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M99.0 

INSTALLATION 

MULTIVAP 118 

 
Dry Bath Setup   (Continued) 
 
6. 

Type-Z Purge Intrinsically Safe Bath option - If you do not have this option, please  

 

proceed  to  the  next  section.      Procedures  for  operating  this  system  may  be  found  in  the 

 

Operation Section.   Quick start instructions are posted on the front of the bath.   A copy 

 

of  the  NFPA  (National  Fire  Protection  Assoc.)  guidelines  for  intrinsically  safe  equip-

 

ment are in the appendix.   Please refer to Figure 3 below for parts list and installation.  

 
 

A. 

Install the Type Z Purge Gauge Assembly to the rear of the bath as shown.    The  

 

 

bracket attaches to the rear of the bath and is held in place by a 6-32 x 1/4” screw  

 

 

on the  shoulder spacer and by a 1/4” bulkhead hex nut on the gas inlet fitting. 

 
 

B. 

Connect the small white silicone tube attached to the gauge to the gas inlet fitting  

 

 

using the compression nut provided. 

 
 

C. 

Attach the filter with 5 foot tube to the plastic elbow fitting located at the base of  

 

 

the bath.   Insert the filter into the fitting and tighten the nut.   Connect the tube to  

 

 

a clean gas source. 

 
 

D. 

Test the system by turning on the gas flow to the Z Purge System.   Adjust the  

 

 

gas flow until the gauge reads 0.1 inches water pressure. 

 
 

WARNING -  If this unit is located in a hazardous area where volatile fumes are present,  

 

 

 

the Z-Purge System must be activated for a minimum of 10 minutes prior  

 

 

 

to activation of bath power.   Please review the Safety and Operations  

 

 

 

sections.                                                                                                                       

FIGURE 3 

1

2

3

4

5

6

7

8

11

12

Gauge and Housing

1/4 White Silicone Tube

10/32 x 1/4 Screw

Tube Fitting Nut

3/8 OD Clear Tube

Bulkhead Hex Nut

Filter

Plastic Elbow Fitting

Shoulder Spacer

Gas Inlet Fitting

Front

Z-Purge Assembly Diagram - Side View

Содержание MULTIVAP 118

Страница 1: ...MULTIVAPTM Nitrogen Evaporation System Model 118 DIGITAL TIME CONTROL SYSTEM INSTRUCTION MANUAL ORGANOMATION ASSOCIATES INC 266 RIVER ROAD WEST BERLIN MA 01503 U S A Tel 888 838 7300 Fax 978 838 2786 ...

Страница 2: ......

Страница 3: ...on Type Z Purge Intrinsically Safe Bath Option Bath Operation Instrument Operation Optimization Maintenance and Cleaning Trouble Shooting Technical Information Parts List Service and Returns Shipping Claims for damage or shortage Specifications UL Underwriters Laboratories Warranty Wiring Diagrams Z Purge NFPA Guidelines Accessories Other Products and Services Contacting Organomation and its Repre...

Страница 4: ...en evaporation system 48 Position MULTIVAP Nitrogen evaporation system 80 Position MULTIVAP Nitrogen evaporation system Flow meter Assembly with Mounting Bracket Connector Tube 0 30 or 0 100 LPM for all Model 118 MULTIVAP 1 ea 11809 11815 11830 11848 2 ea 11880 19 ga x 4 Stainless Steel Needles blunt end 30 48 80 each for respective models and positions 14 ga x 4 Stainless Steel Needles blunt end ...

Страница 5: ...e SS needles and on the MULTIVAP 30 48 60 or 96 pieces are provided with the respective MULTIVAP size ordered reference part NA0637 MULTIVAP Instrument and OA SYS heating unit are coated in Teflon Instrument is black in color The water bath exterior is blue and the heat block is black Pasteur Pipet fittings as above provided with Teflon coated unit SS Needles 19 gauge x 4 100mm Long are coated in ...

Страница 6: ...LTIVAP Nitrogen Evaporation System is designed for general evaporation and or concentration of analytical or biological samples in a variety of test tube based glassware under controlled and reproducible conditions The complete instrument is shown below Figure 1 ...

Страница 7: ...fold On Off gas control for each manifold row Rotate to raise and lower manifold Stand rod for manifold has geared grooves Delivers gas to each sample Teflon coated for acid resistance Aligns needles into sample tubs Optional Allows different diameter sample tubes in heat block Dry block and control system SS tube connects flow meter to manifold Gas delivery system with swing away feature Connects...

Страница 8: ... 3 wire grounded electrical outlet rated for 220 240 VAC 50 60 Hz single phase 15 amps 5 GFCI Ground Fault Circuit Interrupter is an optional safety device which may be present For 110 120 VAC baths the GFCI plugs into the wall outlet and the plug at the end of the power cord plugs into the GFCI For 220 240 VAC baths this item is located inline on the power cord approximately 12 inches behind the ...

Страница 9: ... Connect the small white silicone tube attached to the gauge to the gas inlet fitting using the compression nut provided C Attach the filter with 5 foot tube to the plastic elbow fitting located at the base of the bath Insert the filter into the fitting and tighten the nut Connect the tube to a clean gas source D Test the system by turning on the gas flow to the Z Purge System Adjust the gas flow ...

Страница 10: ...e connector tube to the bulkhead fitting located on the left rear corner of the control box C Connect the 1 4 plastic tube from the control box to the lower fitting on the flow meter D Connect the Connector Tube to a clean gas source Air or Nitrogen Source should be capable of being regulated down to 30 psig maximum If source is in excess of 30 psig then Organomation part NA0630 Pressure Reducing ...

Страница 11: ...nect the SS Gas Tube into the swivel fitting at the top of the instrument Insert the tube into the fitting as far as it will go approximately 1 2 inch 13mm B Connect the lower end of the SS Gas Tube to the fitting on the top of the flow meter Secure with a wrench 5 Connect the coiled black connector tube to the fitting located on the lower back right corner of the control box Press firmly into pla...

Страница 12: ... the needles be installed from the back forward B Pasteur Pipet Adapters Carefully push the pipet onto the Pasteur pipet adapter Install the pipet PPA assembly into the Luer fitting at the bottom of the manifold assembly by rotating 1 2 turn 15cm glass pipets are recommended Needles or PPA s may be used interchangeably in the MULTIVAP at the same time Note It is recommended that the needle guide p...

Страница 13: ... steps which may be necessary for your specific application or material 1 Thoroughly review your MSDS Material Safety Data Sheets for all chemicals to be used with this equipment 2 Do not use this equipment with materials with auto ignition points below 150 ºC 3 Hand and eye protection are required when using this product Additional protection may be required with respect to the materials being us...

Страница 14: ...m Time Light Green indicates timed operation in progress Alert Light Red indicates timed operation complete or inactive Heat Light Amber indicates heat system is active Gas Light Amber indicates gas system is active ON OFF Switch Green Lighted Rocker ALERT Indicator Red Light TIME System ON Green Light HEAT System ON Amber Light GAS System ON Amber Light HEAT Switch ON OFF ON GAS Switch ON OFF ON ...

Страница 15: ...enclosure is replaced multiple times ensuring that no flammable vapors remain which may have entered while the purge system was inactive Active vs Passive OAI currently offers two versions of the Type Z Purged system The passive system is not tied to the electric heating system in any way It is up to the operator to maintain the positive differential pressure within the system during operation The...

Страница 16: ...ree tubing is used on the manifold The black connector tube is polyurethane and internal tubing is polyethylene both of which are Phthalate free CAUTION Samples containing ether based fuel munitions or other extremely flammable or explosive materials compounds or residues should not be used in this equipment unless the heating unit is equipped with the TYPE Z Purged Intrinsically Safe Bath Option ...

Страница 17: ...t depress and hold the key Release when done 4 Manual Gas and Heat Control A To operate the heat system manually depress the heat switch to the lower position The Amber heat light will glow indicating the heat system is active Temperature will be controlled by the digital temperature controller B To operate the gas system manually depress the gas switch to the lower position The Amber gas light wi...

Страница 18: ...am C Program C is DELAY OPERATE time function D Set the right hand dial to 0 1H This will allow time settings to tenths The three center dials may be set to the correct number of hours with the right hand most dial representing 0 1 hours Calculate the amount of time that will elapse from the point the bath will be left until it will be needed the following day less 1 hour for heat up time Example ...

Страница 19: ...vaporative times to dryness an addition period of time should be allowed prior to shutdown Ten to twenty minutes should be adequate Example You wish to process 18 samples in 16 x 100mm test tubes to dryness Experience has shown that this takes approximately 25 minutes to complete As you are expected in a meeting which may take an hour or more you should use the automatic time system as there is no...

Страница 20: ... for operation of the timed system with unattended operation and shut down The following procedures will help to improve accuracy for each run A Set the pressure regulator to a position high enough to meet all flow require ments 20 30 PSIG should be sufficient for most applications B Open each row valve with sample 1 5 revolutions C Gas flow to each position should be increased to 0 5 LPM Position...

Страница 21: ...he aluminum inserts in the heating unit The manifold may be swung away for easy loading 8 Swing the manifold back so that it is positioned over the samples 9 Close all the gas toggle valves located on top of the manifold Valves are closed when the toggle is flipped towards the front of the unit 10 Open the valves for the rows which are to be used To open the valves flip the toggle towards the rear...

Страница 22: ...et to manual For timed operations make the necessary adjustments to the timer and press the start button on the control panel Reference the timed operation instructions in the bath operation section for proper use 17 When the evaporation is complete turn off the heating unit and gas flow 18 Swing the manifold out of the way and lift the test tube rack out of the heating unit 19 The unit may now be...

Страница 23: ...e or gray should be cleaned with non abrasive materials only otherwise scratching will result and the coating will be compromised Acidic Environment When in contact with or exposed to acidic materials vapors or samples The instrument should be cleaned immediately after use and neutralized with a suitable mild base solution of Sodium bicarbonate or similar material followed by a clean water wipe Pr...

Страница 24: ...rvice highly recommended Clean carefully with steel wool Remove source of acidic presence Return unit to factory to be coated in Teflon Purchase Phthalate free tubing Exercise better handling procedures avoid latex gloves hand cream rubber tubing Check all connections soap water Close needle valves open valves one revolution and adjust flow using flow meter Use algaecide change bath water once per...

Страница 25: ...LLER ON OFF SWITCH SOLID STATE RELAY 1 2 3 4 HIGH TEMPERATURE PROTECTION SWITCH DUAL CIRCUIT FLAT HEATER SOLENOID 1 RED ALERT LIGHT 2 GREEN TIME LIGHT 3 AMBER GAS LIGHT 4 AMBER HEAT LIGHT 5 MOMENTARY TIME SWITCH 6 DPST GAS SWITCH 7 DPST HEAT SWITCH 8 DUAL CIRCUIT FLAT HEATER 9 THERMOCOUPLE PROBE 1 2 3 4 9 8 5 6 7 120 VOLT ...

Страница 26: ...LLER ON OFF SWITCH SOLID STATE RELAY 1 2 3 4 HIGH TEMPERATURE PROTECTION SWITCH DUAL CIRCUIT FLAT HEATER SOLENOID 1 RED ALERT LIGHT 2 GREEN TIME LIGHT 3 AMBER GAS LIGHT 4 AMBER HEAT LIGHT 5 MOMENTARY TIME SWITCH 6 DPST GAS SWITCH 7 DPST HEAT SWITCH 8 DUAL CIRCUIT FLAT HEATER 9 THERMOCOUPLE PROBE 1 2 3 4 9 8 5 6 7 240 VOLT ...

Страница 27: ...ts will allow the item to shift in transit and may result in damage 3 Insurance Most common carriers offer insurance UPS and Federal Express automatically insure your product up to 100 00 without charge It is highly recommended that you insure your product Organomation is not liable for any return shipping damages 4 Documentation When returning items to Organomation a packing slip or other documen...

Страница 28: ...nual for a list of items affiliated with your purchase 3 Contact Organomation immediately at 888 838 7300 4 If a damaged item needs to be replaced Organomation will send this item under warranty at no charge The damaged item must be returned to Organomation Please follow the instructions listed in the Service and Returns section Important items not returned or which are further damaged or destroye...

Страница 29: ...as 5 30 Psig adjustable Flow indication standard with all complete MULTIVAP systems Quiet air compressor available Glass or Plastic Test Tubes 10 29mm Dia x 10 160mm Long Scintillation Vials Centrifuge Tubes size range above Auto sampler vials size range above Consult OAI for optional smaller larger sizes Organic Solvents with Boiling Point range 30 140 Celsius Water and aqueous solutions Strong a...

Страница 30: ...harges on warranty items sent to the Customer will be paid by the Supplier 3 Glassware is the responsibility of the Customer after receipt of shipment 4 Shipping damage and shortage must be claimed within 15 days of receipt of the shipment 5 Negligence abuse misuse or alteration of the product shall void the warranty Use of this product beyond its intended purpose shall void the warranty Damage ca...

Страница 31: ...odels 12060 12080 12090 12008 12027 12037 12010 12018 12048 12065 12085 12095 12005 12025 12035 12012 12015 Rot X Tract S solid liquid extractor models 13070 13080 13090 13008 13075 13085 13095 13005 Rot X Tract L liquid liquid extractor models 13318 13305 13308 13310 14060 All of the above wired for 110 and 220 volts 2 option code All of the above with thermostat or electronic digital temperature...

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