returning centrifuges accessories and spare parts Please understand that we cannot carry out any work...

Страница 56: ......

Страница 57: ...eclaration YES NO Decontamination declaration inside Unit component contaminated Unit component unused Thank you very much for a brief problem description This may reduce the repair costs Please make...

Страница 58: ......

Страница 59: ...acteristics of the substances Caustic Toxic Corrosive Explosive Biologically hazardous Radioactive In Combination with which substances can hazardous mixtures develop Names of the substances Have the...

Страница 60: ......

Страница 61: ...0 1 4 1 4 1 1 1 4 Benzaldehyde C7H6O 100 1 3 4 1 1 3 4 4 1 1 Benzene C6H6 100 3 2 4 1 3 4 4 1 1 Boric acid H3BO3 aqueous 1 3 1 2 1 1 1 Butyl acrylate C7H12O2 100 1 2 4 2 3 4 4 4 1 1 Butyl alcohol norm...

Страница 62: ...gen peroxide H2O2 3 1 3 1 1 1 1 1 1 3 Hydrogen peroxide H2O2 30 1 4 1 4 1 1 1 1 3 Hydrogen sulfide H2S 10 1 1 1 1 1 1 1 3 1 1 Iodine tincture of I2 1 4 3 1 1 4 4 1 1 Isopropyl alcohol C3H8O 100 1 1 1...

Страница 63: ...Na2CO3 10 1 1 1 1 1 1 3 Sodium chloride NaCl 30 1 1 1 1 1 1 1 1 1 3 Sodium hydroxide NaOH 30 1 1 4 1 1 1 1 1 1 4 Sodium hydroxide NaOH 50 1 1 4 1 1 1 1 1 4 Sodium sulfate Na2SO4 10 1 1 1 1 1 1 1 1 1 1...

Страница 64: ......

Страница 65: ...35 Corrosion chemical changes of the material surface 18 20 21 32 44 45 46 47 Cracks 21 32 46 Current consumption 13 Damage of the surface 46 Dangerous goods 19 Deceleration curves see also the softs...

Страница 66: ...36 37 39 43 53 Pathogenic substances material including pathogenes 20 44 45 47 Performance data 13 Power consumption 13 Power cord 24 41 42 44 Pressure marks 46 Prevention of accidents 11 17 Program 2...

Страница 67: ...Stress corrosion 46 Supply voltage 24 Toxic substances 18 20 44 45 Transport safety device 23 UV radiation 24 44 Ventilation 24 43 Operating Manual SIGMA 1 6P page 67 of 67 05 2007...

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