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Quick Start Guide

SERVO

PRO CHROMA/NANOCHROME/ULTRA Gas Analyser

13

04400003A_0

1.6.6 Historic values (F3)

Displays the last 20 measures of concentration and Area Counts for the selected
impurity. Select a peak in the upper-left grid of the

REAL-TIME

CHROMATOGRAM MENU

and then press the

Historic Values (F3)

button

to see these values (see Figure 8).

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Содержание 04400003A

Страница 1: ...Part Number 04400003A Revision 0 Language UK English SERVOPRO Chroma NanoChrome NanoChrome ULTRA QUICK START GUIDE...

Страница 2: ...Quick Start Guide SERVOPRO CHROMA NANOCHROME ULTRA Gas Analyser 1 04400003A_0...

Страница 3: ...istoric values F3 13 1 6 7 Historic Alarm F4 14 1 6 8 Range F5 14 1 6 9 Save F6 15 1 6 10 Undo Zoom F8 16 1 6 11 Print Alt F2 16 1 6 12 Remote Countdown 16 1 7 Historic Menu 16 1 7 1 Alarm Menu 16 1 8...

Страница 4: ...terials for the sampling system 40 3 3 2 Carrier Gas Hardware Selection 41 3 3 3 Gas Connections Rear Panel 42 1 Master and Secondary Chassis 42 2 Auxiliary Oven 43 3 3 4 Internal dilution system setu...

Страница 5: ...PRO CHROMA NANOCHROME ULTRA Gas Analyser 4 04400003A_0 LIST OF TABLES Table name Page Table 1 Peak Grid Alarm Status display colours 15 Table 2 Digital Output Contacts 36 Table 3 4 20 mA connections a...

Страница 6: ...Figure 11 Calibration Span menu 23 Figure 12 Calibration 4 20 mA outputs menu 24 Figure 13 Remote Software menu 26 Figure 14 About menu 27 Figure 15 Historic Chromatogram saving menu 28 Figure 16 Mas...

Страница 7: ...ntenance of the analyser including filter and fuse replacement must only be carried out by following the instructions in the operator manual WARNING This analyser is not a medical device as defined in...

Страница 8: ...socket 6 Gas trap outlet 7 Ethernet port 8 USB port 9 Analogue 4 20 mA outputs 10 Digital outputs 11 Digital input 12 Earth terminals for cable screens 13 Carrier gas inlet to detector 1 14 Carrier g...

Страница 9: ...tted to the secondary chassis in a system with a master chassis 1 Power inlet with switch and fuse 2 RS 485 port 3 Carrier gas inlet 4 Carrier gas vent 5 Detector 1 vent 6 Detector 2 vent 7 Sample gas...

Страница 10: ...is connected to the specific channel making the N2 determination and removes the small volume of interfering background gas which has co eluted with the N2 prior to the passing to the detector 1 3 2...

Страница 11: ...itch and fuse 2 RS 232 port for remote terminal marked AUX 3 RS 232 port for secondary unit marked TO ANALYSER 4 USB port 5 Ethernet port 1 5 User Interface Menu structure The analyser functions are g...

Страница 12: ...chromatogram The chromatogram presents all the peak data that can be configured in the CONFIGURATION CYCLE menu To access the RUN REAL TIME CHROMATOGRAM menu see Figure 6 press CTRL R or click on Run...

Страница 13: ...the peak detection process is completed the peak area is converted into the process value and displayed in the grid beside the peak name in the value field Then the analyser waits for other peaks and...

Страница 14: ...0003A_0 1 6 6 Historic values F3 Displays the last 20 measures of concentration and Area Counts for the selected impurity Select a peak in the upper left grid of the REAL TIME CHROMATOGRAM MENU and th...

Страница 15: ...s described in more detail in section 1 7 1 6 8 Range F5 Use the CONFIGURATION SYSTEM MENU to select either Manual or Automatic ranging If Manual ranging is selected press the Range button to toggle b...

Страница 16: ...nabled Warning Span Calibration enabled will be displayed in the chromatogram display with Enhanced View Off During both Threshold and Span calibration the Enhanced View radio control will be disabled...

Страница 17: ...en to identify the zone to zoom Releasing the left mouse button will apply the zoom Press the Undo Zoom button to show the original trending without any zoom 1 6 11 Print Alt F2 The Print button enabl...

Страница 18: ...low alarm is inactive Starting mode is automatic SYSTEM CONFIGURATION MENU for the Starting mode definition No cycle is progressing real time chromatogram stopped or between cycles Plasma ON When the...

Страница 19: ...llow If another alarm occurs it turns red again The button will turn green when all alarms are resolved Every system alarm will activate or deactivate the system status alarm dry contact output depend...

Страница 20: ...nalyser Calibration Note It is recommended to calibrate the analyser once a month Note Recommendation is to calibrate with between 80 110 of Full scale range Click on Calibration on the menu bar and t...

Страница 21: ...automatically switch to range 1 The calibration procedure is described below 1 Check that there is no cycle currently running Click on Run Real Time Chromatogram then select the Manual Injection opti...

Страница 22: ...ed for the process gas and sample inlet 2 is used for the span gas Pressing the Click for Span button will select analyser sample inlet 2 Diluted Value equals the Calib Gas Value column divided by the...

Страница 23: ...the calibration 9 Enable the Span Calibration with the Enable F3 button 10 In the Span column select Yes for the peaks that require calibration 11 Select All peaks or Selected peaks by changing the sl...

Страница 24: ...dilution values based on the dilution factor Calibration enabled will be displayed in the RUN REAL TIME CHROMATOGRAM menu It is recommended to perform the calibration in Automatic injection mode This...

Страница 25: ...Result column Automatic Re Span when the box is checked the analyser automatically performs a re span after a cycle of calibration reaches an end the same action as pressing the Re Span button This m...

Страница 26: ...tput to be calibrated Step 3 Connect an ammeter to the corresponding output on the rear panel of the analyser Step 4 Output a value between 0 and 100 eg 20 by entering the value in the edit box to the...

Страница 27: ...ess the REMOTE REPORT SOFTWARE menu see Figure 13 Figure 13 Remote Software menu This menu is used to configure the IP address of the analyser required to use the Report Software Two types of IP addre...

Страница 28: ...on About on the menu bar to access the ABOUT MENU Figure 14 About menu This menu shows the software version of the user interface PC the firmware versions of the embedded electronic boards and inform...

Страница 29: ...ive This will allow storage of around one month of continuous data depending on the complexity of the analysis When the stored data reaches 99 capacity the new data will over write the files starting...

Страница 30: ...l used space on the hard drive 1 12 2 Quit It is important to use the Quit button on the menu bar before the analyser is powered off If you close the analyser without using Quit there is the risk that...

Страница 31: ...iately contact Servomex or local Servomex agent 4 If the analyser is not going to be used immediately o Place the analyser and any other equipment supplied back in its protective packing o Store the a...

Страница 32: ...lectrical connections Figure 16 shows how to connect an analyser supplied with only a master chassis The master chassis must be connected to a power source using a properly rated cable see section Err...

Страница 33: ...nector named Auxiliary Oven see section operator manual1 2 1 The cable carries the power supply and the temperature measurement The master chassis communicates with the secondary chassis using RS 485...

Страница 34: ...e SERVOPRO CHROMA NANOCHROME ULTRA Gas Analyser 33 04400003A_0 Secondary Chassis 2 Connect both RS 485 ports using the provided high density DB 9 cable Figure 18 Master with 2 Secondary Chassis electr...

Страница 35: ...upplied connect the cable coming out of the auxiliary oven to the connector named Auxiliary Oven on the stand alone PC The cable carries the power supply and the temperature measurement The stand alon...

Страница 36: ...t on Secondary Chassis 2 Both connections should use the provided high density DB 9 cable see section Error Reference source not found and Figure 20 Figure 20 Stand alone PC with two Secondarys electr...

Страница 37: ...ure 21 Digital input connection WARNING The digital input terminals are separated from the analyser mains circuits by reinforced insulation The terminals must only be connected to circuits that are th...

Страница 38: ...s level of protection 3 2 3 4 20 mA outputs The schematic of the 4 20 mA output circuit is shown in Figure 23 Use a shielded twisted cable to connect between the analyser and the monitoring system wit...

Страница 39: ...HR HR F9 Table 3 4 20 mA connections and associated fuses WARNING The analogue output terminals are separated from the analyser mains circuits by reinforced insulation The terminals must only be conn...

Страница 40: ...ing the optional RS 232 port The computer is connected to the analyser by the mean of a DB 9 RS 232C Null modem cable The computer must have appropriate software to read the data transmitted by the an...

Страница 41: ...egulator valve line fitting filter purifier etc which is in contact with the sample or carrier gas to be introduced into the analyser Even small leaks can introduce external contaminants originally no...

Страница 42: ...grade cylinder gas through a gas purifier to generate the carrier gas 1 Gas Purifier The SERVOPRO PureGas purifier is available with either compression or VCR fittings and for use with 110V or 220VAC...

Страница 43: ...ting of a master chassis a master chassis with one or more secondary chassis or a PC with one or more secondary chassis If required each chassis may be fitted with an external oven 1 Master and Second...

Страница 44: ...nnector The oven Outlet gas connector is taken to the analyser chassis Trap Out gas connector VCR tubing should be used in all cases 3 3 4 Internal dilution system setup NanoChrome and Ultra only The...

Страница 45: ...1 to 6 for all chassis CAUTION A SERVOPRO Chroma NanoChrome Ultra may consist of multiple chassis Each chassis has its own internal dilution system which will require verification of the dilution rat...

Страница 46: ...caps are removed Do not pressurise detector vent s The carrier gas must be connected to the analyser before power is applied 1 Verify main voltage rating 2 Connect carrier gas purifier and follow inst...

Страница 47: ...Use a gas sniffer 13 Note It is necessary to purge the optional internal dilution system To purge the internal dilution system go into Calibration Calibration menu and click the button Click for Span...

Страница 48: ...calibrate the analyser see Section 1 9 Then run the analyser continuously on calibration gas for 12 injections Verify that the last 4 results are within repeatability specification Compare with result...

Страница 49: ...ious calibration procedure This will ensure the same sample volume is injected The default value is 50 cc min per channel 4 Clean the cabinet fan filter periodically This will support effective coolin...

Страница 50: ...pment in a clean dry area Do not subject it to excessively hot cold or humid conditions 6 2 Disposal Dispose of the analyser and any associated equipment safely and in accordance with the local and na...

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