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22

 

Troubleshooting 

 

 

Cooling fault diagnosis 

Ensure that all connections to the stage and Dewar are as described in the specific user guide and that the 

stage lid and top windows are properly sealed.

 

 

 

1.  The cooling rate is less than programmed

 

There can be several causes of this problem, the most likely being that one of the connectors has 

become blocked or damaged.  Check that each tube is fitted tightly to the connector and that none 

of the tubing is twisted or has come lose.  The larger diameter tube leading from the LNP96 

 

consists of a tube within a tube, check that the internal tube is connected, it may have come loose.  

Any  constrictions  of  either  the  tubing  or  the  connector  will  have  a  drastic  effect  on  the  cooling 

ability of the LNP96.  If the connectors and  tubing are OK, check that the capillary tubing to the 

Dewar flask is not bent or damaged and that the filter is intact and unblocked.  If any damage has 

occurred to any of these items, they should be replaced. If no damage is found, check that the silver 

block is not constricted.  This can be checked, simply by blowing through one of the steel cooling 

tubes using a compressed air line.

 

 

2.

 

Condensation and ice forming on the upper side  of window

 

 

Realign the window gas tube clip to the required position in the stage lid.

 

 

 

3.

 

Condensation on the sample and/or the underside of lid window

 

 

This is due to the stage not being sealed properly and therefore allowing moisture in during purging 

or cooling.  Check that the lid and bottom window are sealed correctly and that the silicon seals are 

in position.  

 

 

 

 

 

Please visit 

www.Linkam.co.uk

 for more FAQs for the stage and instruments.

 

Содержание LTS420

Страница 1: ...LTS420 Temperature Controlled Stage USER GUIDE Linkam Scientific Instruments...

Страница 2: ...2 This page is intentionally Blank...

Страница 3: ...Water Circulation Pump 9 Sample preparation 10 Loading a Sample 10 Using the Heat Shield 11 Cooling Connections 12 Filling the Liquid Nitrogen Dewar 13 Purging Procedure 13 Purging the Stage Method 1...

Страница 4: ...oducts that prove to be defective For warranty service or repair this product must be returned to Linkam or a designated service facility The warranty shall not apply to defects resulting from interfa...

Страница 5: ...f for any reason it gets wet unplug it from the mains and contact Linkam Scientific Technical Support 6 The equipment is not intended to be used outdoors 7 If any problems occur turn all Linkam equipm...

Страница 6: ...and a T96 LinkPad System Controller allowing for stand alone control of heating Further options to enhance the system include LNP96 S liquid nitrogen cooling pump for cooling below ambient temperature...

Страница 7: ...ole 2 5mm 12 Pure Silver Heating cooling block 43x53mm 13 Heating Cooling Block Support 14 Y manipulator 15 X manipulator 16 Liquid nitrogen cooling connector 17 Stainless steel cooling tube for liqui...

Страница 8: ...the heating element Using the two positioning screws 2 ensure that the aperture is in the centre of the field of view and lock the stage in place by tightening the Locking Thumbscrew 3 For other type...

Страница 9: ...age above 300 C for more than a couple of minutes the metal body of the stage can get quite hot The Water Circulation Pump is used to cool the metal casing Connect the tubing as shown in the picture o...

Страница 10: ...ith a little force to help it to hold the microscope glass slide Place a standard microscope glass slide 26x76mm in the Microscope Slide Holder use a spatula and tap on the microscope glass slide to m...

Страница 11: ...over the microscope slide so that it rests on the heating element The sample is now heated from all sides enabling a very even temperature throughout the sample Heating rates may be slightly compromis...

Страница 12: ...e side of this white connector is the Gas Purging Tube 3 There is a valve opening Insert connector 4 inserted into the end of this tube During the purging procedure insert this connector into the Gas...

Страница 13: ...a LinkPad or LINK software please refer to the relevant user guide Filling the Liquid Nitrogen Dewar Please follow your health and safety user guide for directions on how to handle liquid nitrogen an...

Страница 14: ...nector found on the opposite side to the purging tube and seal the narrow window tube to block it This action will divert all of the nitrogen gas to the purging tube and through the Stage Chamber 6 Wi...

Страница 15: ...he gas regulator to set a gas flow rate of 1L min 5 With the gas flowing through the Sample Chamber block the gas outlet for a few seconds and releasing the gas outlet valve with a finger Repeat this...

Страница 16: ...site and reassembled in the order indicated The Lid Insert should be screwed down until the cover slips are held firmly then turn the assembly over and screw down the Lid Insert until it is felt to co...

Страница 17: ...the 2 holes on the holder are lined up with the two notches 2 on the XY Manipulator Assembly Note when fitted properly the Microscope Slide Holder should not touch the silver heating block 4 the hold...

Страница 18: ...nly read the following if the stage is supplied with internal electrical contacts for the LTSE420 or Liquid Crystal Pro Stage The stage is supplied with two internal electrical contact connectors 1 wi...

Страница 19: ...Contact The internal electrical contact has a self closing spring loaded pin 1 Using a finger tip push in the pin to open the electrical contact and insert a wire into the contact 2 Release the finge...

Страница 20: ...ug by holding it firmly and pull it gently away from the Stage Wire up the Lemo to your instrument To reconnect the Lemo line up the red dot on the Lemo plug 1 to the red dot on the Lemo socket 2 and...

Страница 21: ...d Crystal Holder 1 to the XY Assembly as shown on page 17 Note make sure the Liquid Cell Holder is the right way up as shown in the opposite picture Connect the two wires from the Liquid Cell Holder t...

Страница 22: ...oling ability of the LNP96 If the connectors and tubing are OK check that the capillary tubing to the Dewar flask is not bent or damaged and that the filter is intact and unblocked If any damage has o...

Страница 23: ...23 This page is intentionally Blank...

Страница 24: ...Instruments Ltd Tel 44 0 1737 363 476 Fax 44 0 1737 363 480 Email support linkam co uk Linkam Scientific Instruments Ltd Unit 9 Perrywood Business Park Honeycrock Lane Salfords RH1 5DZ UK www linkam...

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